淬火温度对GE1014超高强度钢组织及性能的影响

doi:10.13251/j.issn.0254-6051.2022.02.022

金属热处理 ›› 2022, Vol. 47 ›› Issue (2): 125-129.DOI: 10.13251/j.issn.0254-6051.2022.02.022

淬火温度对GE1014超高强度钢组织及性能的影响

刘跃¹, 韩顺¹, 厉勇¹, 王春旭¹, 严晓红², 李建新²

1.钢铁研究总院特殊钢研究院, 北京 100081;
2.抚顺特殊钢股份有限公司技术中心, 辽宁抚顺 113001

收稿日期:2021-10-14 修回日期:2021-12-20 出版日期:2022-02-25 发布日期:2022-04-01
通讯作者: 厉勇,正高级工程师,E-mail:liysea@163.com
作者简介:刘跃(1996—),男,硕士研究生,主要研究方向为超高强度钢,E-mail:Junexplore@163.com。
基金资助:
国家重点研发计划(2016YFB0300104)

Effect of quenching temperature on microstructure and mechanical properties of GE1014 ultra-high strength steel

Liu Yue¹, Han Shun¹, Li Yong¹, Wang Chunxu¹, Yan Xiaohong², Li Jianxin²

1. Research Institute of Special Steels, Central Iron and Steel Research Institute, Beijing 100081, China;
2. Technology Center, Fushun Special Steel Co., Ltd., Fushun Liaoning 113001, China

Received:2021-10-14 Revised:2021-12-20 Online:2022-02-25 Published:2022-04-01

摘要/Abstract

摘要： 采用力学性能测试、透射电镜(TEM)、X射线衍射(XRD)仪和电子背散射衍射(EBSD)等分析方法,研究了淬火温度对GE1014超高强度钢组织及性能的影响。结果表明,试验钢的抗拉强度随淬火温度的升高先逐渐升高,随后降低,并且在925 ℃达到峰值2112 MPa,规定塑性延伸强度则呈现随淬火温度的升高小幅降低的趋势,试验钢的断面收缩率和U型冲击性能均随淬火温度的升高缓慢升高,在950 ℃附近出现降低趋势;试验钢的原始奥氏体晶粒和马氏体块的尺寸都随着淬火温度的升高而长大,当淬火温度超过925 ℃时,原始奥氏体晶粒尺寸快速粗化,而马氏体块尺寸则全程长大缓慢;850~925 ℃范围内,基体中的残留奥氏体含量随着淬火温度的升高而显著降低;淬火温度低于900 ℃时,试验钢中存在球状富Mo型M₆C碳化物,淬火温度升高至900 ℃未观察到未溶相。

关键词: GE1014钢, 淬火温度, 力学性能, 微观组织

Abstract: Effect of quenching temperature on mechanical properties and microstructure of the GE1014 ultra-high strength steel was studied by means of mechanical property test, transmission electron microscope (TEM), X-ray diffraction (XRD), electron backscatter diffraction (EBSD) and other analysis methods. The results show that with the increase of quenching temperature, the tensile strength of the tested steel increases first and then decreases and the peak value is 2112 MPa when quenched at 925 ℃, the proof strength, plastic extension decreases slightly with the increase of quenching temperature. The reduction of area and U-notched impact property of the tested steel increase slowly with the increase of quenching temperature, and decrease at near 950 ℃. Both the prior austenite grain size and martensite block size of the tested steel increase with the increase of quenching temperature. When the quenching temperature exceeds 925 ℃, the prior austenite grain coarsens rapidly, while the martensite block grows slowly throughout the whole process. In the range of 850-925 ℃, the volume fraction of retained austenite in the matrix decreases significantly with the increase of quenching temperature. When the quenching temperature is lower than 900 ℃, there are spherical Mo-rich M₆C carbides in the tested steel, while when higher than 900 ℃, no insoluble phase is observed.

Key words: GE1014 steel, quenching temperature, mechanical properties, microstructure

中图分类号:

TG142.1

刘跃, 韩顺, 厉勇, 王春旭, 严晓红, 李建新. 淬火温度对GE1014超高强度钢组织及性能的影响[J]. 金属热处理, 2022, 47(2): 125-129.

Liu Yue, Han Shun, Li Yong, Wang Chunxu, Yan Xiaohong, Li Jianxin. Effect of quenching temperature on microstructure and mechanical properties of GE1014 ultra-high strength steel[J]. Heat Treatment of Metals, 2022, 47(2): 125-129.

参考文献

[1]胡正飞, 吴杏芳, 王春旭. 二次硬化高CoNi超高强度合金钢的研究近况[J]. 钢铁研究学报, 2001, 13(4): 62-68.
Hu Zhengfei, Wu Xingfang, Wang Chunxu. Recent status of enriched CoNi ultra-high strength steel with secondary hardening[J]. Journal of Iron and Steel Research, 2001, 13(4): 62-68.
[2]Gao Y H, Liu S Z, Hu X B, et al. A novel low cost 2000 MPa grade ultra-high strength steel with balanced strength and toughness[J]. Materials Science and Engineering A, 2019, 759: 298-302.
[3]厉勇, 王春旭, 黄顺喆, 等. 超高强度钢中M₂C和β-NiAl相的复合析出强化行为[J]. 金属热处理, 2018, 43(6): 50-54.
Li Yong, Wang Chunxu, Huang Shunzhe, et al. Combined precipitation strengthening behavior of M₂C carbides and β-NiAl intermetallics in ultrahigh strength steel[J]. Heat Treatment of Metals, 2018, 43(6): 50-54.
[4]Perrut M, Mathon M H, Delagnes D. Small-angle neutron scattering of multiphase secondary hardening steels[J]. Journal of Materials Science, 2012, 47(4): 1920-1929.
[5]梁锋. 夹杂物对超高强度钢微观破坏机制的研究[D]. 北京: 清华大学, 2006.
[6]刘路, 詹肇麟, 韩顺, 等. 回火温度对GE1014钢组织与力学性能的影响[J]. 金属热处理, 2018, 43(10): 133-137.
Liu Lu, Zhan Zhaolin, Han Shun, et al. Effect of tempering temperature on microstructure and mechanical properties of GE1014 steel[J]. Heat Treatment of Metals, 2018, 43(10): 133-137.
[7]Delagnes D, Pettinari-Sturmel F, Mathon M H, et al. Cementite-free martensitic steels: A new route to develop high strength/high toughness grades by modifying the conventional precipitation sequence during tempering[J]. Acta Materialia, 2012, 60(16): 5877-5888.
[8]Wang C X, Gao Y H, Li Y, et al. Effects of solid-solution temperature on microstructure and mechanical properties of a novel 2000 MPa grade ultra-high strength steel[J]. Journal of Iron and Steel Research International, 2020, 27(6): 710-718.
[9]梁晓东, 王晨充, 李亮, 等. 淬火温度对C61齿轮钢显微组织和力学性能的影响[J]. 材料热处理学报, 2020, 41(11): 79-86.
Liang Xiaodong, Wang Chenchong, Li Liang, et al. Effect of quenching temperature on microstructure and mechanical properties of C61 gear steel[J]. Transactions of Materials and Heat Treatment, 2020, 41(11): 79-86.
[10]胡成飞, 吴润, 尉文超, 等. 淬火温度对17Cr2Ni2MoVNb重载齿轮钢组织和硬度的影响[J]. 金属热处理, 2019, 44(10): 91-95.
Hu Chengfei, Wu Run, Yu Wenchao, et al. Effect of quenching temperature on microstructure and hardness of 17Cr2Ni2MoVNb heavy gear steel[J]. Heat Treatment of Metals, 2019, 44(10): 91-95.
[11]崔忠圻, 覃耀春. 金属学与热处理[M]. 北京: 机械工业出版社, 2009.
[12]谭玉华, 马跃新. 马氏体新形态学[M]. 北京: 冶金工业出版社, 2013.
[13]李继康, 李昭东. 超低碳马氏体的EBSD结构表征[J]. 电子显微学报, 2011, 30(S1): 394-398.Li Jikang, Li Zhaodong. EBSD characterization on the structure of ultra-low carbon martensite[J]. Journal of Chinese Electron Microscopy Society, 2011, 30(S1): 394-398.
[14]张晓东, 夏佃秀, 王守仁, 等. 奥氏体化温度对51CrV4钢淬火组织和性能的影响[J]. 钢铁, 2019, 54(3): 76-81, 95.
Zhang Xiaodong, Xia Dianxiu, Wang Shouren, et al. Effect of austenitizing temperature on quenching microstructure and properties of 51CrV4 steel[J]. Iron and Steel, 2019, 54(3): 76-81, 95.
[15]钢铁研究总院. 钢和铁、镍基合金的物理化学相分析[M]. 上海: 上海科学技术出版社, 1981.
[16]Wang C, Wang M, Shi J, et al. Effect of microstructural refinement on the toughness of low carbon martensitic steel[J]. Scripta Materialia, 2008, 58(6): 492-495.
[17]张鹏杰, 王春旭, 厉勇, 等. 淬火温度对2200 MPa级超高强度钢力学性能与微观组织的影响[J]. 金属热处理, 2021, 46(1): 70-74.
Zhang Pengjie, Wang Chunxu, Li Yong, et al. Effect of quenching temperature on mechanical properties and microstructure of 2200 MPa ultra high strength steel[J]. Heat Treatment of Metals, 2021, 46(1): 70-74.
[18]Liu T Q, Cao Z X, Wang H, et al. A new 2.4 GPa extra-high strength steel with good ductility and high toughness designed by synergistic strengthening of nano-particles and high-density dislocations[J]. Scripta Materialia, 2020, 178: 285-289.
[19]王春芳. 低合金马氏体钢强韧性组织控制单元的研究[D]. 北京: 钢铁研究总院, 2008.
[20]惠卫军, 董瀚, 王毛球, 等. 淬火温度对Cr-Mo-V系低合金高强度钢力学性能的影响[J]. 金属热处理, 2002, 27(3): 14-16.
Hui Weijun, Dong Han, Wang Maoqiu, et al. Effect of quenching temperature on mechanical properties of Cr-Mo-V series low alloy high strength steel[J]. Heat Treatment of Metals, 2002, 27(3): 14-16.

淬火温度对GE1014超高强度钢组织及性能的影响

Effect of quenching temperature on microstructure and mechanical properties of GE1014 ultra-high strength steel

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