固溶温度对DD416镍基单晶高温合金组织及拉伸性能的影响

doi:10.13251/j.issn.0254-6051.2024.01.018

金属热处理 ›› 2024, Vol. 49 ›› Issue (1): 119-126.DOI: 10.13251/j.issn.0254-6051.2024.01.018

固溶温度对DD416镍基单晶高温合金组织及拉伸性能的影响

陈博文¹, 曾强^2,3, 李钢⁴, 彭文雅⁴, 刘国怀¹

1. 东北大学轧制技术及连轧自动化国家重点实验室, 辽宁沈阳 110819;
2. 北京钢研高纳科技股份有限公司, 北京 100081;
3. 河北钢研德凯科技有限公司, 河北涿州 072700;
4. 中国航发湖南动力机械研究所, 湖南株洲 412002

收稿日期:2023-07-28 修回日期:2023-11-09 发布日期:2024-02-29
通讯作者: 刘国怀,副教授,博士,E-mail:liugh@ral.neu.edu.cn
作者简介:陈博文(1997—),男,硕士研究生,主要研究方向为单晶高温合金组织演化规律与长期组织稳定性,E-mail:17854172272@163.com。
基金资助:
国家自然科学基金(52071065);中央高校基础科研业务费(N2007007)

Effect of solution temperature on microstructure and tensile properties of DD416 nickel-based single crystal superalloy

Chen Bowen¹, Zeng Qiang^2,3, Li Gang⁴, Peng Wenya⁴, Liu Guohuai¹

1. State Key Laboratory of Rolling Technology and Continuous Rolling Automation, Northeastern University, Shenyang Liaoning 110819, China;
2. Beijing Cisri-Gaona Materials & Technology Co., Ltd., Beijing 100081, China;
3. Hebei Gangyan Dekai Technology Co., Ltd., Zhuozhou Hebei 072700, China;
4. AECC Hunan Aviation Powerplant Research Institute, Zhuzhou Hunan 412002, China

Received:2023-07-28 Revised:2023-11-09 Published:2024-02-29

摘要/Abstract

摘要： 研究了固溶处理温度对一种高强低密度第一代的镍基单晶高温合金DD416的组织及拉伸性能的影响。结果表明,铸态试样中存在着明显的成分偏析与元素偏析现象。经过固溶处理后,合金中的成分偏析与元素偏析现象得到明显改善,随着固溶温度的提高,合金中的共晶组织含量逐渐减少。铸态合金中存在的孔洞为铸造疏松,在经过固溶处理后,由于元素扩散速率的不同会出现小部分的固溶孔洞,合金中空洞较多也会影响合金性能。通过对760 ℃高温拉伸数据可以看出,合金的拉伸性能在经过热处理后得到较为明显的提高,随着固溶温度的提高,合金的抗拉强度和屈服强度有所提高,合金的断后伸长率和断面收缩率也有着较为显著的增加,即经过固溶处理+时效处理后,随着固溶温度的提高,合金的强度与塑性得到改善与提高。

关键词: DD416单晶高温合金, 固溶温度, 显微组织, 拉伸性能

Abstract: Effect of solution treatment temperature on microstructure and tensile properties of the first generations nickel-based single crystal superalloy DD416 with high strength and low density was studied. The results show that there are obvious component segregation and element segregation in the as-cast specimens. After solution treatment, the component segregation and element segregation in the alloy are obviously improved. With the increase of solution temperature, the content of eutectic structure in the alloy decreases gradually. The pores in the as-cast alloy are cast porosity. After solution treatment, a small number of solution pores appear due to the different diffusion rates of elements, and many hollow pores in the alloy also affect the properties of the alloy. According to the 760 ℃ high temperature tensile data, the tensile properties of the alloy are significantly improved after complete heat treatment. With the increase of solution temperature, the tensile strength and yield strength of the alloy increase, and the elongation after fracture and the percontage reduction of area significantly increase. As a result, after solution treatment+aging, with the increase of solution temperature, the strength and plasticity of the alloy are improved.

Key words: DD416 single crystal superalloy, solution temperature, microstructure, tensile properties

中图分类号:

TG142.1

陈博文, 曾强, 李钢, 彭文雅, 刘国怀. 固溶温度对DD416镍基单晶高温合金组织及拉伸性能的影响[J]. 金属热处理, 2024, 49(1): 119-126.

Chen Bowen, Zeng Qiang, Li Gang, Peng Wenya, Liu Guohuai. Effect of solution temperature on microstructure and tensile properties of DD416 nickel-based single crystal superalloy[J]. Heat Treatment of Metals, 2024, 49(1): 119-126.

参考文献

[1]Guo Jianting. Materials Science and Engineering for Superalloys[M]. Beijing: Science Press, 2008: 300-301.
[2]殷凤仕, 孙晓峰, 胡壮麒, 等. 热处理对M963合金显微组织和拉伸性能的影响[J]. 稀有金属材料与工程, 2004, 33(1): 23-26.
Yin Fengshi, Sun Xiaofeng, Hu Zhuangqi, et al. Effect of heat treatment on the microstructure and tensile properties of the cast nickel-base superalloy M963[J]. Rare Metal Materials and Engineering, 2004, 33(1): 23-26.
[3]Yang J X, Zhang Q, Sun X F, et al. Morphological evolution of γ′ phase in K465 superalloy during thermal fatigue[J]. Transactions of Nonferrous Metals Society of China, 2006, 16(Z3)1: 986-1989.
[4]Jackson M P, Reed R C. Heat treatment of UDIMET 720Li: The effect of microstructure on properties[J]. Materials Science and Engineering A, 1999, 259(1): 85-97.
[5]Monajati H, Jahazi M, Bahrami R, et al. The influence of heat treatment conditions on γ′ characteristics in Udimet[J]. Materials Science and Engineering A, 2004, 373(1): 286-293.
[6]Ges A M, Fornaro O, Palacio H A. Coarsening behavior of a Ni-base superalloy under different heat treatment conditions[J]. Materials Science and Engineering A, 2007, 458(1): 96-100.
[7]Rzyankina E, Pytel M, Mahomed N, et al. Solution heat treatment of single crystal castings of CMSX-4 nickel-base superalloy[C]//International Conference on Competitive Manufacturing. 2016(1): 307-311.
[8]郭建亭, 朱耀宵, 师昌绪. 国外涡轮喷气发动机涡轮盘材料的现状及发展[J]. 金属学报, 1974(1): 74-98.
[9]Sun J X, Liu J L, Liu L R, et al. Effects of Al on microstructural stability and related stress rupture properties of a third generation single crystal superalloy[J]. Journal of Materials Sciences and Technology, 2019, 35(11): 2537-2542.
[10]Zuback J S, Moradifar P, Khayat Z, et al. Impact of chemical composition on precipitate morphology in an additively manufactured nickel base superalloy[J]. Journal of Alloys and Compounds, 2019(7): 446-457.
[11]赵德孜. 海洋环境下燃气轮机涡轮叶片的热腐蚀与防护[J]. 装备环境工程, 2011, 8(5): 100-103.
Zhao Dezi. Hot corrosion and protection of gas turbine blade in marine environment[J]. Equipment Environmental Engineering, 2011, 8(5): 100-103.
[12]Ma S, Zhang J. Alloying effects of refractory elements in the dislocation of Ni-based single crystal superalloys[J]. Progress in Natural Science: Materials International, 2016, 26(6): 636-642.
[13]余竹焕. 碳对单晶高温合金凝固组织及力学性能的影响[D]. 西安: 西北工业大学, 2011.
[14]Coutsouraclis D, 傅恒志. 镍基高温合金中显微疏松程度的评价[J]. 铸造技术, 1984(4): 59-60.
[15]秦升学, 王艳, 张弘斌, 等. 固溶处理对GH99合金组织的影响[J]. 金属热处理, 2020, 45(8): 173-178.
Qin Shengxue, Wang Yan, Zhang Hongbin, et al. Effect of solution treatment on microstructure of GH99 alloy[J]. Heat Treatment of Metals, 2020, 45(8): 173-178.

固溶温度对DD416镍基单晶高温合金组织及拉伸性能的影响

Effect of solution temperature on microstructure and tensile properties of DD416 nickel-based single crystal superalloy

PDF

可视化

摘要/Abstract

引用本文

使用本文

参考文献

相关文章 15

编辑推荐

Metrics

本文评价

[1]	宋体杰, 王长宇, 王珏, 于妍妍, 卢增威, 金冬岩. 热暴露对Ti55合金显微组织及力学性能的影响[J]. 金属热处理, 2024, 49(1): 15-21.
[2]	朱嘉武, 欧阳晟. 退火对FeCoNi_2-xMnGa_x高熵合金微观组织、力学性能和磁性能的影响[J]. 金属热处理, 2024, 49(1): 22-31.
[3]	原海瑞, 陈玉波, 王培杰, 李振江. 40Cr/Q345B双金属复合行为及界面组织演变[J]. 金属热处理, 2024, 49(1): 90-95.
[4]	靖青秀, 彭勇, 肖翔鹏, 韦丹丹, 杨雪晴, 黄晓东. Fe含量对Cu-Ti-Ni-xFe合金组织与性能的影响[J]. 金属热处理, 2024, 49(1): 96-102.
[5]	崔岩, 梁家瑞, 曹雷刚, 杨越, 刘园. 时效处理对中高体积分数SiC_p/2024Al复合材料力学性能的影响[J]. 金属热处理, 2024, 49(1): 131-136.
[6]	刘文明, 张新明, 程新路, 欧阳凯. 焊后热处理对S30408/Q345R不锈钢复合板耐蚀性能的影响[J]. 金属热处理, 2024, 49(1): 172-178.
[7]	田少鲲, 金圆平, 王萍, 杨堃, 刘晓霏, 郭占, 郁瑞兴, 范庆利. 时效处理对低压铸造ZL114A合金力学性能及显微组织的影响[J]. 金属热处理, 2024, 49(1): 179-185.
[8]	李志平, 王宏霞, 赵刚, 王俊海. 退火工艺对T4003高强度铁素体不锈钢组织和性能的影响[J]. 金属热处理, 2024, 49(1): 198-201.
[9]	樊明强, 赵英利, 李素芳, 梁佳, 王超, 徐军君, 王建强, 赵峥嵘. 扩散退火对H13钢显微组织和成分偏析的影响[J]. 金属热处理, 2024, 49(1): 211-214.
[10]	杨源远, 王栋, 黄利, 刘宝志. HiB与CGO取向硅钢的对比及其常化退火工艺[J]. 金属热处理, 2024, 49(1): 228-234.
[11]	汪英芝, 谢波, 纪超, 王红霞, 郑留伟, 梁伟. 34CrNiMo6钢曲轴轴颈感应淬火硬化微观机理[J]. 金属热处理, 2024, 49(1): 242-248.
[12]	崔毅, 崔继红, 王艳, 张雲飞, 俞峰, 赵英利, 曹文全. 淬火工艺对GCr4Mo4V钢组织及耐磨性的影响[J]. 金属热处理, 2023, 48(9): 23-29.
[13]	李文刚, 炊鹏飞, 程尊鹏, 李春梅, 景然, 李江华, 廖仲尼. 硼含量对Ti-Zr-Nb-B合金显微组织及性能的影响[J]. 金属热处理, 2023, 48(9): 157-164.
[14]	戴钊, 郭智, 龙晓燕, 冯晓勇, 刘伟, 张福成, 李艳国. Si含量对高碳贝氏体钢微观组织与性能的影响[J]. 金属热处理, 2023, 48(9): 165-173.
[15]	李鑫, 武志广, 赵吉庆, 杨钢. 20Cr1Mo1VTiB螺栓钢高温长期时效后的组织演变及力学性能[J]. 金属热处理, 2023, 48(9): 197-202.