金属热处理 ›› 2024, Vol. 49 ›› Issue (1): 215-222.DOI: 10.13251/j.issn.0254-6051.2024.01.035

• 工艺研究 • 上一篇    下一篇

均匀化制度对6014铝合金显微组织的影响

迟蕊1, 李延成1, 孟双1, 徐志远1, 于俊芃1, 张德镇1, 郭丰佳1,2, 孙宁1,2   

  1. 1. 山东南山铝业股份有限公司 国家铝合金压力加工工程技术研究中心, 山东 烟台 265700;
    2. 山东南山铝业股份有限公司 有色金属产业研究院, 山东 烟台 265700
  • 收稿日期:2023-07-28 修回日期:2023-10-25 发布日期:2024-02-29
  • 作者简介:迟 蕊(1992—),女,工程师,硕士,主要研究方向为汽车铝合金板材研发,E-mail:chirui@nanshan.com.cn

Effect of homogenization process on microstructure of 6014 aluminum alloy

Chi Rui1, Li Yancheng1, Meng Shuang1, Xu Zhiyuan1, Yu Junpeng1, Zhang Dezhen1, Guo Fengjia1,2, Sun Ning1,2   

  1. 1. National Engineering Research Center for Plastic Working of Aluminum Alloys, Shandong Nanshan Aluminum Co.,Ltd., Yantai Shandong 265700, China;
    2. Non-ferrous Metal Industry Research Institute, Shandong Nanshan Aluminum Co., Ltd., Yantai Shandong 265700, China
  • Received:2023-07-28 Revised:2023-10-25 Published:2024-02-29

摘要: 借助光学显微镜的明暗场像、差示扫描量热法、扫描电镜及透射电镜等手段,研究了不同均匀化制度对6014铝合金的组织、富铁相转变、元素分布和弥散相均匀性的影响。结果表明,6014铝合金铸锭中存在枝晶偏析现象和非平衡共晶组织,合金元素含量波动较大,晶粒为等轴晶。铸锭中的第二相含量明显高于单级和双级均匀化态,由于第二相形态和分布不同,可分为α-AlFeMnSi、β-AlFeSi、Mg2Si和Q-AlCuMgSi相。采用560 ℃×4 h+540 ℃×6 h双级均匀化处理制度时,网状枝晶并未全部断裂,延长560 ℃一级均匀化保温时间至12 h时,较多的β-AlFeSi相转变为α-AlFeMnSi相。采用560 ℃×19 h单级均匀化处理时,枝晶基本由网状形态转变为链状形态。采用580 ℃×4 h+540 ℃×6 h双级均匀化制度时,弥散相α-AlFeMnSi分布较为均匀,延长580 ℃一级均匀化保温时间至12 h时,组织发生过烧,弥散相尺寸增大且在晶界周围富集。

关键词: 6014铝合金, 均匀化制度, 组织, 弥散相均匀性

Abstract: Effect of homogenization process on microstructure, iron-rich phase transformation, element distribution and dispersion phase uniformity of 6014 aluminum alloy was studied by means of bright and dark field images of optical microscope, differential scanning calorimetry, scanning electron microscope, transmission electron microscope. The results show that the dendrite segregation and non-equilibrium eutectic structure are found in the 6014 aluminum alloy ingot, the element content fluctuates greatly, and the grain is equiaxed. The content of the second phase in the ingot is significantly higher than that after homogenization treatment. Due to the different morphology and distribution of the second phase, it can be divided into α-AlFeMnSi, β-AlFeSi, Mg2Si and Q-AlCuMgSi phase, respectively. After two-stage homogenization at 560 ℃ for 4 h and 540 ℃ for 6 h, the reticular dendrites are not completely broken. When the holding time of first-stage homogenization at 560 ℃is extended to 12 h, more β-AlFeSi phase is transformed into α-AlFeMnSi phase. After single-stage homogenization at 560 ℃for 19 h, the dendrites are basically changed from reticular morphology to chain morphology. After two-stage homogenization at 580 ℃ for 4 h and 540 ℃ for 6 h, the dispersed α-AlFeMnSi phase is distributed more uniform. When the holding time of first-stage homogenization at 580 ℃ is extended to 12 h, overburing occurrs and the size of the dispersion phase increases which enriches around the grain boundary.

Key words: 6014 aluminum alloy, homogenization process, microstructure, dispersion phase uniformity

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