非线性超声表征HR3C钢时效过程中析出相的变化

doi:10.13251/j.issn.0254-6051.2020.02.048

金属热处理 ›› 2020, Vol. 45 ›› Issue (2): 242-249.DOI: 10.13251/j.issn.0254-6051.2020.02.048

非线性超声表征HR3C钢时效过程中析出相的变化

范德良¹, 王志武¹, 袁廷碧²

1. 武汉大学动力与机械学院, 湖北武汉 430072;
2. 国电科学技术研究院, 北京 102209

收稿日期:2019-08-28 出版日期:2020-02-25 发布日期:2020-04-03
通讯作者: 王志武,教授,博士,联系电话:13807153446,E-mail:wzw1618@163.com
作者简介:范德良(1994—),男,硕士研究生,主要从事奥氏体不锈钢的组织与性能研究,E-mail:fandeliang@foxmai.com。
基金资助:
国家自然科学基金(51071113)

Precipitated phase change of HR3C steel during aging characterized by nonlinear ultrasonic technique

Fan Deliang¹, Wang Zhiwu¹, Yuan Tingbi²

1. School of Power and Mechanical Engineering, Wuhan University, Wuhan Hubei 430072, China;
2. Guodian Science and Technology Research Institute, Beijing 102209, China

Received:2019-08-28 Online:2020-02-25 Published:2020-04-03

摘要/Abstract

摘要：

研究了HR3C钢在700和750 ℃下时效过程的组织演变,并用非线性超声技术来进行表征。在时效过程中主要析出相为M₂₃C₆和Z相,其总体面积分数和平均直径随着时效时间和温度的增加而增加。用非线性超声技术对时效试样进行测量,试验结果表明,非线性超声系数也随着时效时间和温度的增加而增加,其上升趋势和析出相的总面积分数呈现一定的相关性。这说明非线性超声系数对析出相的变化趋势敏感,可以用来表征HR3C钢时效过程中的微观结构变化。

关键词: HR3C钢, 时效, 非线性超声技术, 微观结构, 析出相

Abstract:

Microstructure change of HR3C steel during long-term aging at 700 ℃ and 750 ℃ was studied and characterized by nonlinear ultrasonic technique. Test results show that the main precipitated phases are M₂₃C₆ and Z-phase during aging, and their total area fraction and average diameter increase with the increase of aging time and temperature. The aged specimens were measured by nonlinear ultrasonic technique. The results show that the nonlinear ultrasonic coefficient increases with the increase of aging time and temperature, and the rising trend is correlated with the total area fraction of the precipitated phases, which indicates that the nonlinear ultrasonic coefficient is sensitive to the change of precipitates and can be used to characterize the microstructure change of HR3C steel during aging.

Key words: HR3C steel, aging, nonlinear ultrasonic technique, microstructure, precipitated phase

中图分类号:

TG142.73

范德良, 王志武, 袁廷碧. 非线性超声表征HR3C钢时效过程中析出相的变化[J]. 金属热处理, 2020, 45(2): 242-249.

Fan Deliang, Wang Zhiwu, Yuan Tingbi. Precipitated phase change of HR3C steel during aging characterized by nonlinear ultrasonic technique[J]. HTM, 2020, 45(2): 242-249.

参考文献

[1]于鸿垚, 董建新, 谢锡善. 新型奥氏体钢HR3C的研究进展[J]. 世界钢铁, 2010(2): 42-49.
Yu Hongyao, Dong Jianxin, Xie Xishan. Research Development of new austenitic heat-resistant steel HR3C[J]. World Iron & Steel, 2010(2): 42-49.
[2]方圆圆, 赵杰, 李晓娜. HR3C高温时效过程中的析出相[J]. 金属学报, 2010, 46(7): 844-849.
Fang Yuanyuan, Zhao Jie, Li Xiaona. Precipitates in HR3C steel aged at high temperature[J]. Acta Metallurgica Sinica, 2010, 46(7): 844-849.
[3]Wang Wei, Wang Zhiwu, Li Wensheng, et al. Evolution of M₂₃C₆phase in HR3C steel aged at 650 ℃[J]. Materials at High Temperatures, 2016, 33(3): 276-282.
[4]Bai X, Pan J, Chen G, et al. Effect of high temperature aging on microstructure and mechanical properties HR3C heat resistant steel[J]. Materials Science and Technology, 2014, 30(2): 205-210.
[5]Wang Xiao, Wang Xue, Niu Xiaoguang, et al. Application of nonlinear ultrasonic technique to characterize the creep damage in ASME T92 steel welded joints[J]. NDT&E International, 2018, 8(16): 8-16.
[6]John H Cantrell, William T Yost. Effect of precipitate coherency strains on acoustic harmonic generation[J]. Journal of Applied Physics, 1997, 81(7): 2956-2962.
[7]Daniel Marino, Jin Yeon Kim, Alberto Ruiz, et al. Using nonlinear ultrasound to track microstructural changes due to thermal aging in modified 9%Cr ferritic martensitic steel[J]. NDT&E International, 2016, 79: 46-52.
[8]Wang Xue, Wang Xiao, Hu Xianlong, et al. Damage assessment in structural steel subjected to tensile load using nonlinear and linear ultrasonic techniques[J]. Applied Acoustics, 2019, 144: 40-50.
[9]Cantrell John H, Zhang X G. Nonlinear acoustic response from precipitate-matrix misfit in a dislocation network[J]. Journal of Applied Physics, 1998, 84(10): 5468-5472.
[10]Wang Bin, Liu Zhengdong, Cheng Shichang, et al. Microstructure evolution and mechanical properties of HR3C steel during long-term aging at high temperature[J]. Journal of Iron and Steel Research, International, 2014, 21(8): 765-773.
[11]李铁英, 石治峰, 雷宏刚, 等. 金属材料损伤描述及损伤演化[J]. 工程力学, 2001(增刊): 298-302.
Li Tieying, Shi Zhifeng, Lei Honggang, et al. Damage description and evolution of metal materials[J]. Engineering Mechanics, 2001(S): 298-302.
[12]Kyung Young Jhang. Applications of nonlinear ultrasonics to the NDE of material degradation[J]. IEEE Transaction on Ultrasonics Ferroelectrics and Frequency Control, 2000, 47(3): 540-548.

[1]	张子延, 陈君, 陈晓亚, 李全安, 刘建鑫. 固溶时效处理对Mg-4Sm-3Gd-0.5Zr合金显微组织和耐蚀性能的影响[J]. 金属热处理, 2022, 47(4): 10-16.
[2]	陈东俊, 李广阳, 刘刚. 时效处理对AlSi9Cu3压铸铝合金组织和力学性能的影响[J]. 金属热处理, 2022, 47(4): 53-56.
[3]	陈思君, 陈送义, 陈庚, 袁丁玲, 陈康华. Mg含量对2A14铝合金组织和力学性能的影响[J]. 金属热处理, 2022, 47(4): 86-92.
[4]	孙凯, 陈研, 杨绍斌. 时效温度对激光选区熔化TC21钛合金微观组织及硬度的影响[J]. 金属热处理, 2022, 47(4): 155-158.
[5]	胡静, 陶科, 杨庆松, 李刚, 张德汉. 机械抛光后的时效工艺对0Cr25Al5电热合金拉拔性能的影响[J]. 金属热处理, 2022, 47(4): 171-177.
[6]	孙建, 黄贞益, 李景辉, 王萍. 固溶和时效处理对Fe-Mn-Al-C轻质钢组织和硬度的影响[J]. 金属热处理, 2022, 47(3): 34-38.
[7]	杨春苗, 王珊, 王淑慧, 李延珍, 刘文文. RRA过程中预时效时间对7A85铝合金组织性能的影响[J]. 金属热处理, 2022, 47(3): 44-47.
[8]	熊金生, 宁静, 苏杰, 姜庆伟. 淬火温度对低钴二次硬化钢组织和性能的影响[J]. 金属热处理, 2022, 47(3): 92-96.
[9]	姜中涛, 汪鑫, 周志明, 林海涛, 杨绪盛, 代芳芳. 双级固溶工艺对7050铝合金组织与力学性能的影响[J]. 金属热处理, 2022, 47(3): 102-106.
[10]	郝天赐, 吴雍壕, 阴树标, 曹建春, 罗瀚宇. Zr对Ti-Mo复合微合金化钢形变奥氏体静态再结晶动力学和析出相的影响[J]. 金属热处理, 2022, 47(2): 41-47.
[11]	闵旭东, 黄元春, 肖政兵, 刘宇, 任贤魏, 邹倜. 预处理对汽车用Al-Mg-Si合金组织和晶间腐蚀行为的影响[J]. 金属热处理, 2022, 47(2): 78-85.
[12]	曾煜, 吴畏, 莫燕. 一种汽车发动机气阀用节镍型高温合金的固溶时效工艺[J]. 金属热处理, 2022, 47(2): 188-192.
[13]	邱旭扬帆, 杨卓越, 丁雅莉. 提高Cr-Ni-Mo-Ti马氏体时效不锈钢超低温韧性的固溶处理工艺[J]. 金属热处理, 2022, 47(1): 44-48.
[14]	强菲, 王文, 张婷, 杨娟, 蔡军, 王快社. Al-Zn-Mg-Cu铝合金厚板搅拌摩擦焊接头搅拌区微观组织[J]. 金属热处理, 2022, 47(1): 135-141.
[15]	崔岩, 董和谦, 曹雷刚, 杨越, 蒙毅. 55%SiC_p/2024Al复合材料时效过程的微观组织与力学性能[J]. 金属热处理, 2022, 47(1): 142-148.

非线性超声表征HR3C钢时效过程中析出相的变化

Precipitated phase change of HR3C steel during aging characterized by nonlinear ultrasonic technique

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价