Heat Treatment of Metals ›› 2025, Vol. 50 ›› Issue (2): 29-35.DOI: 10.13251/j.issn.0254-6051.2025.02.005

• MICROSTRUCTURE AND PROPERTIES • Previous Articles     Next Articles

Microstructure and hot deformation behavior of U-50%Zr alloy for nuclear fuel

Li Yanfeng1,2, Guo Hong1,2, Li Mingyang1,2, Hu Bingkun1,2, Liu Jiancheng1,2   

  1. 1. CNNC Key Laboratory on New Materials Research and Application Development, Baotou Inner Mongolia 014035, China;
    2. China North Nuclear Fuel Co., Ltd., Baotou Inner Mongolia 014035, China
  • Received:2024-12-06 Revised:2024-12-17 Published:2025-04-10

Abstract: U-50%Zr alloy for nuclear fuel was prepared by high-frequency induction melting, and its microstructure and phase constituent were analyzed using metallographic microscope and X-ray diffractometer. The Gleeble-3800 thermal simulation test machine was used to conduct hot compression tests at different deformation temperatures (500, 550 and 600 ℃) and strain rates (0.01 s, 0.1 and 1 s-1) to investigate its hot deformation behavior. The results show that, except for a deformation temperature of 600 ℃ and a strain rate of 0.01 s-1, the U-50%Zr alloy exhibits significant work hardening characteristics under other deformation conditions. At the same strain rate, the peak stress decreases with the increase of deformation temperature, especially at 600 ℃, where the peak stress decreases significantly compared to 500 ℃ and 550 ℃. At the same deformation temperature, the peak stress increases with the increase of strain rate. After hot deformation, no phase transformation occurs in the microstructure, all of which are δ-UZr2 phase. As the hot deformation temperature increases, the grain size of the alloy initially remains basically unchanged and then increases. At 500 ℃ and 550 ℃, the grain size is around 250 μm, and at 600 ℃, the grain size significantly increases to 493 μm. Based on peak stress, the constitutive equation of U-50%Zr alloy is established using the hyperbolic sine function Arrhenius model and temperature compensation factor Z parameter, with a hot deformation activation energy Q=694.9 kJ/mol. A hot working map is constructed using DMM dynamic material model, and the appropriate processing range is determined as follows: deformation temperature above 540 ℃, strain rate between 0.01 s-1 and 1 s-1.

Key words: nuclear fuel U-50%Zr alloy, hot compression deformation, constitutive equation, hot working map, microstructure

CLC Number: