金属热处理 ›› 2025, Vol. 50 ›› Issue (1): 81-87.DOI: 10.13251/j.issn.0254-6051.2025.01.013

• 工艺研究 • 上一篇    下一篇

深冷处理对核电级低碳钢微观组织及性能的影响

徐科1, 胡明磊1, 张维1, 胡斌1, 李冬升2, 刘仁才2   

  1. 1.中核核电运行管理有限公司, 浙江 海盐 314300;
    2.江苏大学 材料科学与工程学院, 江苏 镇江 212013
  • 收稿日期:2024-07-29 修回日期:2024-11-05 出版日期:2025-01-25 发布日期:2025-03-12
  • 通讯作者: 李冬升,正高级实验师,博士,E-mail:13952883863@163.com
  • 作者简介:徐 科(1982—),男,高级工程师,硕士,主要研究方向为核电厂材料、失效分析,E-mail:xke@cnnp.com.cn。

Effect of cryogenic treatment on microstructure and properties of nuclear grade low carbon steel

Xu Ke1, Hu Minglei1, Zhang Wei1, Hu Bin1, Li Dongsheng2, Liu Rencai2   

  1. 1. CNNC Nuclear Power Operation Management Co., Ltd., Haiyan Zhejiang 314300, China;
    2. School of Materials Science and Engineering, Jiangsu University, Zhenjiang Jiangsu 212013, China
  • Received:2024-07-29 Revised:2024-11-05 Online:2025-01-25 Published:2025-03-12

摘要: 为研究深冷处理对核电级低碳钢材料力学性能及组织演变的影响,利用显微硬度计、X射线衍射仪、扫描电镜及透射电镜等对经不同热处理工艺后20钢的力学性能及显微组织进行了表征。结果表明,回火处理促进部分残留奥氏体转变为马氏体以及碳原子的析出导致马氏体细化,使得硬度从淬火态的468.5 HV0.1提高至回火态的480.3 HV0.1;深冷处理促进试验钢中残留奥氏体转变为细小的板条状马氏体,同时,深冷处理引起试验钢中的马氏体产生晶格畸变,使得组织内应力和位错等缺陷增多,进而促进马氏体中碳原子的析出,导致析出强化作用增强,致使试验钢经淬火-深冷-回火处理的硬度提高至495.3 HV0.1。

关键词: 低碳钢, 深冷处理, 显微硬度, 板条状马氏体, 残留奥氏体

Abstract: In order to study the effect of cryogenic treatment on mechanical properties and microstructure evolution of nuclear grade mild steel, the mechanical properties and microstructure of 20 steel after different heat treatments were characterized by means of microhardness tester, XRD, SEM and TEM. The results show that the tempering treatment promotes the transformation of partial retained austenite into martensite and the precipitation of carbon atoms leading to martensite refinement, resulting in an increase in hardness from 468.5 HV0.1 of the quenched steel to 480.3 HV0.1 of the tempered steel. The cryogenic treatment promotes the transformation of the retained austenite into fine lath martensite in the tested steel, and at the same time, the cryogenic treatment causes lattice distortion in the martensite, which leads to the increase of stresses and defects such as dislocations in the microstructure, which in turn promotes the precipitation of carbon atoms in the martensite, leading to the enhancement of precipitation strengthening, resulting in the increase of hardness of the tested steel to 495.3 HV0.1 after quenching-cryogenic-tempering treatment.

Key words: mild steel, cryogenic treatment, microhardness, lath martensite, retained austenite

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