成品退火工艺对Cu-20wt%Fe原位复合带材组织和性能的影响

doi:10.13251/j.issn.0254-6051.2022.10.028

金属热处理 ›› 2022, Vol. 47 ›› Issue (10): 169-172.DOI: 10.13251/j.issn.0254-6051.2022.10.028

成品退火工艺对Cu-20wt%Fe原位复合带材组织和性能的影响

曾延琦¹, 余辉辉¹, 陆德平¹, 张友亮¹, 胡强¹, 郭军力¹, 胡斐斐², 邹晋^1,3

1.江西省科学院应用物理研究所, 江西南昌 330096;
2.江西铜业集团铜板带有限公司, 江西南昌 330096;
3.中国科学院江西稀土研究院, 江西赣州 341001

收稿日期:2022-05-26 修回日期:2022-08-24 出版日期:2022-10-25 发布日期:2022-12-15
通讯作者: 邹晋,副研究员,博士,E-mail: zoujin@jxas.ac.cn
作者简介:曾延琦(1987—),男,高级工程师,硕士,主要研究方向为先进铜基复合材料的制备加工,E-mail: zengyanqi@jxas.ac.cn。
基金资助:
江西省重大科技研发专项(20212AAE01003);江西省重点研发计划(20202BBEL53022);江西省科学院重点科研开发项目(2020-YZD-07);江西省科学院稀土专项(2020-YZD-2)

Effect of finished product annealing process on microstructure and properties of Cu-20wt%Fe in-situ composite strip

Zeng Yanqi¹, Yu Huihui¹, Lu Deping¹, Zhang Youliang¹, Hu Qiang¹, Guo Junli¹, Hu Feifei², Zou Jin^1,3

1. Institute of Applied Physics, Jiangxi Academy of Sciences, Nanchang Jiangxi 330096, China;
2. Jiangxi Copper Corporation Copper Strip Company Limited, Nanchang Jiangxi 330096, China;
3. Jiangxi Rare-earth Academy, Chinese Academy of Sciences, Ganzhou Jiangxi 341001, China

Received:2022-05-26 Revised:2022-08-24 Online:2022-10-25 Published:2022-12-15

摘要/Abstract

摘要： 通过拉伸性能和导电率测试、扫描电镜微观组织观察和能谱分析,研究了不同成品退火工艺下Cu-20wt%Fe原位复合带材的抗拉强度、导电率和富铁相的变化规律。结果表明,经退火处理后,部分厚度较小的富铁相可以回溶到铜基体中,随着退火温度的升高,富铁相回溶增多,残留的扁长富铁相最终呈断续分布。带材抗拉强度随退火时间的延长先显著下降至380~440 MPa,随后下降速率明显放缓,甚至出现轻微波动上升,最终趋于平稳,而退火温度越高,抗拉强度越低。带材导电率随退火时间的延长迅速提高至31%IACS~37%IACS,随后变化缓慢、略有波动,最终趋于平稳。Cu-20wt%Fe原位复合带材较理想退火工艺为450 ℃×60 min。

关键词: Cu-20wt%Fe, 原位复合材料, 带材, 显微组织, 抗拉强度, 导电率

Abstract: Varying rules of tensile strength, electrical conductivity and iron-rich phase evolution of Cu-20wt%Fe in-situ composite strips under different finished product annealing processes were studied by means of tensile test, electrical conductivity test, SEM microstructure observation and energy spectrum analysis. The results show that after annealing, some iron-rich phases with small thickness can be dissolved into copper matrix. With the increase of annealing temperature, the dissolution of iron-rich phase increases, and the residual flat and long iron-rich phases eventually distribute intermittently. With the extension of annealing time, the tensile strength of the strip first decreases significantly to 380-440 MPa, then the decline rate slows down significantly, even fluctuates up slightly, and finally tends to be stable, meanwhile, the tensile strength decreases with the increase of annealing temperature. The conductivity of the strip increases rapidly to 31%IACS-37%IACS with the extension of annealing time, then changes slowly, fluctuates slightly, and finally tends to be stable. The ideal finished product annealing process for Cu-20wt%Fe in-situ composite strip is at 450 ℃ for 60 min.

Key words: Cu-20wt%Fe, in-situ composite, strip, microstructure, tensile strength, electrical conductivity

中图分类号:

TG146.31

曾延琦, 余辉辉, 陆德平, 张友亮, 胡强, 郭军力, 胡斐斐, 邹晋. 成品退火工艺对Cu-20wt%Fe原位复合带材组织和性能的影响[J]. 金属热处理, 2022, 47(10): 169-172.

Zeng Yanqi, Yu Huihui, Lu Deping, Zhang Youliang, Hu Qiang, Guo Junli, Hu Feifei, Zou Jin. Effect of finished product annealing process on microstructure and properties of Cu-20wt%Fe in-situ composite strip[J]. Heat Treatment of Metals, 2022, 47(10): 169-172.

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成品退火工艺对Cu-20wt%Fe原位复合带材组织和性能的影响

Effect of finished product annealing process on microstructure and properties of Cu-20wt%Fe in-situ composite strip

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