HRB400E钢等温热处理过程中的奥氏体晶粒长大和钒析出物的影响

doi:10.13251/j.issn.0254-6051.2024.08.003

金属热处理 ›› 2024, Vol. 49 ›› Issue (8): 15-21.DOI: 10.13251/j.issn.0254-6051.2024.08.003

HRB400E钢等温热处理过程中的奥氏体晶粒长大和钒析出物的影响

陈石¹, 汪家晗¹, 张云祥¹, 骆艳萍², 孙钊洋¹, 叶传龙¹

1.武汉科技大学材料学部, 湖北武汉 430081;
2.中冶南方工程技术有限公司, 湖北武汉 430223

收稿日期:2024-01-28 修回日期:2024-06-12 出版日期:2024-08-25 发布日期:2024-09-27
通讯作者: 张云祥,副教授,博士,E-mail:zhangyunxiang@wust.edu.cn
作者简介:陈石(1994—),男,硕士研究生,主要研究方向为金属材料组织与性能控制,E-mail:1479433434@qq.com。
基金资助:
国家自然科学基金(51774219)

Austenite grain growth of HRB400E steel during isothermal treatment and effect of vanadium precipitates

Chen Shi¹, Wang Jiahan¹, Zhang Yunxiang¹, Luo Yanping², Sun Zhaoyang¹, Ye Chuanlong¹

1. Materials Department of Wuhan University of Science and Technology, Wuhan Hubei 430081, China;
2. MCC Southern Engineering Technology Corporation, Wuhan Hubei 430223, China

Received:2024-01-28 Revised:2024-06-12 Online:2024-08-25 Published:2024-09-27

摘要/Abstract

摘要： 利用高温激光扫描共聚焦显微镜和透射电镜(TEM)等研究了含钒钢HRB400E在不同等温温度(950~1200 ℃)下保温30 min的加热过程中的奥氏体晶粒长大行为以及钒析出物对奥氏体晶粒长大的影响。结果表明,加热温度对试验钢奥氏体晶粒长大的影响明显大于保温时间,加热温度超过1100 ℃时,奥氏体晶粒等温长大速率明显加大。TEM观察表明钢中奥氏体晶粒长大行为受基体中V(C, N)粒子的影响,当加热温度为950 ℃时,钢中存在大量未溶的V(C, N)粒子,能有效钉扎奥氏体晶界,晶粒长大缓慢;当加热温度升高至1100 ℃时,随保温时间延长,细小的V(C, N)粒子溶解和粗化,钉扎效果下降,此时奥氏体晶粒快速长大。根据实测奥氏体晶粒尺寸结合Sellars模型和Anelli模型建立了试验钢奥氏体晶粒等温长大动力学模型,模型计算值与实测值吻合较好。

关键词: 抗震钢HRB400E, 奥氏体晶粒长大, 动力学模型, V(C, N)析出物

Abstract: Austenite grain growth behavior during the isothermal heating processes at different heating temperatures(950-1200 ℃) holding for 30 min of vanadium containing steel HRB400E and the effect of vanadium precipitates on the austenite grain growth was studied by using high-temperature laser scanning confocal microscope and transmission electron microscope(TEM). The results show that the effect of heating temperature on the austenite grain growth in the tested steel is significantly greater than that of the holding time, and the isothermal growth rate of austenite grains increases significantly when the heating temperature exceeds 1100 ℃. The TEM observation shows that the growth behavior of austenite grains in the steel is influenced by V(C, N) particles in the matrix. When the heating temperature is 950 ℃, there is a large amount of undissolved V(C, N) particles in the steel, which can effectively pin the austenite grain boundaries and slow the grain growth. When the heating temperature rises to 1100 ℃, the fine V(C, N) particles dissolve and coarsen with the prolongation of the holding time, the pinning effect decreases, at this time the austenite grains grow rapidly. A kinetic model for the isothermal growth of austenite grains in the tested steel is established based on the measured austenite grain size and combined with the Sellers model and Anelli model, and it is found that the calculated values of the model are in good agreement with the measured values.

Key words: seismic steel HRB400E, austenite grain growth, kinetic model, V(C,N) precipitate

中图分类号:

TG142.1⁺3

陈石, 汪家晗, 张云祥, 骆艳萍, 孙钊洋, 叶传龙. HRB400E钢等温热处理过程中的奥氏体晶粒长大和钒析出物的影响[J]. 金属热处理, 2024, 49(8): 15-21.

Chen Shi, Wang Jiahan, Zhang Yunxiang, Luo Yanping, Sun Zhaoyang, Ye Chuanlong. Austenite grain growth of HRB400E steel during isothermal treatment and effect of vanadium precipitates[J]. Heat Treatment of Metals, 2024, 49(8): 15-21.

参考文献

[1]詹苏宇, 盛光敏, 刘旭东, 等. 高强HRB400E建筑用抗震钢筋高应变低周疲劳性能研究[J]. 热加工工艺, 2010, 39(16): 22-26.
Zhan Suyu, Sheng Guangmin, Liu Xudong, et al. Study on high strain and low cycle fatigue properties of seismic steel bars for high-strength HRB400E construction[J]. Hot Working Technology, 2010, 39(16): 22-26.
[2]盛光敏, 吕煜坤, 黄振华. 细晶化和余热处理抗震钢筋的高应变低周疲劳行为分析[J]. 功能材料, 2014, 45(15): 15124-15128.
Sheng Guangmin, Lü Yukun, Huang Zhenhua. Analysis on the high strain and low cycle fatigue behaviors of seismic rebar between the grain refinement and tempcore technology[J]. Journal of Functional Materials, 2014, 45(15): 15124-15128.
[3]谢雄科. 热轧带肋螺纹钢筋HRB500E奥氏体晶粒长大行为[J]. 河北冶金, 2022, 10(12): 9-13.
Xie Xiongke. Austenite grain growth behavior of hot-rolled ribbed bar HRB500E[J]. Hebei Metallurgy, 2022, 10(12): 9-13.
[4]韩汝洋, 杨庚蔚, 孙新军, 等. 钒微合金化中锰马氏体耐磨钢奥氏体长大行为[J]. 金属学报, 2015, 58(12): 1589-1599.
Han Ruyang, Yang Gengwei, Sun Xinjun, et al. Austenite grain growth behavior of vanadium microalloying medium manganese martensitic wear-resistant steel[J]. Acta Metallurgica Sinica, 2015, 58(12): 1589-1599.
[5]]Dong Dingqian, Chen Fei, Cui Zhenshan. Modeling of austenite grain growth during austenitization in a low alloy steel[J]. Journal of Materials Engineering and Performance, 2016, 25(1): 152-164.
[6]]罗许, 康永林, 李俊洪. 加热温度对钛微合金化钢奥氏体晶粒长大的影响[J]. 钢铁钒钛, 2016, 37(2): 133-138.
Luo Xu, Kang Yonglin, Li Junhong. Effect of heating temperature on the growth of austenite grain of titanium microalloyed steel[J]. Iron Steel Vanadium Titanium, 2016, 37(2): 133-138.
[7]]Kim T H, Park J K. Austenite grain coarsening of V-microalloyed medium carbon steel during high frequency induction heating: Monte Carlo simulation study[J]. Materials Science Technology, 2013, 29(12): 1414-1422.
[8]]李奇, 张旭, 李晓晴, 等. Nb、Ti对耐热钢中δ铁素体固溶行为的影响[J]. 钢铁, 2023, 58(10): 131-139.
Li Qi, Zhang Xu, Li Xiaoqing, et al. Effect of Nb and Ti on dissolution behavior of delta ferrite in heat-resistant steel[J]. Iron and Steel, 2023, 58(10): 131-139.
[9]]苑少强, 梁国俐, 武会宾. 超低碳微合金钢中碳氮化物的溶解行为[J]. 材料热处理学报, 2011, 32(S1): 83-85.
Yuan Shaoqiang, Liang Guoli, Wu Huibin, Dissolving behavior of carbonitrides in a ultra-low carbon microalloyed steel[J]. Transactions of Materials and Heat Treatment, 2011, 32(S1): 83-85.
[10]杨清, 张立文, 张驰, 等. 低碳Nb-V-Ti微合金钢X70的奥氏体晶粒长大行为[J]. 金属热处理, 2019, 44(4): 1-5.
Yang Qing, Zhang Liwen, Zhang Chi, et al. Austenite grain growth behavior of low-carbon Nb-V-Ti microalloyed steel X70[J]. Heat Treatment of Metals, 2019, 44(4): 1-5.
[11]]高彩茹, 霍喜伟, 宋玉卿, 等. 500 MPa级门架型钢的奥氏体晶粒长大行为[J]. 金属热处理, 2020, 45(1): 139-142.
Gao Cairu, Huo Xiwei, Song Yuqing, et al. Austenite grain growth behavior of 500 MPa class gantry steel[J]. Heat Treatment of Metals, 2020, 45(1): 139-142.
[12]]刘豪, 张立文, 李飞, 等. 38CrMoAl钢的奥氏体晶粒长大行为[J]. 金属热处理, 2020, 45(8): 38-42.
Liu Hao, Zhang Liwen, Li Fei, et al. Austenite grain growth behavior of 38CrMoAl steel[J]. Heat Treatment of Metals, 2020, 45(8): 38-42.
[13]]Najafkhani F, Mirzadeh H, Zamani M. Effect of intercritical annealing conditions on grain growth kinetics of dual phase steel[J]. Metals and Materials International, 2019, 25: 39-46.

HRB400E钢等温热处理过程中的奥氏体晶粒长大和钒析出物的影响

Austenite grain growth of HRB400E steel during isothermal treatment and effect of vanadium precipitates

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