金属热处理 ›› 2024, Vol. 49 ›› Issue (4): 83-88.DOI: 10.13251/j.issn.0254-6051.2024.04.014

• 组织与性能 • 上一篇    下一篇

长期时效对GH4169合金组织与性能的影响

陶天成, 臧凯, 朱治愿   

  1. 江苏科技大学 材料科学与工程学院, 江苏 镇江 212000
  • 收稿日期:2023-10-31 修回日期:2024-03-05 出版日期:2024-04-25 发布日期:2024-05-27
  • 通讯作者: 朱治愿,教授,博士,E-mail:salanganezhu@just.edu.cn
  • 作者简介:陶天成(1997—),男,硕士研究生,主要研究方向为镍基高温合金,E-mail:2363287042@qq.com。

Effect of long-term aging on microstructure and properties of GH4169 alloy

Tao Tiancheng, Zang Kai, Zhu Zhiyuan   

  1. School of Materials Science and Engineering, Jiangsu University of Science and Technology, Zhenjiang Jiangsu 212000, China
  • Received:2023-10-31 Revised:2024-03-05 Online:2024-04-25 Published:2024-05-27

摘要: 分析了GH4169合金经960 ℃×1 h+720 ℃×8 h+620 ℃×8 h标准热处理后再经650 ℃长期时效(100~4000 h)后的组织演变规律和力学性能,探究合金在长期时效过程中的组织演变与力学性能变化之间的关系。结果表明:合金在650 ℃时效100~800 h时,晶内会持续析出较多细小γ″、γ′相,晶界处伴有δ相析出,合金的硬度呈上升趋势;时效1600~2400 h时,γ″、γ′相逐渐长大,δ相逐渐粗化并且周围出现贫γ″区,合金硬度上升趋缓;时效3200~4000 h时,γ″、γ′相粗化明显且晶内大量γ″相转变为δ相,合金的硬度下降。长期时效过程中合金的抗拉强度及屈服强度变化规律与硬度一致,塑性呈现不断下降的趋势。

关键词: GH4169合金, 长期时效, 析出相, 力学性能

Abstract: After standard heat treatment of 960 ℃×1 h+720 ℃×8 h+620 ℃×8 h, GH4169 alloy was subjected to long-term aging at 650 ℃ for 100-4000 h. The microstructure evolution law mechanical properties and their relationship of the alloy during long-term aging was explored. The results show that after aging at 650 ℃ for 100-800 h, a large number of γ″ and γ′ phases precipitate in the grain, δ phase precipitates at the grain boundary, and the hardness of the alloy increases. After aging for 1600-2400 h, γ″ and γ′ phases grow up gradually, δ phase coarsens gradually and γ″ poor zone appears around the δ phase, and the alloy hardness increases slowly. After aging for 3200-4000 h, γ″ and γ′ phases coarsen obviously and a large number of γ″ phases change into δ phase, and the hardness of the alloy decreases. Meanwhile, the tensile strength and yield strength of the alloy after long-term aging are consistent with the change of hardness, and the plasticity shows a decreasing trend.

Key words: GH4169 alloy, long-term aging, precipitated phase, mechanical properties

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