Heat Treatment of Metals ›› 2022, Vol. 47 ›› Issue (12): 201-209.DOI: 10.13251/j.issn.0254-6051.2022.12.034

• MICROSTRUCTURE AND PROPERTY • Previous Articles     Next Articles

Evolution of microstructure and properties of nickel-based N06022 alloy pipe during solution treatment

Qin Xingwen, Ding Wenyan, Tu Zhengping, Shen Chengfei   

  1. Zhejiang Jiuli Hi-Tech Metals Co., Ltd., Huzhou Zhejiang 313028, China
  • Received:2022-08-07 Revised:2022-10-10 Online:2022-12-25 Published:2023-01-05

Abstract: Influence of solution treatment on microstructure evolution and properties of nickel-based N06022 alloy pipe was investigated by metallographic microscopy, scanning electron microscopy, energy spectrum analyzer, mechanical and corrosion performance test. The results show that the cold-rolled N06022 alloy pipe contains a large amount of precipitated phases, which have a pinning effect on grain boundaries, and the average grain size of the steel is hardly affected by the holding time, when the solution temperature is below 1100 ℃. When solution temperature increases to 1150 ℃, the grain size and growth rate increase sharply, which is mainly related to the dissolution of the precipitated phase. In the solution temperature range of 1000-1200 ℃, the activation energy of grain growth for 15 min and 30 min is QB=646.56 kJ/mol, QC=566.45 kJ/mol, respectively, and the relationship between the properties of the alloy and the grain size satisfies the Hall-Petch relationship. With the increase of solution temperature, the intergranular corrosion rate of the alloy decreases first and then stabilizes, the strength and hardness show slow-fast downward trend, and the elongation shows slow-fast upward trend. When the holding time is 15 min and the solution temperature is about 1150 ℃, the intersection of hardness curve and elongation curve appears, and the corrosion rate is stable, which is the optimal solution treatment process.

Key words: N06022 alloy, solution treatment, microstructure, tensile properties, hardness

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