退火工艺对平整轧制后50W800无取向硅钢磁性能的影响

doi:10.13251/j.issn.0254-6051.2022.11.020

金属热处理 ›› 2022, Vol. 47 ›› Issue (11): 117-121.DOI: 10.13251/j.issn.0254-6051.2022.11.020

退火工艺对平整轧制后50W800无取向硅钢磁性能的影响

谯德高¹, 赵小龙², 狄彦军², 郭渊强², 蔺晓亮²

1.酒钢宏兴股份公司碳钢薄板厂,甘肃嘉峪关 735100;
2.酒钢宏兴股份公司钢铁研究院, 甘肃嘉峪关 735100

收稿日期:2022-07-05 修回日期:2022-09-27 出版日期:2022-11-25 发布日期:2023-01-04
通讯作者: 赵小龙,正高级工程师,博士,E-mail:zhaoxiaolong@jiugang.com
作者简介:谯德高(1983—),男,高级工程师,主要研究方向为无取向硅钢及薄板坯连铸工艺,E-mail:qiaodegao@jiugang.com。
基金资助:
嘉峪关市2021年科技重大专项(21-03)

Effect of annealing process on magnetic properties of flattening rolled 50W800 non-oriented silicon steel

Qiao Degao¹, Zhao Xiaolong², Di Yanjun², Guo Yuanqiang², Lin Xiaoliang²

1. Carbon Steel & Thin Slab Rolling Plant, Hongxing Iron & Steel Co., Ltd., Jiayuguan Gansu 735100, China;
2. Iron and Steel Research Institute, Hongxing Iron & Steel Co., Ltd., Jiayuguan Gansu 735100, China

Received:2022-07-05 Revised:2022-09-27 Online:2022-11-25 Published:2023-01-04

摘要/Abstract

摘要： 为提高50W800无取向硅钢的板形,需要对再结晶退火后的硅钢进行平整轧制,在平整后会出现硅钢片磁性能下降现象。对平整轧制后的50W800无取向硅钢进行400~800 ℃的去应力退火,利用单片测量法测量其铁损和磁感应强度,并用EBSD技术对组织织构进行分析。结果表明,经过平整轧制后,50W800无取向硅钢小角度晶界增加,但晶粒不均匀性会导致磁性能下降;采用700 ℃×2 min去应力退火后,50W800无取向硅钢磁性能得到较好的改善。EBSD技术分析发现,去应力退火能消耗大量小角度晶界,使晶界含量降低,晶粒均匀性增加,不利形变织构{111}<112>强度降低,这是50W800无取向硅钢磁性能改善的主要原因。

关键词: 无取向硅钢, 小角度晶界, 平整退火, 磁性能

Abstract: In order to improve the sheet shape of the 50W800 non-oriented silicon steel, the silicon steel after recrystallization annealing needs to be flattened, but the magnetic properties of the silicon steel sheet will decrease after flattening. The stress relief annealing test of the flattening rolled 50W800 non-oriented silicon steel was designed at 400-800 ℃, the iron loss and magnetic induction strength were measured by a single chip measuring method and the microstructure and texture were analyzed by EBSD technology. The results show that the small angle grain boundary of the 50W800 non-oriented silicon steel increases after flattening, but the nonuniformity of grain leads to the decrease of magnetic properties. It is found that after stress relief annealing at 700 ℃ for 2 min, the magnetic properties of 50W800 non-oriented silicon steel are improved. EBSD technology analysis shows that the stress relief annealing can consume a large amount of small angle grain boundary, reduce the grain boundary content, increase the grain uniformity, and reduce the strength of unfavorable deformation texture {111} <112>, which is the main reason for the improvement of magnetic properties of the 50W800 non-oriented silicon steel.

Key words: non-oriented silicon steel, small angle grain boundary, flattening and annealing, magnetic properties

中图分类号:

TG335.21

谯德高, 赵小龙, 狄彦军, 郭渊强, 蔺晓亮. 退火工艺对平整轧制后50W800无取向硅钢磁性能的影响[J]. 金属热处理, 2022, 47(11): 117-121.

Qiao Degao, Zhao Xiaolong, Di Yanjun, Guo Yuanqiang, Lin Xiaoliang. Effect of annealing process on magnetic properties of flattening rolled 50W800 non-oriented silicon steel[J]. Heat Treatment of Metals, 2022, 47(11): 117-121.

参考文献

[1]熊文涛, 郭德福, 丁美良, 等. 冷轧无取向硅钢横向厚度差控制技术[J]. 钢铁, 2016, 51(1): 65-69.
Xiong Wentao, Guo Defu, Ding Meiliang, et al. Technology of the transverse thickness difference control for cold rolled non-oriented silicon steel[J]. Iron and Steel, 2016, 51(1): 65-69.
[2]曹建国, 唐慧, 杨光辉, 等. 有高温相变的电工钢热轧起浪的有限元分析[J]. 哈尔滨工业大学学报, 2016, 48(1): 146-151.
Cao Jianguo, Tang Hui, Yang Guanghui, et al. Finite element analysis of edge wave for non-oriented electrical strip with high temperature phase transition[J]. Journal of Harbin Institute of Technology, 2016, 48(1): 146-151.
[3]李俊洪, 李军, 樊华, 等. 无取向电工钢平整工艺研究[J]. 钢铁, 2010, 45(2): 66-69.
Li Junhong, Li Jun, Fan Hua, et al. Study on skin passing technology of non-oriented silicon steel[J]. Iron and Steel, 2010, 45(2): 66-69.
[4]王健, 李俊, 郭文渊, 等. 冷轧无取向硅钢再结晶退火组织和织构演变研究进展[J]. 材料导报, 2010, 24(19): 100-103.
Wang Jian, Li Jun, Guo Wenyuan, et al. Progress in evolution of structure and texture during annealing in cold rolled non-oriented silicon steels[J]. Materials Reports, 2010, 24(19): 100-103.
[5]董强, 刘慧慧, 张建水. 横向温度分布对无取向电工钢热轧板形的影响[J]. 中国冶金, 2019, 29(8): 19-23.
Dong Qiang, Liu Huihui, Zhang Jianshui. Effects of transverse temperature distribution on strip shape of non-orientation electrical steel in hot rolling process[J]. China Metallurgy, 2019, 29(8): 19-23.
[6]张清东, 李博, 张晓峰. 带钢平整轧制板形控制行为及效应的研究[J]. 机械工程学报, 2014, 50(8): 45-52.
Zhang Qingdong, Li Bo, Zhang Xiaofeng. Research on the behavior and effects of flatness control in strip temper rolling process[J]. Journal of Mechanical Engineering, 2014, 50(8): 45-52.
[7]Rodrigues M F, Da C M A, Da C P S, et al. Texture and magnetic properties improvement of a 3%Si non-oriented electrical steel by Sb addition[J]. Journal of Magnetism and Magnetic Materials, 2013, 331: 24-27.
[8]骆忠汉, 汪汝武, 曾春, 等. 平整轧制量对6.5%Si硅钢薄带组织和织构及磁性能的影响[J]. 金属功能材料, 2015, 22(1): 6-10.
Luo Zhonghan, Wang Ruwu, Zeng Chun, et al. Effects of temper rolling rate on the microstructure, texture an magnetic properties of Fe-6.5%Si thin strip[J]. Metallic Functional Materials, 2015, 22(1): 6-10.
[9]毛卫民, 杨平. 电工钢的材料学原理[M]. 北京: 高等教育出版社, 2013: 91-336.
[10]刘涛. 形变与退火对无取向硅钢组织和磁性能的影响研究[D]. 合肥: 合肥工业大学, 2019.
[11]Argon A S, Haasen P. A new mechanism of work hardening in the late stages of large strain plastic flow in FCC and diamond cubic crystals[J]. Acta Metallurgica et Materialia, 1993, 41(11): 3289-3306.
[12]钟文定. 铁磁学(中册)[M]. 北京: 科学技术出版社, 1987.
[13]李毅伟, 李德君, 乔浩浩. 高冲片性50BW600电磁性能影响因素及工艺控制[J]. 电工钢, 2020, 2(2): 31-34, 52.
Li Yiwei, Li Dejun, Qiao Haohao. Analysis of the factors influencing the electromagnetic properties of high punching 50BW600 non-oriented silicon steel[J]. Electrical Steel, 2020, 2(2): 31-34, 52.
[14]刘爱国. 冷轧硅钢产品品质对冲片性影响的研究分析[J]. 机械工程与自动化, 2004(6): 82-83.
Liu Aiguo. Study and analysis of the cold rolling silicon steel product quality on the blanking property[J]. Mechanical Engineering and Automation, 2004(6): 82-83.

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退火工艺对平整轧制后50W800无取向硅钢磁性能的影响

Effect of annealing process on magnetic properties of flattening rolled 50W800 non-oriented silicon steel

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