金属热处理 ›› 2023, Vol. 48 ›› Issue (11): 230-234.DOI: 10.13251/j.issn.0254-6051.2023.11.037

• 工艺研究 • 上一篇    下一篇

退火处理对稀土镁合金组织和性能的影响

徐向美1, 王琪晨2, 马胜宾3   

  1. 1.烟台理工学院 信息工程学院, 山东 烟台 264005;
    2.中集海洋工程研究院有限公司, 山东 烟台 264670;
    3.辽宁农业职业技术学院, 辽宁 营口 115007
  • 收稿日期:2023-07-17 修回日期:2023-08-28 出版日期:2023-11-25 发布日期:2023-12-27
  • 通讯作者: 马胜宾,讲师,硕士,E-mail:547407381@qq.com
  • 作者简介:徐向美(1983—),女,讲师,硕士,主要研究方向为金属材料设计,E-mail:xuxiangmei3112@163.com。

Effect of annealing on microstructure and properties of a rare earth magnesium alloy

Xu Xiangmei1, Wang Qichen2, Ma Shengbin3   

  1. 1. College of Information Engineering, Yantai Institute of Technology, Yantai Shandong 264005, China;
    2. Department, CIMC Offshore Engineering Institute Co., Ltd., Yantai Shandong 264670, China;
    3. Liaoning Agricultural Vocational and Technical College, Yingkou Liaoning 115007, China
  • Received:2023-07-17 Revised:2023-08-28 Online:2023-11-25 Published:2023-12-27

摘要: 研究了退火制度对一种稀土镁合金微观组织演变和力学性能的影响。利用光学显微镜和扫描电镜观察显微组织,用XRD进行物相分析和织构分析,并在万能拉伸试验机上进行了力学性能测试。结果表明,随着退火温度的升高,形变孪晶逐渐消失,变形晶粒发生回复和再结晶,平均晶粒逐渐长大,由200 ℃时的6.35 μm长大到350 ℃时的12.45 μm,增大了96.1%。退火时间对稀土镁合金晶粒尺寸和织构构成的影响较小。稀土镁合金的基体晶内和晶界处分布着Al2Y相,在液相中结晶,同时在固相中析出,凝固过程抑制α-Mg结晶晶粒的长大,细化凝固态初始晶粒尺寸;Al2Y相在形变和热处理过程钉扎再结晶晶粒晶界,细化晶粒。随退火温度的升高,屈服强度和抗拉强度先降低后升高,伸长率先升高后降低。稀土镁合金试样经300 ℃保温60 min的退火处理后可获得最低的屈服强度和抗拉强度,分别为158 MPa和215 MPa,最高的伸长率16.0%。

关键词: 稀土镁合金, 退火, 微观组织, 力学性能

Abstract: Effect of annealing process on microstructure and mechanical properties of a rare earth magnesium was investigated. The microstructure was characterized by using optical microscope and scanning electron microscope. The phase constitution and texture were analyzed by using X-ray diffractometer. The mechanical properties were tested by means of universal tensile testing machine. The results indicate that as the annealing temperature increases, the deformation twins gradually disappear, and the deformed grains undergo recovery and recrystallization. The average grain size gradually grows from 6.35 μm at 200 ℃ to 12.45 μm at 350 ℃, increased by 96.1%. Annealing time has a little effect on the grain size and texture constitution of the rare earth magnesium alloy. The Al2Y phase is distributed within and at the grain boundaries of the matrix of the rare earth magnesium, which crystallizes in the liquid phase and precipitates in the solid phase, to inhibite the growth of crystalline grains during solidification, refine the initial grain size of the solidified state and pin the recrystallized grain boundaries during deformation and heat treatment processes to refine the grains. As the annealing temperature increases, the yield strength and tensile strength first decrease and then increase, and the elongation first increases and then decreases. After annealing at 300 ℃ for 60 min, the lowest yield strength and tensile strength of a rare earth magnesium alloy specimen can be obtained, with 158 MPa and 215 MPa, respectively, and the highest elongation is 16.0%.

Key words: rare earth magnesium alloy, annealing, microstructure, mechanical properties

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