Comparative analysis of standards for determining average grain size

doi:10.13251/j.issn.0254-6051.2020.04.045

Abstract

Abstract: Five aspects of 17 standards for determining average grain size of metallic materials were compared and analyzed, including the definitions of the grain size, the chart comparison procedure, the planimetric procedure, the intercept procedure, and the accuracy. The consistencies, differences and shortcomings among these standards were clarified through comparative analysis, and the results were conducive to the selecting and using of the standards by metallographers and the continual improvement of standardization work.

Key words: average grain size, standardization, comparative analysis of standards

CLC Number:

TG157

Bi Geping, Chen Jinzhe, Tan Wenhua, Li Qiao. Comparative analysis of standards for determining average grain size[J]. Heat Treatment of Metals, 2020, 45(4): 212-220.

References

[1]ISO 643: 2012, Steels — Micrographic Determination of the Apparent Grain Size[S].
[2]ASTM E112-13, Standard Test Methods for Determining Average Grain Size[S].
[3]GB/T 6394—2017, 金属平均晶粒度测定方法[S].
GB/T 6394—2017, Determination of Estimating the Average Grain Size of Metal[S].
[4]GB/T 4296—2004, 变形镁合金显微组织检验方法[S].
GB/T 4296—2004, Inspection Method for Microstructure of Wrought Magnesium Alloy[S].
[5]YS/T 347—2004, 铜及铜合金平均晶粒度测定法[S].
YS/T 347—2004, Copper and Copper Alloys—Estmation of Average Grain Size[S].
[6]GB/T 3246.1—2000, 变形铝及铝合金制品显微组织检验方法[S].
GB/T 3246.1—2000, Inspection Method for Structure of Wrought Aluminum and Aluminum Alloy Products—Part 1: Inspection Method for Microstructure[S].
[7]GB/T 3246.2—2012, 变形铝及铝合金制品组织检验方法第2部分低倍组织检验方法[S].
GB/T 3246.2—2012, Inspection Method for Structure of Wrought Aluminum and Aluminum Alloy Products—Part 2: Inspection Method for Macrostructure[S].
[8]GB/T 4335—2013, 低碳钢冷轧薄板铁素体晶粒度测定法[S].
GB/T 4335—2013, Determination of Ferrite Grain Size For Cold Rolled Low Carbon Steel Sheets[S].
[9]JB/T 5108—2018, 铸造黄铜金相检验[S].
JB/T 5108—2018, Metallographic Test for Cast Brass[S].
[10]JB/T 7946.4—2017, 铸造铝合金金相第4部分: 铸造铝铜合金晶粒度[S].
JB/T 7946.4—2017, Metallograph of Cast Aluminium Alloys—Part 4: Cast Aluminium-Copper Alloys Grain Size[S].
[11]GB/T 4197—1984, 钨、钼及其合金的烧结坯条、棒材晶粒度测试方法[S].
GB/T 4197—1984, Method for Measuring the Average Grain Size of Sintered Bas and Rod of Tungsten Molybdenum and Alloys[S].
[12]GB/T 24177—2009, 双重晶粒度表征与测定方法[S].
GB/T 24177—2009, Standard Test Methods for Characterizing Duplex Grain Sizes[S].
[13]ASTM E1181-02, Standard Test Methods for Characterizing Duplex Grain Sizes[S].
[14]YB/T 4290—2012, 金相检测面上最大晶粒尺寸级别(ALA晶粒度)测定方法[S].
YB/T 4290—2012, Test Methods for Estimating the Largest Grain Observed in a Metallographic Section (ALA Grain Size)[S].
[15]ASTM E930-99(2007), Standard Test Methods for Estimating the Largest Grain Observed in a Metallographic Section (ALA Grain Size)[S].
[16]JB/T 9204—2008, 钢件感应淬火金相检验[S].
JB/T 9204—2008, Metallographic Examination Of Induction Hardened Steel Parts[S].
[17]GB/T 36165—2018, 金属平均晶粒度的测定电子背散射衍射(EBSD)法[S].
GB/T 36165—2018, Determination of Average Grain Size of Metal Electron Backscatter Diffraction(EBSD) Method[S].
[18]GB/T 30067—2013, 金相学术语[S].
GB/T 30067—2013, Standard Terminology Relating to Metallography[S].
[19]ASTM E7-03, Standard Terminology Relating to Metallography[S].
[20]毕革平, 吴京利, 李江豫, 等. 数码照相技术在金相显微镜上的应用[J]. 钢铁研究学报, 1999, 11(6): 57-59.
Bi Geping, Wu Jingli, Li Jiangyu, et al. Application of digital photographic technology in metallurgical microscope[J]. Journal of Iron and Steel Research, 1999, 11(6): 57-59.
[21]毕革平, 林家明, 吴伯群. 金相显微镜数字化照相系统[J]. 材料工程, 2000(5): 45-48.
Bi Geping, Lin Jiaming, Wu Boqun. Digital photo graphic system of metallurgical microscope[J]. Journal of Materials Engineering, 2000(5): 45-48.
[22]CNAS-CL01: 2018, 检测和校准实验室能力认可准则[S].
CNAS-CL01: 2018, Accreditation Criteria for the Competence of Testing and Calibration Laboratories[S].
[23]ISO/IEC 17025: 2017, Accreditation Criteria for the Competence of Testing and Calibration Laboratories[S].
[24]RB/T 214—2017, 检验检测机构资质认定能力评价检验检测机构通用要求[S].
RB/T 214—2017, Competence Assessment for Inspection Body and Laboratory Mandatory Approval—Genaral Requirements for Inspection Body and Laboratory[S].
[25]毕革平, 李俏, 雷闽, 等. 热处理金相照片技术要求标准化研究[J]. 金属热处理, 2016, 41(12): 216-220.
Bi Geping, Li Qiao, Lei Min, et al. Standardization of heat treatment metallograph[J]. Heat Treatment of Metals, 2016, 41(12): 216-220.
[26]GB/T 4889—2008, 数据的统计处理和解释正态分布均值和方差的估计与检验[S].
GB/T 4889—2008, Statistical Interpretation of Data — Techniques of Estimation and Tests Relating to Means and Variances of Normal Distribution[S].
[27]GB/T 3358.2—2009, 统计学词汇及符号第2部分: 应用统计[S].
GB/T 3358.2—2009, Statistics — Vocabulary and Symbols — Part 2: Applied Statistics[S].
[28]ISO 3534.2: 2006, Statistics Vocabulary and Symbols. Part 2: Applied Statistics[S].
[29]JJF 1001—2011, 通用计量术语及定义[S].
JJF 1001—2011, General Terms in Metrology and Their Definitions[S].
[30]Bi Geping, Guan Yong, Chen Xiaoyu, et al. Evaluation of uncertainty in determining average grain size by ASTM E112 standard[J]. Materials Science and Engineering, 2020, 733: 012045.
[31]Bi Geping, Guan Yong, Chen Xiaoyu, et al. Acceptability analysis of determining average grain size by ASTM E112 standard[J]. Materials Science and Engineering, 2020, 770: 012023.