金属热处理 ›› 2020, Vol. 45 ›› Issue (10): 54-59.DOI: 10.13251/j.issn.0254-6051.2020.10.011

• 工艺研究 • 上一篇    下一篇

回火温度对不同淬火处理0.6C超级贝氏体钢组织及性能的影响

孙林1, 洪振军2,3, 胡坤4, 苏震1, 徐新乐1, 金阳1, 董达善4   

  1. 1.中国兵器工业新技术推广研究所, 北京 100089;
    2.上海交通大学 材料科学与工程学院, 上海 200240;
    3.内蒙古第一机械集团有限公司, 内蒙古 包头 014030;
    4.上海海事大学 物流工程学院, 上海 201306
  • 收稿日期:2020-04-19 出版日期:2020-10-25 发布日期:2020-12-29
  • 通讯作者: 董达善,教授,博士,E-mail: dsdong@shmtu.edu.cn
  • 作者简介:孙 林(1985—),男,高级工程师,博士,主要研究方向为热处理工艺和设备,E-mail: sunlinbeijing@163.com。
  • 基金资助:
    国防基础科研计划(JCKY2017208B003)

Effect of tempering temperature on microstructure and properties of 0.6C super bainitic steel quenched by different methods

Sun Lin1 , Hong Zhenjun2,3, Hu Kun4, Su Zhen1, Xu Xinle1, Jin Yang1, Dong Dashan4   

  1. 1. China North Advanced Technology Generalization Institute, Beijing 100089, China;
    2. School of Materials Science and Engineering, Shanghai Jiao Tong University, Shanghai 200240, China;
    3. Inner Mongolia First Machinery Group Co., Ltd., Baotou Inner Monglia 014030, China;
    4. Logistics Engineering College, Shanghai Maritime University, Shanghai 201306, China
  • Received:2020-04-19 Online:2020-10-25 Published:2020-12-29

摘要: 分析了不同回火温度下等温盐浴和淬火-配分-回火(Q-P-T)工艺处理0.6C超级贝氏体钢的微观组织和力学性能。结果表明:经230 ℃×10 h+320 ℃×7 h两步法等温淬火处理后,试样在360~500 ℃温度区间出现明显的第二类回火脆性,而Q-P-T试样回火脆性温度区间为450~470 ℃,经Q-P-T工艺处理后,回火脆性温度区间明显变窄,试样力学性能全面提高。利用SEM、TEM、XRD等手段对显微组织进行表征,揭示了Q-P-T试样优于等温处理的两个主要因素:经Q-P-T工艺处理后,微观组织更为细化,随着亚晶界的增多,组织稳定性进一步增强,碳化物晶界偏聚受到阻碍,难以连接成网状,故经Q-P-T工艺处理后试样第二类回火脆性区间极大缩小;经Q-P-T工艺处理后薄膜状残留奥氏体含量增大,奥氏体更为稳定,有利于减弱第二类回火脆性的影响。

关键词: 超级贝氏体钢, Q-P-T工艺, 第二类回火脆性, 碳化物偏聚, 薄膜状残留奥氏体

Abstract: Microstructure and mechanical properties of the 0.6C super bainitic steel were analyzed after isothermal salt bath quenching and quenching-partitioning-tempering (Q-P-T) respectively and then tempering at different temperatures. The results indicate that the reversible temper brittleness appears in the temperature range of 360-500 ℃ after treated by two-step austempering at 230 ℃×10 h and 320 ℃×7 h, while the tempering brittleness temperature range of Q-P-T specimen is 450-470 ℃. Respectively, after Q-P-T process, the tempering brittleness temperature range is obviously narrowed and the mechanical properties of the specimen are improved. The microstructural characterization by SEM, TEM and XRD reveals two main factors resulting in the mechanical properties of the Q-P-T specimen superior to those of the isothermal treatments: after the Q-P-T treatment, the microstructure is more refined, and with the increase of subgrain boundaries, the stability of the microstructure is further enhanced, and the carbide segregation to the grain boundaries is hindered, so it is difficult to connect into a network. Therefore, after the Q-P-T treatment, the reversible temper brittleness temperature range is greatly reduced; after the Q-P-T treatment, the film-like retained austenite increases in the content and is more stable, which is beneficial to weaken the influence of reversible temper brittleness.

Key words: super-bainitic steel, Q-P-T process, reversible temper brittleness, carbide segregation, film-like retained austenite

中图分类号: