金属热处理 ›› 2024, Vol. 49 ›› Issue (11): 246-255.DOI: 10.13251/j.issn.0254-6051.2024.11.038

• 工艺研究 • 上一篇    下一篇

时效温度对轧制Mg-Al-Ca-Mn-Zn合金组织及阻尼性能的影响

裴梦雨1, 孙有平1,2,3, 何江美1, 刘华燊1, 刘鑫雨1   

  1. 1.广西科技大学 机械与汽车工程学院, 广西 柳州 545006;
    2.广西土方机械协同创新中心, 广西 柳州 545006;
    3.广西汽车零部件与整车技术重点实验室, 广西 柳州 545006
  • 收稿日期:2024-05-26 修回日期:2024-09-18 出版日期:2024-11-25 发布日期:2025-01-09
  • 通讯作者: 孙有平,教授,博士,E-mail:syptaiii@126.com
  • 作者简介:裴梦雨(1999—),女,硕士研究生,主要研究方向为镁合金塑性成形,E-mail:peimengyude@163.com。
  • 基金资助:
    广西重点研发计划(桂科AB23026104)

Effect of aging temperature on microstructure and damping properties of rolled Mg-Al-Ca-Mn-Zn alloy

Pei Mengyu1, Sun Youping1,2,3, He Jiangmei1, Liu Huashen1, Liu Xinyu1   

  1. 1. School of Mechanical and Automotive Engineering, Guangxi University of Science and Technology, Liuzhou Guangxi 545006, China;
    2. Guangxi Earthmoving Machinery Collaborative Innovation Center, Liuzhou Guangxi 545006, China;
    3. Guangxi Key Laboratory of Automobile Components and Vehicle Technology, Liuzhou Guangxi 545006, China
  • Received:2024-05-26 Revised:2024-09-18 Online:2024-11-25 Published:2025-01-09

摘要: 采用光学显微镜(OM)、动态热分析仪、X射线衍射仪(XRD)、拉伸试验机以及扫描电镜(SEM)等设备,研究了时效处理对多道次轧制+退火处理Mg-1.2Al-0.4Ca-0.3Mn-0.3Zn镁合金板材的显微组织、力学性能以及阻尼性能的影响。结果表明,退火态的平均晶粒尺寸为4.82 μm,存在少量孪晶,抗拉强度和伸长率分别为212.09 MPa和9.87%;时效温度为150 ℃时,平均晶粒尺寸为4.95 μm,抗拉强度为207.84 MPa,伸长率为6.58%;时效温度为190 ℃时,平均晶粒尺寸为4.05 μm,晶粒细小且分布均匀,合金晶界处中出现Al-Mn、Al-Ca以及Mg2Ca等第二相,使得综合力学性能良好,抗拉强度为224.21 MPa,伸长率为14.2%。在低应变振幅区(ε≤0.1%),轧制态、退火态、150 ℃和190 ℃时效态合金的阻尼值差别不大,在高应变振幅区(ε>0.1%),190 ℃时效合金的阻尼性能最好;在低温区(35~150 ℃),4种状态合金的阻尼峰均由位错滑移引起;在高温区(150~375 ℃),轧制态合金的阻尼峰最高,轧制态、退火态和150 ℃时效态合金的阻尼峰由位错滑移引起,190 ℃时效态合金的阻尼峰由位错滑移和晶界滑移叠加得到。

关键词: 时效温度, 显微组织, 阻尼性能, Mg-Al-Ca-Mn-Zn合金

Abstract: Effect of aging treatment on microstructure, mechanical properties and damping properties of Mg-1.2Al-0.4Ca-0.3Mn-0.3Zn magnesium alloy plates after multi-pass rolling+annealing was investigated by means of optical microscope (OM), dynamic thermal analyzer, X-ray diffractor (XRD), tensile testing machine and scanning electron microscope (SEM). The results show that the average grain size of the annealed alloy is 4.82 μm with a small amount of twin, and the tensile strength and elongation are 212.09 MPa and 9.87%, respectively. When the aging temperature is 150 ℃, the average grain size is 4.95 μm, the tensile strength is 207.84 MPa, and the elongation is 6.58%. When the aging temperature is 190 ℃, the average grain size is 4.05 μm, the grains are fine and uniformly distributed and the second phases such as Al-Mn, Al-Ca and Mg2Ca appear at the grain boundaries of the alloy, which results in good mechanical properties, with tensile strength of 224.21 MPa and elongation of 14.2%. In the low strain amplitude region (ε≤0.1%), the damping values of the alloy rolled, annealed, 150 ℃ aged and 190 ℃ aged are not significantly different. While, in the high strain amplitude region (ε>0.1%), the damping properties of the 190 ℃ aged alloy is the best. In the low-temperature range of 35-150 ℃, the damping peaks of the alloy in four states are all caused by dislocation slip, but in the high temperature range of 150-375 ℃, the damping peak of the rolled state alloy is the highest, and the damping peaks of the rolled, annealed and 150 ℃ aged alloys are caused by dislocation slip, and the damping peak of the 190 ℃ aged alloy is obtained by the superposition of the dislocation slip and the sliding of the grain boundary.

Key words: aging temperature, microstructure, damping properties, Mg-Al-Ca-Mn-Zn alloy

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