加热温度和保温时间对Ti1023钛合金再结晶行为的影响

doi:10.13251/j.issn.0254-6051.2024.12.018

金属热处理 ›› 2024, Vol. 49 ›› Issue (12): 103-106.DOI: 10.13251/j.issn.0254-6051.2024.12.018

加热温度和保温时间对Ti1023钛合金再结晶行为的影响

李雪飞^1,2, 黄利军^1,2, 佟健博^1,2, 颜孟奇^1,2

1.中国航发北京航空材料研究院, 北京 100095;
2.中国航发先进钛合金重点实验室, 北京 100095

收稿日期:2024-09-27 修回日期:2024-11-09 出版日期:2024-12-25 发布日期:2025-02-05
作者简介:李雪飞(1989—),男,高级工程师,硕士,主要研究方向为高强高韧钛合金,E-mail:lixuefeiavic@163.com

Effects of heating temperature and holding time on recrystallization behavior of Ti1023 titanium alloy

Li Xuefei^1,2, Huang Lijun^1,2, Tong Jianbo^1,2, Yan Mengqi^1,2

1. AECC Beijing Institute of Aeronautical Materials, Beijing 100095, China;
2. AECC Key Laboratory of Advanced Aeronautical Titanium Alloys, Beijing 100095, China

Received:2024-09-27 Revised:2024-11-09 Online:2024-12-25 Published:2025-02-05

摘要/Abstract

摘要： 通过对Ti1023钛合金在两相区进行70%的锻造变形,并将其进行785~885 ℃保温30~300 min的热处理,观察分析不同加热温度和不同保温时间下变形组织的回复和再结晶规律。结果表明,Ti1023钛合金在两相区变形后,在800 ℃以下保温时,变形组织以发生回复为主,再结晶为辅,保留了变形后的组织形态,再结晶晶粒未发生长大。在800~885 ℃保温时,变形组织以发生再结晶为主,回复为辅。当加热温度一定时,随着保温时间延长,再结晶晶粒会发生长大;当保温时间一定时,加热温度越高,完成再结晶所需要的时间越短,晶粒长大的趋势越明显,再结晶晶粒长大不利于变形组织的细化。

关键词: Ti1023钛合金, 回复, 再结晶, 晶粒长大

Abstract: By forging 70% deformation of the Ti1023 titanium alloy in the two-phase region and heating at 785-885 ℃ for 30-300 min, the recovery and recrystallization law of the deformed microstructure under different heating temperatures and holding time were observed and analyzed. The results show that after the deformation of the Ti1023 titanium alloy in the two-phase region, the deformed microstructure is dominated by recovery when the heating temperature below 800 ℃, supplemented by recrystallization, the microstructure retains the deformed morphology, and the recrystallized grains don't grow. When heated at 800-885 ℃, the deformed microstructure is dominated by recrystallization, supplemented by recovery. When the heating temperature is constant and the holding time is prolonged, the recrystallized grains grow. When the holding time is constant, the higher the heating temperature, the shorter the time required to complete recrystallization, and the more obvious the trend of grain growth. The recrystallized grain growth is not conducive to the refinement of the deformed microstructure.

Key words: Ti1023 titanium alloy, recovery, recrystallization, grain growth

中图分类号:

TG335.6⁺2

李雪飞, 黄利军, 佟健博, 颜孟奇. 加热温度和保温时间对Ti1023钛合金再结晶行为的影响[J]. 金属热处理, 2024, 49(12): 103-106.

Li Xuefei, Huang Lijun, Tong Jianbo, Yan Mengqi. Effects of heating temperature and holding time on recrystallization behavior of Ti1023 titanium alloy[J]. Heat Treatment of Metals, 2024, 49(12): 103-106.

参考文献

[1]黄旭, 朱知寿, 王红红. 先进航空钛合金材料与应用[M]. 北京: 国防工业出版社, 2012.
Huang Xu, Zhu Zhishou, Wang Honghong.Advanced Aeronautical Titanium Alloys and Applications[M]. Beijing: National Defense Industry Press, 2012.
[2]马超, 王高潮. TB6钛合金定m值法高温超塑性拉伸试验研究[J]. 锻压技术, 2016, 41(10): 88-91.
Ma Chao, Wang Gaochao. Superplastic tensile experiment by the fixed m value method at high-temperature for titanium alloy TB6[J]. Forging and Stamping Technology, 2016, 41(10): 88-91.
[3]Goken J, Fayed S, Skubisz P. Strain-dependent damping of Ti-10V-2Fe-3Al at room temperature[J]. Acta Physica Polonica A, 2016, 130(6): 1352-1360.
[4]Illarionov A G, Trubochkin A V, Shalaev A M, et a1. Isothermal decomposition of β-solid solution in titanium alloy Ti-10V-2Fe-3Al[J]. Metal Science and Heat Treatment, 2017, 58(11/12): 674-684.
[5]Wu J F, Zou S K, Zhang Y K, et a1. Microstructures and mechanical properties of β forging Ti17 alloy under combined laser shock processing and shot peening[J]. Surface and Coatings Technology, 2017, 328: 283-291.
[6]Sun Z C, Wu H L, Sun Q F, et a1. Tri-modal microstructure in high temperature toughening and low temperature strengthening treatments of near-β forged TAl5 Ti-alloy[J]. Materials Characterization, 2016, 12l: 213-222.
[7]Guo Z, Miodownik A P, Saunders N, et a1. Influence of stacking fault energy on high temperature creep of alpha titanium alloys[J]. Scripta Materialia, 2006, 54: 2175-2186.
[8]刘丽娟, 吕明, 武文革. 钛合金Ti-6Al-4V热变形中的动态再结晶研究[J]. 热加工工艺, 2014, 43(24): 1-6.
Liu Lijuan, Lü Ming, Wu Wenge. Dynamic recrystallization of Ti-6Al-4V during hot deformation[J]. Hot Working Technology, 2014, 43(24): 1-6.
[9]丁小明, 高星, 张宁, 等. 激光选区熔化成形TC4钛合金的热处理组织演变机理[J]. 热加工工艺, 2023, 52(14): 126-130.
Ding Xiaoming, Gao Xing, Zhang Ning, et a1. Mechanism of heat treatment microstructural evolution of TC4 alloy fabricated by selective laser melting[J]. Hot Working Technology, 2023, 52(14): 126-130.
[10]Bao R Q, Huang X, Cao C X. Deformation behavior and mechanisms of Ti-1023 alloy[J]. Transactions of Nonferrous Metals Society of China, 2006, 16(2): 274-284.
[11]Ouyang D L, Fu M W, Lu S Q. Study on the dynamic recrystallization behavior of Ti-alloy Ti-10V-2Fe-3V in β processing via experiment and simulation[J]. Materials Science and Engineering A, 2014, 619: 26-27.
[12]Zhang Z X, Qu S J, Feng A H, et a1. Achieving grain refinement and enhanced mechanical properties in Ti-6Al-4V alloy produced by multidirectional isothermal forging[J]. Materials Science and Engineering A, 2017, 692: 127-136.
[13]黄烁, 王磊, 张北江, 等. GH4706合金的动态再结晶与晶粒控制[J]. 材料研究学报, 2014, 28(5): 362-370.
Huang Shuo, Wang Lei, Zhang Beijiang, et al. Dynamic recrystallization behavior and grain size control of GH4706 superalloy[J]. Chinese Journal of Materials Research, 2014, 28(5): 362-370.

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加热温度和保温时间对Ti1023钛合金再结晶行为的影响

Effects of heating temperature and holding time on recrystallization behavior of Ti1023 titanium alloy

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