金属热处理 ›› 2023, Vol. 48 ›› Issue (4): 303-306.DOI: 10.13251/j.issn.0254-6051.2023.04.048

• 测试与分析 • 上一篇    下一篇

采用金相法对17-7PH不锈钢钢丝表层残留奥氏体深度测试

林文钦, 李东升, 邓枫, 吴佳欣, 蒋洪俊, 杨元熙, 徐心洁, 刘吕波   

  1. 航空工业成都飞机工业集团有限责任公司, 四川 成都 610091
  • 收稿日期:2022-10-08 修回日期:2023-01-10 发布日期:2023-05-27
  • 作者简介:林文钦(1986—),男,高级工程师,主要研究方向为金属材料分析, E-mail:463716670@qq.com

Retained austenite depth test of 17-7PH stainless steel wire by metallographic method

Lin Wenqin, Li Dongsheng, Deng Feng, Wu Jiaxin, Jiang Hongjun, Yang Yuanxi, Xu Xinjie, Liu Lübo   

  1. AVIC Chengdu Aircraft Industrial Group Co., Ltd., Chengdu Sichuan 610091, China
  • Received:2022-10-08 Revised:2023-01-10 Published:2023-05-27

摘要: AMS5678G材料规范要求采用金相法对17-7PH不锈钢钢丝表层残留奥氏体深度进行测试,针对测试中存在的试样制备和残留奥氏体层深度界定问题,对试样夹的选择、侵蚀方式与侵蚀时间、残留奥氏体层深度界定进行了试验。结果表明,为避免残留奥氏体显示时化学浸蚀电位的影响,宜采用塑料试样夹进行镶嵌;使用Fry's 试剂以擦拭的方式,擦拭5~10 s显示组织较合适;当钢丝表层存在残留奥氏体层时,其深度界定为致密的残留奥氏体层深度,得到材料规范归口单位认可。

关键词: 17-7PH钢丝, 表层残留奥氏体, 深度测试, 金相法

Abstract: In accordance with the AMS5678G material specification of 17-7PH stainless steel wire, metallographic method is required to test the depth of retained austenite on surface. In view of the problem of specimen preparation and the definition of the depth of retained austenite layer, the selection of specimen clips, erosion method and etching time, and depth definition of retained austenitic layer were tested. It is concluded that in order to avoid the influence of chemical erosion potential during retained austenite display, plastic sample clip should be used for inlay; using Fry's reagent to wipe the specimen with a wiping time of 5-10 s is a more suitable way to reveal the microstructure. When there is a retained austenitic layer on surface of the steel wire, its depth is defined as the dense retained austenitic layer depth, which is approved by the material specification unit.

Key words: 17-7PH steel wire, retained austenite on surface layer, depth test, metallographic method

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