Heat Treatment of Metals ›› 2024, Vol. 49 ›› Issue (7): 186-194.DOI: 10.13251/j.issn.0254-6051.2024.07.029

• SURFACE ENGINEERING • Previous Articles     Next Articles

Effect of medium-low temperature annealing on morphology, structure and electrical properties of MoS2 nano films

Liu Chunquan1, Xiong Fen1,2, Ma Jiayi2, Zhou Jintian1, Liang Zexun2, Huang Jianping1   

  1. 1. School of Materials Science and Engineering, Hunan Institute of Technology, Hengyang Hunan 421002, China;
    2. School of Computer Science and Engineering, Hunan Institute of Technology, Hengyang Hunan 421002, China
  • Received:2024-01-15 Revised:2024-04-17 Online:2024-07-25 Published:2024-08-29

Abstract: MoS2 nano films with different thicknesses were prepared by radio frequency (RF) magnetron sputtering via deposition at room temperature, and then annealed by different processes in 95%Ar+5%H2 mixed atmosphere. The structure, surface morphology and electrical properties of the MoS2 films were studied by means of atomic force microscope(AFM), Raman spectrum, four-probe and Hall tester. The results show that the MoS2 films grown on the silicon substrate are uniform and continuous. The annealing process can effectively remove the impurity oxygen in MoS2 films and improve its crystallinity, stability and structural integrity. The comprehensive properties of the MoS2 films are better when the deposition time is 40 min (the thickness is about 300 nm), while the crystallinity and electrical properties of the films after annealing at 500 ℃ for 60 min are all better.

Key words: MoS2 film, medium-low temperature annealing, crystallinity

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