固溶时效对节镍型高氮奥氏体不锈钢组织的影响

doi:10.13251/j.issn.0254-6051.2020.02.023

金属热处理 ›› 2020, Vol. 45 ›› Issue (2): 120-124.DOI: 10.13251/j.issn.0254-6051.2020.02.023

固溶时效对节镍型高氮奥氏体不锈钢组织的影响

常金宝¹, 赵英利¹, 嵇爽¹, 张福利¹, 杨现亮¹, 裴建明²

1. 河钢集团钢研总院, 河北石家庄 052165;
2. 燕山大学机械工程学院, 河北秦皇岛 066000

收稿日期:2019-08-25 出版日期:2020-02-25 发布日期:2020-04-03
通讯作者: 嵇爽(1992—),男,硕士,工程师,主要从事不锈钢研究工作,E-mail:779533356@qq.com
作者简介:常金宝(1968—),男,教授级高工,主要从事钢铁材料的研发与生产,E-mail:hbisjs@126.com。

Effect of solution treatment and aging on microstructure of low-nickel high nitrogen austenitic stainless steel

Chang Jinbao¹, Zhao Yingli¹, Ji Shuang¹, Zhang Fuli¹, Yang Xianliang¹, Pei Jianming²

1. HESTEEL Group Technology Research Institute, Shijiazhuang Hebei 052165, China;
2. College of Mechanical Engineering, Yanshan University, Qinhuangdao Hebei 066000, China

Received:2019-08-25 Online:2020-02-25 Published:2020-04-03

摘要/Abstract

摘要：

对热轧态节镍型高氮奥氏体不锈钢进行固溶及时效处理,利用光学显微镜、电子背散射衍射,结合相图系统分析该材料固溶处理及时效后组织变化规律。结果表明,1050 ℃固溶处理后,试验钢基体为奥氏体,存在少量的铁素体,奥氏体晶粒形状偏等轴,晶粒内部存在大量孪晶。时效后,析出相主要为Cr₂N、CrN、Cr₂₃C₆。在时效时间为5 h不变的条件下,温度由650 ℃升高至800 ℃,碳化物及氮化物数量呈现先增长后降低的趋势,在750 ℃时数量最多。而在750 ℃时效5~10 h范围内,随着时效时间的增加,析出相数量变化不大。析出相的析出过程为:先在晶界交叉处析出胞状析出物,随时间的延长,在晶界逐渐析出条状析出物,在晶内开始出现并逐渐长大,最终形成类珠光体的片层状析出。

关键词: 节镍型高氮奥氏体不锈钢, 固溶处理, 时效, 微观组织

Abstract:

Solid solution treatment and aging of hot rolled low-nickel high nitrogen austenitic stainless steel were carried out. Metallographic microscope, electron backscatter diffraction and phase diagram were used to systematically analyze the microstructure changes of the steel after solid solution treatment and aging. The results show that after solid solution treatment at 1050 ℃, the steel matrix is austenite with nearly equiaxial grains containing a large number of twins, and with a small amount of ferrite. After aging, the precipitated phases are mainly Cr₂N, CrN, and Cr₂₃C₆. With the increase of aging temperature from 650 ℃ to 800 ℃ under the same aging time of 5 h, the amounts of carbides and nitrides increase first and then decrease, reaching to the maximum at 750 ℃. With the increase of aging time in the range of 5-10 h at 750 ℃, the amount of precipitates has little change. The precipitation process of the precipitated phases is as follows: Firstly, cellular precipitation occurs at the triple junctions of grain boundaries. With the extension of aging time, strip precipitates are gradually precipitated at the grain boundaries, and begin to appear and grow up inside the grains, finally form pearlite-like lamellar precipitates.

Key words: low-nickel high nitrogen austenitic stainless steel, solution treatment, aging, microstructure

中图分类号:

TG142.1

常金宝, 赵英利, 嵇爽, 张福利, 杨现亮, 裴建明. 固溶时效对节镍型高氮奥氏体不锈钢组织的影响[J]. 金属热处理, 2020, 45(2): 120-124.

Chang Jinbao, Zhao Yingli, Ji Shuang, Zhang Fuli, Yang Xianliang, Pei Jianming. Effect of solution treatment and aging on microstructure of low-nickel high nitrogen austenitic stainless steel[J]. HTM, 2020, 45(2): 120-124.

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固溶时效对节镍型高氮奥氏体不锈钢组织的影响

Effect of solution treatment and aging on microstructure of low-nickel high nitrogen austenitic stainless steel

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