金属热处理 ›› 2024, Vol. 49 ›› Issue (12): 85-89.DOI: 10.13251/j.issn.0254-6051.2024.12.014

• 工艺研究 • 上一篇    下一篇

风电螺栓用4140圆钢的球化退火工艺

陶涛, 陈颖, 熊兵, 赵海洋, 张世平   

  1. 南京钢铁股份有限公司, 江苏 南京 210044
  • 收稿日期:2024-07-01 修回日期:2024-10-29 出版日期:2024-12-25 发布日期:2025-02-05
  • 作者简介:陶 涛(1983—),男,工程师,硕士,主要研究方向为特殊钢棒线材产品开发及其工艺研究,E-mail:ttmset@163.com

Spheroidizing annealing process of 4140 steel bar used in wind power bolts

Tao Tao, Chen Ying, Xiong Bing, Zhao Haiyang, Zhang Shiping   

  1. Nanjing Iron and Steel Co., Ltd., Nanjing Jiangsu 210044, China
  • Received:2024-07-01 Revised:2024-10-29 Online:2024-12-25 Published:2025-02-05

摘要: 针对新设计的4140钢在热膨胀仪测定其相变点的基础上,利用Gleeble-3800热力模拟试验机对其进行不同的球化退火(亚温球化退火、逐步冷却球化退火和等温球化退火)热模拟。结果表明,进行亚温球化退火试验时,即使长时间保温,原马氏体区域已经球化,而原贝氏体区域才刚开始球化;进行逐步冷却球化退火试验时,球化率提高至75%,且随着加热温度的升高,片状渗碳体含量增加;等温球化退火工艺试验采用760 ℃加热+720 ℃等温时,4140钢球化率可提升至82%,硬度也满足用户≤185 HBW的要求,但微区有碳化物聚集现象,因此根据Thermo-Calc计算4140钢等温转变曲线,在等温球化退火前增加一个700 ℃的预热段。结合改进后的预热+等温球化退火工艺试验,在现场连续式热处理炉生产线上实现满足设计要求的4140圆钢,球化率≥90%,布氏硬度≤175 HBW,且组织均匀。

关键词: 4140钢, 球化退火, 球化率, 布氏硬度

Abstract: Based on the phase transition points of a new designed 4140 steel determined using a dilatometer, the Gleeble-3800 thermal simulator was used to conduct different spheroidizing annealing simulations, including subcritical spheroidizing annealing, step cooling spheroidizing annealing, and isothermal spheroidizing annealing. The results show that during subcritical spheroidizing annealing, even after a long holding time, the original martensitic region is spheroidized, while the original bainitic region just begins to spheroidize. In the step cooling spheroidizing annealing test, the spheroidization rate is increased to 75%, and as the heating temperature increases, the amount of lamellar cementite also increases. For the isothermal spheroidizing annealing process, heating at 760 ℃ followed by isothermal holding at 720 ℃ results in a spheroidization rate of 82%, with hardness meeting the user's requirement of ≤185 HBW. However, localized carbide aggregation is observed. Therefore, based on Thermo-Calc calculations of the isothermal transformation curve for the 4140 steel, a preheating stage at 700 ℃ is added before the isothermal spheroidizing annealing. With the optimized preheating+isothermal spheroidizing annealing process, the continuous heat treatment furnace in the production line successfully produces 4140 round steel that meets the design specifications, achieving spheroidization rate of ≥90%, Brinell hardness of ≤175 HBW, with uniformly distributed microstructure.

Key words: 4140 steel, spheroidizing annealing, spheroidization rate, Brinell hardness

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