金属热处理 ›› 2020, Vol. 45 ›› Issue (11): 11-14.DOI: 10.13251/j.issn.0254-6051.2020.11.003

• 材料研究 • 上一篇    下一篇

Ti对9Cr-3Si-Al铁素体耐热钢微观组织及力学性能的影响

黄俊斌, 黄维刚   

  1. 四川大学 材料科学与工程学院, 四川 成都 610064
  • 收稿日期:2020-04-25 出版日期:2020-11-25 发布日期:2020-12-29
  • 通讯作者: 黄维刚,教授,博士生导师,E-mail: huangwg56@163.com
  • 作者简介:黄俊斌(1994—),男,硕士研究生,主要研究方向为金属材料结构与性能,E-mail: 3496831510@qq.com。
  • 基金资助:
    四川省科技厅专项基金(2017CC0069)

Effect of Ti on microstructure and mechanical properties of 9Cr-3Si-Al ferritic heat-resistant steel

Huang Junbin, Huang Weigang   

  1. College of Materials Science and Engineering, Sichuan University, Chengdu Sichuan 610064, China
  • Received:2020-04-25 Online:2020-11-25 Published:2020-12-29

摘要: 研究了Ti元素对9Cr-3Si-Al系铁素体耐热钢显微组织以及力学性能的影响。研究发现试验钢锻态试样晶粒内分布着大量的碳化物颗粒且细小均匀,经固溶处理后部分碳化物颗粒溶入试样基体。结合XRD以及EDS能谱分析试样表面的碳化物颗粒主要为Ti(C,N)的MX相,而晶界上检测到少量的Cr23C6相。经600 ℃时效后试样的抗拉强度、屈服强度均明显高于固溶态试样。通过对室温以及650 ℃高温断口形貌观察,发现室温下的断口为脆性断口,呈河流花样状,周围有少量微孔,为准解理断裂;而高温下断口呈微孔聚集型特征,韧窝密度较大,韧性较好。

关键词: 含Ti铁素体耐热钢, 显微组织, 力学性能, 断裂行为

Abstract: Effect of Ti on microstructure and mechanical properties of 9Cr-3Si-Al ferritic heat-resistant steel was studied. The results show that a large number of carbide particles which are fine and even, are distributed in the grains of the forged tested steel, and some of them are dissolved into the matrix after solution treatment. Combined with XRD and EDS tests, it is shown that the carbide particles are mainly Ti(C,N) phase which is MX phase on the specimen surface, while a small amount of Cr23C6 phase is detected on the grain boundary. The tensile strength and yield strength of the tested steel specimens aged at 600 ℃are higher than those of the solid solution specimens. Through the observation of the fracture morphology at room temperature and 650 ℃, it is found that the fracture at room temperature is brittle fracture with a small amount of micropores, which is a quasi-cleavage fracture. While the fracture at high temperature is microporous aggregation features, the density of dimples is higher and the toughness is better.

Key words: Ti-containing ferritic heat-resistant steel, microstructure, mechanical properties, fracture behavior

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