冷轧方式和退火温度对Al-4Cu-0.73Mg合金织构和微观组织的影响

doi:10.13251/j.issn.0254-6051.2021.09.010

金属热处理 ›› 2021, Vol. 46 ›› Issue (9): 58-64.DOI: 10.13251/j.issn.0254-6051.2021.09.010

冷轧方式和退火温度对Al-4Cu-0.73Mg合金织构和微观组织的影响

蒋莺鸽, 黄继武, 江福清, 许成龙

中南大学材料科学与工程学院, 湖南长沙 410083

收稿日期:2021-03-11 出版日期:2021-09-25 发布日期:2021-12-09
通讯作者: 黄继武,教授,博士,E-mail:huangjw@csu.edu.cn
作者简介:蒋莺鸽(1996—),女,硕士研究生,主要研究方向为Al-Cu-Mg合金交叉轧制后织构及各向异性,E-mail:1575770084@qq.com。
基金资助:
广东省重点领域研发计划(2020B010186002)

Effect of cold rolling mode and annealing temperature on microstructure and texture evolution of Al-4Cu-0.73Mg alloy

Jiang Yingge, Huang Jiwu, Jiang Fuqing, Xu Chenglong

School of Materials Science and Engineering, Central South University, Changsha Hunan 410083, China

Received:2021-03-11 Online:2021-09-25 Published:2021-12-09

摘要/Abstract

摘要： 采用硬度测试、X射线衍射(XRD)、电子背散射衍射(EBSD)等方法研究了单向轧制、交叉轧制和退火温度对Al-4Cu-0.73Mg(wt%)合金织构演变和微观组织的影响。结果表明:单向轧制试样在100~300 ℃退火保温1 h后显示出明显的Copper织构{112} <111>、S织构{123} <634>和Brass织构{011}<211>,而交叉轧制试样表现出强烈的Brass织构和H织构{011}<755>。当退火温度高于300 ℃,单向轧制和交叉轧制试样中的变形织构逐渐沿α取向线转变为由P织构{011}<001>、L织构{011}<011>、E织构{111}<110>和R织构{124}<211>等组成的再结晶织构。单向轧制和交叉轧制试样的晶粒尺寸随退火温度的升高先增加后减小,均在350 ℃退火1 h后有最大晶粒尺寸,分别约为8.2 μm和11.5 μm。单向轧制和交叉轧制试样均在冷轧后硬度值最高,约为108 HV,之后硬度值随退火温度的升高而逐渐下降,两种轧制试样的硬度值最终均稳定在50 HV左右。总体来看,轧制方式对试样织构的影响比对力学性能的影响大。

关键词: Al-4Cu-0.73Mg合金, 单向轧制, 交叉轧制, 织构, 再结晶

Abstract: Effects of parallel rolling (PR), cross rolling (CR) and annealing temperature on microstructure and texture evolution of the Al-4Cu-0.73Mg(wt%) alloy were investigated by means of mechanical properties test, X-ray diffraction(XRD) and electron backscatter diffraction(EBSD). The results show that after annealing at 100-300 ℃ for 1 h, the PR specimens show obvious copper{112}<111>, S{123}<634> and Brass{011}<211> textures, while the CR specimens exhibit strong Brass texture and H{011}<755> texture. When the annealing temperature exceeds 300 ℃, the deformation textures in the PR and CR specimens gradually transform into recrystallization textures along α fiber, which consist of P {011} <001>, L {011} <011>, E {111} < 110> and R {124} <211>. The grain size of PR and CR specimens first increase and then decrease with the increase of annealing temperature, and the largest grain size can be obtained after annealing at 350 ℃ for 1 h, which are about 8.2 μm and 11.5 μm, respectively. Both the PR and CR specimens without annealing show the highest hardness values of ~108 HV, which gradually decrease with the increase of annealing temperature and finally are stable at about 50 HV. Overall, the effect of rolling modes on specimen textures is greater than that on mechanical properties.

Key words: Al-4Cu-0.73Mg alloy, parallel rolling, cross rolling, texture, recrystallization

中图分类号:

TG146.2⁺1

蒋莺鸽, 黄继武, 江福清, 许成龙. 冷轧方式和退火温度对Al-4Cu-0.73Mg合金织构和微观组织的影响[J]. 金属热处理, 2021, 46(9): 58-64.

Jiang Yingge, Huang Jiwu, Jiang Fuqing, Xu Chenglong. Effect of cold rolling mode and annealing temperature on microstructure and texture evolution of Al-4Cu-0.73Mg alloy[J]. Heat Treatment of Metals, 2021, 46(9): 58-64.

参考文献

[1]Williams James C, StarkeJr Edgar A. Progress in structural materials for aerospace systems[J]. Acta Materialia, 2003, 51(19): 5775-5799.
[2]Zhang J X, Ma M, Liu W C. Effect of initial grain size on the recrystallization and recrystallization texture of cold-rolled AA 5182 aluminum alloy[J]. Materials Science and Engineering A, 2017, 690: 233-243.
[3]Kong X Y, Liu W C, Li J, et al. Deformation and recrystallization textures in straight-rolled and pseudo cross-rolled AA 3105 aluminum alloy[J]. Journal of Alloys and Compounds, 2010, 491(1/2): 301-307.
[4]Öztürk T. Deformation and recrystallization textures in cross-rolled sheets of copper and α-brass[J]. Scripta Metallurgica, 1988, 22(10): 1611-1616.
[5]Takeshita T, Kurata Y, Hasegawa S. Bonding properties of glow-discharge polycrystalline and amorphous Si-C films studied by X-ray diffraction and X-ray photoelectron spectroscopy[J]. Journal of Applied Physics, 1992, 71: 5395-5400.
[6]Yang H W, Widiantara I P, Ko Y G. Effect of deformation path on texture and tension properties of submicrocrystalline Al-Mg-Si alloy fabricated by differential speed rolling[J]. Materials Letters, 2018, 213: 54-57.
[7]Hong S H, Dong N L. Deformation and recrystallization textures in cross-rolled copper sheet[J]. Journal of Engineering Materials and Technology, 2002, 124(1): 13-22.
[8]Hong S H, Dong N L. Deformation of cube-oriented grains and formation of recrystallized cube grains in a hot deformed commercial AlMgMn aluminium alloy[J]. Acta Materialia, 1996, 44(11): 4447-4462.
[9]El-Baradie Z M, El-Sayed M. Effect of double thermomechanical treatments on the properties of 7075 Al alloy[J]. Journal of Materials Processing Technology, 1996, 62(1/3): 76-80.
[10]Zhao Q, Liu Z, Hu Y, et al. Evolution of Goss texture in an Al-Cu-Mg alloy during cold rolling[J]. Archives of Civil and Mechanical Engineering, 2020, 20(1):Doi:10.1007/S43452-020-00023-3.
[11]宋旭东, 袁鸽成, 黎小辉, 等. 异步轧制Mg-3Zn-2(Ce/La)-1Mn合金的微观组织及织构演变[J]. 金属热处理, 2020, 45(2): 1-6.
Song Xudong, Yuan Gecheng, Li Xiaohui, et al. Microstructure and texture evolution of differential speed rolled Mg-3Zn-2(Ce/La)-1Mn alloy[J]. Heat Treatment of Metals, 2020, 45(2): 1-6.
[12]Daaland O, Nes E. Recrystallization texture development in commercial Al-Mn-Mg alloys[J]. Acta Materialia, 1996, 44(4): 1413-1435.
[13]SjLstad K, Engler O, Tangen S, et al. Recrystallization textures and the evolution of the P-orientation as a function of precipitation in an AA3103 alloy[J]. Materials Science Forum, 2002, 408-412: 1471-1476.
[14]刘杨邦, 苏学宽, 黄晖, 等. 退火温度对Al-4.5Mg-0.7Mn-0.4Er-0.1Zr铝合金组织与性能的影响[J]. 金属热处理, 2008, 33(12): 77-80.
Liu Yangbang, Su Xuekuan, Huang Hui, et al. Effect of annealing temperature on microstructure and properties of Al-4.5Mg-0.7Mn-0.4Er-0.1Zr alloy[J]. Heat Treatment of Metals, 2008, 33(12): 77-80.
[15]Engler O. On the origin of the R orientation in the recrystallization textures of aluminum alloys[J]. Metallurgical and Materials Transactions A, 1999, 522(491): 524-538.
[16]Wei W, Wei K X, Fan G J. A new constitutive equation for strain hardening and softening of fcc metals during severe plastic deformation[J]. Acta Materialia, 2008, 56(17): 4771-4779.
[17]Shi C, Lai J, Chen X G. Microstructural evolution and dynamic softening mechanisms of Al-Zn-Mg-Cu alloy during hot compressive deformation[J]. Materials, 2014, 7(1): 244-264.
[18]Li H, Chen P, Wang Z, et al. Tensile properties, microstructures and fracture behaviors of an Al-Zn-Mg-Cu alloy during ageing after solution treating and cold-rolling[J]. Materials Science and Engineering A, 2019, 742: 798-812.

冷轧方式和退火温度对Al-4Cu-0.73Mg合金织构和微观组织的影响

Effect of cold rolling mode and annealing temperature on microstructure and texture evolution of Al-4Cu-0.73Mg alloy

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