热处理温度对Al-Gd合金凝固组织和硬度的影响

doi:10.13251/j.issn.0254-6051.2022.08.031

金属热处理 ›› 2022, Vol. 47 ›› Issue (8): 182-187.DOI: 10.13251/j.issn.0254-6051.2022.08.031

热处理温度对Al-Gd合金凝固组织和硬度的影响

石向东^1,2,3, 李德贵^1,2, 曹阿林^1,2, 古斌^1,2, 梁柳青^1,2

1.百色学院材料科学与工程学院, 广西百色 533000;
2.广西壮族自治区铝基新材料工程研究中心, 广西百色 533000;
3.中国热处理行业协会, 北京 100101

收稿日期:2022-03-20 修回日期:2022-06-21 出版日期:2022-08-25 发布日期:2022-09-19
通讯作者: 李德贵,副教授,博士,E-mail:lidegui354@163.com
作者简介:石向东(1972—),男,高级工程师,博士,主要研究方向为金属材料组织与性能,E-mail:sxdcd@126.com。
基金资助:
国家自然科学基金 (51861001);广西自然科学基金联合资助培育项目(2018GXNSFAA138133);广西高等教育本科教学改革工程项目(2021JGZ157)

Effect of heat treatment temperature on solidification microstructure and hardness of Al-Gd alloy

Shi Xiangdong^1,2,3, Li Degui^1,2, Cao Alin^1,2, Gu Bin^1,2, Liang Liuqing^1,2

1. School of Materials Science and Engineering, Baise University, Baise Guangxi 533000, China;
2. Engineering Research Center of Aluminum-based New Materials of Guangxi Zhuang Autonomous Region, Baise Guangxi 533000, China;
3. China Heat Treatment Association, Beijing 100101, China

Received:2022-03-20 Revised:2022-06-21 Online:2022-08-25 Published:2022-09-19

摘要/Abstract

摘要： 对真空电弧炉熔炼后的Al-52%Gd(质量分数)合金在不同温度下进行热处理,利用光学显微镜、扫描电镜、洛氏硬度计等研究了不同加热温度对其凝固组织和硬度的影响。结果表明,当加热温度为600 ℃时,初晶相由粗大发达树枝晶被较均匀的等轴晶取代;共晶相的形态由片网状向短杆状、点状过渡,生长方式逐渐由附着在初晶相周围生长向独立生长转变;硬度的变化为随着加热温度升高先下降后上升再迅速下降,中心硬度值与均值硬度在不同加热温度下有所差异,主要由凝固组织的疏松和初晶相Al₃Gd的形态与分布决定。

关键词: 热处理温度, Al-Gd合金, 凝固组织, 硬度

Abstract: Al-52%Gd(mass fraction)alloy smelted by vacuum arc furnace was heat treated at different temperatures. The effect of heating temperature on solidification microstructure and hardness of the Al-52%Gd alloy was studied by means of optical microscope, scanning electron microscope, Rockwell hardness tester and so on. The results show that the primary crystal phase changes from coarse developed dendrites to more uniform equiaxed crystals when the heating temperature is 600 ℃. The morphology of eutectic phase transforms from lamellar network to short rod and dot, and the growth mode gradually changes from attaching the primary phase to independence. As the heating temperature increases, the hardness decreases first, then increases and then rapidly decreases. The central hardness value and average hardness value have difference at different heating temperatures, which is mainly determined by the porosity of solidification microstructure as well as the morphology and distribution of primary phase Al₃Gd.

Key words: heat treatment temperature, Al-Gd alloy, solidification microstructure, hardness

中图分类号:

TG166.3

石向东, 李德贵, 曹阿林, 古斌, 梁柳青. 热处理温度对Al-Gd合金凝固组织和硬度的影响[J]. 金属热处理, 2022, 47(8): 182-187.

Shi Xiangdong, Li Degui, Cao Alin, Gu Bin, Liang Liuqing. Effect of heat treatment temperature on solidification microstructure and hardness of Al-Gd alloy[J]. Heat Treatment of Metals, 2022, 47(8): 182-187.

参考文献

[1]孙学智, 罗朝晖. 全球乏燃料后处理现状与分析[J]. 核安全, 2016, 15(2): 13-16.
Sun Xuezhi, Luo Zhaohui. Status of global spent fuel reprocessing[J]. Nuclear Safety, 2016, 15(2): 13-16.
[2]霍嘉杰, 郑岳山, 姚琳, 等. 乏燃料干法贮存标准和监管要求浅析[J]. 核安全, 2019, 18(5): 13-18.
Huo Jiajie, Zheng Yueshan, Yao Lin, et al. Analysis of standards and supervision requirement of dry storage for spent fuel[J]. Nuclear Safety, 2019, 18(5): 13-18.
[3]王玉容, 赵勇, 蒋明忠, 等. 功能/结构一体化中子屏蔽材料的研究现状[J]. 精密成形工程, 2019, 2(3): 166-170.
Wang Yurong, Zhao Yong, Jiang Mingzhong, et al. Research status in neutron shielding materials with combined functional and structural performance[J]. Journal of Netshape Forming Engineering, 2019, 2(3): 166-170.
[4]李刚, 简敏, 王美玲, 等. 反应堆乏燃料贮运用中子吸收材料的研究进展[J]. 材料导报A, 2011, 25(7): 110-113.
Li Gang, Jian Min, Wang Meiling, et al. Research progress in neutron absorbers materials for reactor spent fuel storage and transportation applications[J]. Materials Review A, 2011, 25(7): 110-113.
[5]何林, 蔡永军, 李强. 中子和伽马射线综合屏蔽材料研究进展[J]. 材料导报A, 2018, 32(4): 1107-1113.
He Lin, Cai Yongjun, Li Qiang. Research progress in radiation shielding materials serving as the combined barrier against neutron and gamma-ray[J]. Materials Review A, 2018, 32(4): 1107-1113.
[6]Wang W, Xiong L, Zhu H Y, et al. Segregation of B in steel and remelting phenomenon after solidification of SS400B-bearing steel[J]. Journal of Iron and Steel Research, 2015, 27(2): 36-40.
[7]Murari F D, Silva A V, Avillez R R. Cold-rolled multiphase boron steels: Microstructure and mechanical properties[J]. Journal of Materials Research and Technology, 2015, 4(2): 191-196.
[8]Tsubota M, Oikawa M. Boron-bearing stainless steels for thermal neutron shielding[J]. Bullutin of the Iron and Steel Institute of Japan, 2005, 10(12): 25-32.
[9]佴启亮, 郑文杰, 宋志刚, 等. 硼含量对含硼不锈钢组织和性能的影响[J]. 钢铁研究学报, 2013, 25(6): 53-57.
Nai Qiliang, Zheng Wenjie, Song Zhigang, et al. Effect of boron content on microstructure and property of boron stainless steel[J]. Journal of Iron and Steel Research, 2013, 25(6): 53-57.
[10]元琳琳, 韩静涛, 刘靖, 等. 热中子屏蔽用高硼不锈钢复合板的组织与性能[J]. 材料热处理学报, 2015, 36(8): 104-110.
Yuan Linlin, Han Jingtao, Liu Jing, et al. Microstructure and performance of high boron stainless steel composite plate for neutron shielding[J]. Transactions of Materials and Heat Treatment, 2015, 36(8): 104-110.
[11]Electric Power Research Institute. Handbook of neutron absorber materials for spent nuclear fuel transportation and storage applications-2009 edition[R]. American: EPRI, 2009.
[12]Moldovan P, Popesus G. The grain refinement of 6063 aluminum using Al-5Ti-1B and Al-3Ti-0.15C grain refiners[J]. JOM, 2004, 56(11): 59-63.
[13]Electric Power Research Institute. Pressurized water reactor chemically enhanced ultrasonic fuel cleaning: Feasibility study[R]. American: EPRI, 2009.
[14]Machiels A, Lindquist K O. Qualification of METAMIC for Spent Fuel Storage Application[M]. California: Electric Power Research Institute, 2001.
[15]王莉雅. 中子准直器用金属隔片组织与性能的研究[D]. 沈阳: 中国科学院金属研究所, 2015.
Wang Liya. The microstructure and properties of metal spacer for neutron soller collimator[D]. Shenyang: Institute of Metal Research, Chinese Academy of Sciences, 2015.
[16]田娜, 井晓天, 卢正欣, 等. 稀土和镍含量对Al-Gd-Er-Ni金属玻璃初晶化的影响[J]. 材料热处理学报, 2007, 28(3): 39-43.
Tian Na, Jing Xiaotian, Lu Zhengxin, et al. Influence of rare earth and Ni content on the primary crystallization of Al-Gd-Er-Ni metallic glass[J]. Transactions of Materials and Heat Treatment, 2007, 28(3): 39-43.
[17]田瑞, 罗林, 肖学山. 多元Gd(Tb)-Ni-Al合金系中非晶形成能力的成分依赖性研究[J]. 中国稀土学报, 2008, 6(3): 363-367.
Tian Rui, Luo Lin, Xiao Xueshan. Composition dependence of glass-forming ability in Gd(Tb)-Ni-Al alloys[J]. Journal of the Chinese Rare Earth Society, 2008, 6(3): 363-367.
[18]Bykov V, Uporov S, Kulikova T. Thermal conductivity of Al-Gd-TM glass-forming alloys[J]. Transactions of Nonferrous Metals Society of China, 2015, 25: 1911-1916.
[19]静永娟, 张继. 热处理对γ-TiAl合金中Gd化合物的影响研究[J]. 金属功能材料, 2013, 20(3): 32-35.
Jing Yongjuan, Zhang Ji. Effect of heat-treatment on Gd-compound of TiAl alloys[J]. Metallic Functional Material, 2013, 20(3): 32-35.
[20]刘楚明, 蒋树农, 陈志永, 等. 铝合金相图集[M]. 长沙: 中南大学出版社, 2014.
Liu Chuming, Jiang Shunong, Chen Zhiyong, et al. Aluminum Alloy Phase Atlas[M]. Changsha: Central South University Press, 2014.

热处理温度对Al-Gd合金凝固组织和硬度的影响

Effect of heat treatment temperature on solidification microstructure and hardness of Al-Gd alloy

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	周丽娜, 刘明, 高翔, 王文雪, 童锐. 奥氏体化过程对Cr14Mo4V高温轴承钢微观组织的影响[J]. 金属热处理, 2022, 47(8): 7-15.
[2]	何博, 彭天恩, 胡学文, 蒋波, 郭锐, 石践, 汪飞, 王海波. Nb对高Ti耐候钢连续冷却后显微组织及硬度的影响[J]. 金属热处理, 2022, 47(8): 46-51.
[3]	彭龙生, 林英华, 黄伟, 陈皓. 感应淬火对Cr12MoV钢轧辊硬度和硬化层深度的影响[J]. 金属热处理, 2022, 47(8): 118-122.
[4]	魏海霞, 潘吉祥, 纪显斌, 李照国, 徐斌. 热处理对经济型高碳马氏体不锈钢J50Cr13组织和硬度的影响[J]. 金属热处理, 2022, 47(8): 148-151.
[5]	李向川, 杨吉春, 白国君, 樊志明. 热处理对U76CrRE稀土重轨钢夹杂物和微观组织的影响[J]. 金属热处理, 2022, 47(8): 200-210.
[6]	田春英, 董纪, 王军, 张慧星, 冯天建, 刘晓凡. 淬火温度对5Cr15MoV钢空冷淬火组织与性能的影响[J]. 金属热处理, 2022, 47(8): 211-216.
[7]	朱德荣, 李豪, 柳翊, 王利鸽, 陈智勇, 张慧贤, 梁莉. 固溶时效对SLM成形316L不锈钢块体件显微组织及硬度的影响[J]. 金属热处理, 2022, 47(8): 237-241.
[8]	刘港, 刘静, 杨峰, 向庆. 钛合金化学热处理研究进展[J]. 金属热处理, 2022, 47(8): 249-256.
[9]	魏永强, 顾艳阳, 赵重轻, 蒋志强. 脉冲偏压占空比对TiSiN薄膜结构和性能的影响[J]. 金属热处理, 2022, 47(8): 279-286.
[10]	牛毅, 贺占胥, 王明利, 张杰, 牛文朋, 刘贯军. 离子渗氮对304不锈钢组织和性能的影响[J]. 金属热处理, 2022, 47(8): 287-291.
[11]	郑洪, 林文钦, 杨元熙, 徐心洁, 邓枫, 吴佳欣, 蒋洪俊. 30CrMnSiA合金前端吊耳断裂原因分析[J]. 金属热处理, 2022, 47(8): 292-295.
[12]	钟修杨, 邓同生, 朱志云, 李尚, 钟明, 郭涛. 时效处理对稀土钪微合金化钛合金组织与性能的影响[J]. 金属热处理, 2022, 47(7): 40-46.
[13]	索忠源, 杜阳, 付立铭, 单爱党. 配分工艺对5CrMnNiMo超高强度钢摩擦磨损性能的影响[J]. 金属热处理, 2022, 47(7): 134-137.
[14]	蒋文淼, 胡志华, 栾道成, 张旭, 凌俊华, 阴志铭, 李缘, 周新宇, 王正云. 新型贝氏体板簧钢的组织及性能[J]. 金属热处理, 2022, 47(7): 151-155.
[15]	李春辉, 李晓源, 尉文超, 王毛球, 吴润. 冷却速度对超高强马氏体钢的马氏体相变起始温度和硬度的影响[J]. 金属热处理, 2022, 47(7): 183-189.