热处理对激光增材制造IN718合金组织及析出相演变的影响

doi:10.13251/j.issn.0254-6051.2023.02.028

金属热处理 ›› 2023, Vol. 48 ›› Issue (2): 180-188.DOI: 10.13251/j.issn.0254-6051.2023.02.028

热处理对激光增材制造IN718合金组织及析出相演变的影响

曹宇^1,2,3, 白朴存¹, 魏安妮¹, 刘飞¹, 侯小虎¹

1.内蒙古工业大学材料科学与工程学院, 内蒙古呼和浩特 015000;
2.呼伦贝尔学院机电工程学院, 内蒙古呼伦贝尔 021008;
3.内蒙古自治区矿产资源开采与综合利用研究中心, 内蒙古呼伦贝尔 021008

收稿日期:2022-09-08 修回日期:2022-12-08 出版日期:2023-02-25 发布日期:2023-03-22
通讯作者: 白朴存,教授,博士,E-mail:Pcbai@imut.edu.cn
作者简介:曹宇(1988—),女,副教授,博士,主要研究方向为金属材料微观组织结构,E-mail:ngdcaoyu@126.com。
基金资助:
国家自然科学基金(11672140);内蒙古自治区矿产资源安全开采与综合利用研究中心重点项目(2021KZZD04);内蒙古自治区高校科研一般项目(NJZY23051)

Effect of heat treatment on microstructure and precipitate evolution of IN718 alloy prepared by laser additive manufacturing

Cao Yu^1,2,3, Bai Pucun¹, Wei Anni¹, Liu Fei¹, Hou Xiaohu¹

1. School of Materials Science and Engineering, Inner Mongolia University of Technology, Hohhot Inner Mongolia 015000, China;
2. School of Mechanical and Electrical Engineering, Hulunbuir University, Hulunbuir Inner Mongolia 021008, China;
3. Research Center for Mining and Comprehensive Utilization of Mineral Resources of Inner Mongolia Autonomous Region, Hulunbuir Inner Mongolia 021008, China

Received:2022-09-08 Revised:2022-12-08 Online:2023-02-25 Published:2023-03-22

摘要/Abstract

摘要： 研究了经过固溶+双时效(SA)、均匀化+双时效(HA)、均匀化+固溶+双时效(HSA)3种热处理后IN718合金的微观组织、析出相的演变。结果表明,沉积态试样中的显微组织为柱状晶结构,并贯穿多个沉积层;经过SA热处理后开始发生再结晶;经HA和HSA热处理后再结晶程度显著提高。热处理能够促进沉积态中的柱状晶逐渐向等轴晶转变。沉积态试样中存在γ基体、Laves相和一些碳化物;经过SA热处理后溶解了大部分的Laves偏析相,并在晶界、晶内、枝晶间析出大量的针状δ相,还有部分碳化物残留;经过HA热处理后,Laves偏析相、δ相全部溶解,只有少量的碳化物残留;经过HSA热处理后Laves偏析相全部溶解,在晶界处析出部分δ相,还有少量的碳化物残留。沉积态试样中没有γ′、γ″相析出,3种热处理状态均有大量的γ′、γ″相析出。

关键词: 激光增材制造, IN718高温合金, 热处理, 析出相

Abstract: Evolution of microstructure and precipitates of the IN718 alloy after heat treatments was investigated by using solid solution+double aging(SA), homogenization+double aging(HA), homogenization+solid solution+double aging(HAS), respectively. The results show that the microstructure in the as-deposited specimen is a columnar crystal microstructure and runs through multiple sedimentary layers. Recrystallization occurs after SA heat treatment. Recrystallization is significantly improved after heat treatment of HA and HSA. Heat treatment can promote the progressive transformation of columnar crystals into equiaxed crystals. There are γ matrix, Laves segregation phase and some carbides in the as-deposited specimen. After SA heat treatment, most of the Laves segregation phase is dissolved, and a large number of acicular δ phases precipitate between the grain boundaries, the crystals, and the dendrites, and some carbides remain. After HSA heat treatment, the Laves segregation phase is completely dissolved, and some δ phase precipitate at the grain boundary, and a small amount of carbides retain. There is no γ′ and γ″ phase precipitated in the as-deposited specimen, and a large number of γ′ and γ″ phases precipitate in the three heat treatment states.

Key words: laser additive manufacturing, IN718 superalloy, heat treatment, precipitates

中图分类号:

TG156

曹宇, 白朴存, 魏安妮, 刘飞, 侯小虎. 热处理对激光增材制造IN718合金组织及析出相演变的影响[J]. 金属热处理, 2023, 48(2): 180-188.

Cao Yu, Bai Pucun, Wei Anni, Liu Fei, Hou Xiaohu. Effect of heat treatment on microstructure and precipitate evolution of IN718 alloy prepared by laser additive manufacturing[J]. Heat Treatment of Metals, 2023, 48(2): 180-188.

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热处理对激光增材制造IN718合金组织及析出相演变的影响

Effect of heat treatment on microstructure and precipitate evolution of IN718 alloy prepared by laser additive manufacturing

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