金属热处理 ›› 2022, Vol. 47 ›› Issue (7): 221-226.DOI: 10.13251/j.issn.0254-6051.2022.07.038

• 表面工程 • 上一篇    下一篇

超声冲击处理S30408不锈钢的微观组织演变与电化学性能

王振飞1, 杨新俊1,2   

  1. 1.江南大学 机械工程学院, 江苏 无锡 214122;
    2.江南大学 江苏省食品先进制造装备技术重点实验室, 江苏 无锡 214122
  • 收稿日期:2022-01-26 修回日期:2022-04-30 出版日期:2022-07-25 发布日期:2022-08-12
  • 通讯作者: 杨新俊,副教授,硕士生导师,E-mail: xinjun_yang@163.com
  • 作者简介:王振飞(1996—),男,硕士研究生,主要研究方向为特种设备延寿技术,E-mail:748158688@qq.com。
  • 基金资助:
    国家自然科学基金(51505189);国家重点研发计划(2018YFA0704604)

Microstructure evolution and electrochemical properties of S30408 stainless steel treated by ultrasonic impact treatment

Wang Zhenfei1, Yang Xinjun1,2   

  1. 1. School of Mechanical Engineering, Jiangnan University, Wuxi Jiangsu 214122, China;
    2. Jiangsu Key Laboratory of Advanced Food Manufacturing Equipment & Technology, Jiangnan University, Wuxi Jiangsu 214122, China
  • Received:2022-01-26 Revised:2022-04-30 Online:2022-07-25 Published:2022-08-12

摘要: 通过超声冲击处理(UIT)方法在S30408奥氏体不锈钢表面构筑梯度纳米结构,通过XRD、硬度测试、光学显微镜、扫描电镜和电化学测试等方法研究了超声冲击时间对试验钢表层纳米微观结构和耐腐蚀性能的影响。结果表明,超声冲击处理后在材料表层产生了一定深度的硬化层,同时引入了残余压应力,且残余压应力和硬度均随着超声冲击时间的增加而增加,在超声冲击时间为300 s时分别达到最大值740.12 MPa和82.22 HRB。超声冲击处理后试样表层观察到呈梯度变化的微观结构,可分为纳米层、剧烈塑性变形层和基体。超声冲击使表层晶粒得到细化,并引发了马氏体转变,超声冲击时间为300 s时的晶粒尺寸最小,马氏体转变量最大,分别为14.82 nm和39.80%。超声冲击处理对S30408不锈钢耐蚀性能的影响是晶粒尺寸、残余应力、马氏体相变含量、表面缺陷等因素共同作用的结果,超声冲击时间为180 s时试样的耐蚀性最好,自腐蚀电流密度为1.22 μA/cm2

关键词: 超声冲击处理, 梯度纳米结构, 马氏体, 电化学, 腐蚀

Abstract: Gradient nanostructure was constructed on the surface of S30408 austenitic stainless steel by using ultrasonic impact treatment (UIT), and the effect of different ultrasonic impact time on surface nanostructure and corrosion resistance of the steel was studied by means of XRD, hardness test, optical microscope, scanning electron microscope and electrochemical test. The results show that after ultrasonic impact treatment, a certain depth of hardened layer is produced on the surface of the material, and the residual compressive stress is introduced. Moreover, both hardness and residual compressive stress increase with the increase of ultrasonic impact time, and reach the maximum 740.12 MPa and 82.22 HRB respectively when the ultrasonic impact time is 300 s. Gradient microstructure is observed on the surface of the steel after ultrasonic impact treatment, which can be divided into nanocrstalline layer, severe plastic deformation layer and matrix. The ultrasonic impact process refines the surface grains and induces martensite transformation, as the grain size is the smallest and the martensite transformation is the largest when the ultrasonic impact time is 300 s, which are 14.82 nm and 39.80%, respectively. The effect of ultrasonic impact treatment on corrosion resistance of the S30408 stainless steel is the result of the joint action of grain size, residual stress, martensitic transformation content, surface defects and so on. When the ultrasonic impact time is 180 s, the corrosion resistance of the specimen is the best, and the self-corrosion current density is 1.22 μA/cm2.

Key words: ultrasonic impact treatment, gradient nanostructure, martensite, electrochemistry, corrosion

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