金属热处理 ›› 2023, Vol. 48 ›› Issue (2): 195-199.DOI: 10.13251/j.issn.0254-6051.2023.02.030

• 工艺研究 • 上一篇    下一篇

固溶处理对TC11钛合金组织与性能的影响

同晓乐1,3, 张明玉2, 岳旭1,3, 杨斌1, 王玉佳1, 阿热达克·阿力玛斯1   

  1. 1.新疆湘润新材料科技有限公司, 新疆 哈密 839000;
    2.大连交通大学 连续挤压教育部工程研究中心, 辽宁 大连 116028;
    3.新疆钛基新材料重点实验室, 新疆 哈密 839000
  • 收稿日期:2022-09-01 修回日期:2022-12-11 出版日期:2023-02-25 发布日期:2023-03-22
  • 通讯作者: 岳 旭,高级工程师,硕士, E-mail:yuexu100@163.com
  • 作者简介:同晓乐 (1987—),男,工程师,主要研究方向为钛合金塑性成形,E-mail: xjxrunjs@163.com。
  • 基金资助:
    自治区创新环境(人才、基地)建设专项(XJQY2009);自治区创新环境(人才、基地)建设专项—天山创新团队计划(2020D14041)

Effect of solution treatment on microstructure and properties of TC11 titanium alloy

Tong Xiaole1,3, Zhang Mingyu2, Yue Xu1,3, Yang Bin1, Wang Yujia1, Ardak Almas1   

  1. 1. Xinjiang Xiangrun New Materials Technology Co., Ltd., Hami Xinjiang 839000, China;
    2. Engineering Research Center of Continuous Extrusion,Dalian Jiaotong University,Dalian Liaoning 116028, China;
    3. Xinjiang Key Laboratory of Titanium-based New Materials, Hami Xinjiang 839000, China
  • Received:2022-09-01 Revised:2022-12-11 Online:2023-02-25 Published:2023-03-22

摘要: 通过光学显微镜、扫描电镜、X射线衍射仪以及室温拉伸性能测试,研究TC11钛合金分别在955、975、995和1015 ℃固溶处理后的微观组织与力学性能的对应关系。结果表明,合金原始锻态显微组织为α+β两相区锻造形成的双态组织,以αp相和β转变组织为主。经固溶处理后,原始锻态组织中被扭转和拉长的αp相随着固溶温度升高逐渐变小、变圆,同时体积较小的αp相逐渐消失。固溶温度为995 ℃时,合金强度达到最大值,抗拉强度(Rm)为1403 MPa,屈服强度(Rp0.2)为1158 MPa;固溶温度为955 ℃时,合金塑性最佳,断后伸长率(A)为9.5%,断面收缩率(Z)为32%。当固溶温度位于两相区时,其拉伸断口微观形貌相似,均以韧窝为主;当固溶温度位于单相区时,断口形貌结晶状明显,且有较大的撕裂棱,在岩石状表面有大量撕裂状小韧窝。

关键词: TC11钛合金, 固溶处理, 微观组织, 力学性能, 断口形貌

Abstract: Relationship between microstructure and mechanical properties of the TC11 titanium alloy after solution treatment at 955, 975, 995 and 1015 ℃, respectively, was studied by means of optical microscope, scanning electron microscope, X-ray diffraction and room temperature tensile test. The results show that the original as-forged microstructure of the alloy is a bimodal structure formed by forging in the α+β two-phase region, which is dominated by αp phase and β transformation structure. After solution treatment, the twisted and elongated αp phase in the original as-forged structure gradually becomes smaller and rounded with the increase of solution treatment temperature, and the smaller αp phase gradually disappears. When the solution treatment temperature is 995 ℃, the strengths of the alloy reach the maximum, of which the tensile strength (Rm) is 1403 MPa and the yield strength (Rp0.2) is 1158 MPa. When the solution treatment temperature is 955 ℃, the plasticity of the alloy is the best, of which the elongation after fracture (A) is 9.5% and the percentage reduction of area (Z) is 32%. When the solution treatment temperature is in the two-phase region, the tensile fracture morphology is similar, which is mainly dimples. When the solution treatment temperature is in the single-phase region, the fracture morphology is obviously crystalline and has large tearing edges, and there are a large number of small tearing dimples on the rock-like surface.

Key words: TC11 titanium alloy, solution treatment, microstructure, mechanical properties, fracture morphology

中图分类号: