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  • MICROSTRUCTURE AND PROPERTIES
    Pore morphologies and compressive strength of TiC/NiAl porous composites
    Guo Fengxue, Wu Jie, Chen Yunbo, Zuo Lingli, Liu Xiaoping
    2020, 45(5):  1-4.  doi:10.13251/j.issn.0254-6051.2020.05.001
    Abstract ( 69 )   PDF (670KB) ( 30 )  
    TiC/NiAl porous composites were synthesized in situ by self-propagating technology through controlling the reaction among Ti, C, Ni and Al powers. Influences of Ti-C contents (molar ratio 1∶1) on the pore morphologies and compressive strength of the porous materials were investigated. The results show that the pore morphology of the porous materials is mainly affected by the volatilization of adsorbed gases and the flow of liquid phase, the porosity and pore size increase with the increase of Ti-C content. When Ti-C content is 0-25%, the distribution of pores with near spherical morphology is uniform, and the pore size ranges between 20-70 μm, the compressive strength of the porous material increases with the increase of Ti-C content. When Ti-C content is 30%, besides the near spherical pores, some irregular and long narrow pores larger than 100 μm are formed, and the compressive strength decreases.
    Microstructure and properties of H13 steel treated by chromium plating and gas nitriding
    Li Chunming, Zhu Weiheng, Jiao Dongling, Wei Xingzhao
    2020, 45(5):  5-11.  doi:10.13251/j.issn.0254-6051.2020.05.002
    Abstract ( 66 )   PDF (589KB) ( 30 )  
    The chromium nitride was obtained on the quenched and tempered H13 steel substrate by using chromium plating and gas nitriding at 540 ℃. Then the abrasion resistance test was performed and the microstructure and wear resistance of H13 steel specimens after conventional gas nitriding and ion nitriding at the same temperature were compared. The results show that the main wear mechanisms of the specimens after three different heat treatment are adhesion wear and abrasive wear. The chromium plated and gas nitrided specimens show the lowest average friction coefficient, 0.44, and the wear resistance is the best, but the adhesion between the Cr-plated+gas nitriding layer and the substrate is the worst.
    Effect of isothermal oxidation on luminescent property and microstructure of YSZ∶Eu thermal barrier coating
    Liu Yankuan, Yang Liping, Wang Zhiping
    2020, 45(5):  12-16.  doi:10.13251/j.issn.0254-6051.2020.05.003
    Abstract ( 65 )   PDF (590KB) ( 22 )  
    Three different types of coatings were deposited by pure YSZ powders and 2mol% Eu3+ doped powders. The luminescent properties of the coatings were tested by using a laser spectrometer after isothermal oxidation treatment at 1100 ℃ for 100, 300, 800 h respectively, the morphologies of the three different types of coatings were analyzed by scanning electron microscope (SEM), and the element analysis of the coatings was studied by energy dispersive spectrometer (EDS). The results show that the fluorescence intensities of the YSZ∶Eu coatings decrease with the increase of the isothermal oxidation treatment time, and the as-received specimen without heat treatment has the highest fluorescence intensity. The YSZ∶Eu emission spectrum mainly consists of two emission peaks at 502 nm and 606 nm, and the emission peak at 606 nm is stronger than that at 592 nm. Under the same heat treatment conditions, the fluorescence intensity of the YSZ∶Eu coating is proportional to the content of Eu3+. The porosity ratio of the three coatings is 8.41%, 8.48% and 8.37%, respectively. The Vickers hardness of the coatings is between 430 and 440 HV0.3, indicating that the doping of 2mol% of Eu3+ ions cannot cause any influence on the density and the hardness of the YSZ coatings. And the Eu3+ ions do not diffuse inside the coating even after isothermal oxidation treatment at 1100 ℃ for 800 h.
    Structure analysis on stress rupture notch sensitivity for GH2909 alloy forgings
    Li Zhao, Wang Tao, Xu Xiong, Luo Junpeng, Sheng Junying
    2020, 45(5):  17-22.  doi:10.13251/j.issn.0254-6051.2020.05.004
    Abstract ( 56 )   PDF (589KB) ( 21 )  
    Structure analysis on stress rupture specimens were conducted by the means of metallographic and SEM methods, to define the problem of different level notch sensitivity for GH2909 alloy forgings. The results show that whether the alloy exhibits persistent notch sensitivity is a probabilistic event to the GH2909 alloy with a particular phase distribution. The occurrence probability of notch sensitivity increases apparently when the Laves phase precipitates in film-like shape on grain boundary.
    Microstructure evolution of 6063 aluminum alloy during double-pass hot deformation
    Wang Guan, Tian Changling, Kou Linyuan, Bian Dongwei
    2020, 45(5):  23-28.  doi:10.13251/j.issn.0254-6051.2020.05.005
    Abstract ( 61 )   PDF (589KB) ( 26 )  
    Double-pass hot rolling test on 6063 aluminum alloy was carried out by using Gleeble-1500 thermal simulator. Flow stress and microstructure of the alloy when the deformation temperature was 300-500 ℃, the strain rate was 0.001-0.1 s-1 and the residence time between passes was 10-90 s were analyzed. The results show that the yield stress of the second pass decreases with the increase of the residence time between passes, and the static softening rate of the alloy is affected by the temperature and the residence time between passes. There is more strengthening phase in the double-pass hot rolled alloy under the condition of low temperature, high strain rate and short residence time between passes, which morphology is mainly strip and round, however, when under the condition of high temperature, low strain rate and long residence time between passes, the content of the strengthening phase decreases and its morphology is mainly round. Besides, the strengthening phase in the alloy is mainly AlFeSi phase, and the strip-like phase has a length of about 6 μm and the round phase has a size of about 2 μm.
    Microstructure and damping property of as-cast Mg-xSn-1Mn alloy
    Feng Xuhui, Sun Youping, He Jiangmei
    2020, 45(5):  29-33.  doi:10.13251/j.issn.0254-6051.2020.05.006
    Abstract ( 63 )   PDF (593KB) ( 22 )  
    Effect of Sn content on the microstructure, damping properties and mechanical properties of Mg-xSn-1Mn alloy were studied by optical metallographic microscope (OM), Vickers hardness tester, thermal dynamic analyzer, X-ray diffraction (XRD) and multifunctional internal consumption meter. The results show that with the Sn content increasing from 2% to 8%, the dendrite clearance of the Mg-xSn-1Mn alloy shows the tendency of refining, and the hardness increases from 43.84 HV0.1 to 54.00 HV0.1 with tendency of monotonic increasing. The strain independent damping increases first then decreases with the increase of Sn content, and reaches the maximum when the Sn content is 4%. The strain dependent damping decreases with the increase of Sn content. At low temperature, the damping of the alloy with the same Sn content increases as the frequency increases, but at high temperatures, the rise of damping at low frequency is faster than that at high frequency. With the increase of temperatures, the low-frequency damping and the high-frequency damping tend to be equal. When the Sn content is different, with the increase of temperature, the damping value of the alloy with higher Sn content increases faster.
    Precipitation behaviors of second phase in toxic stainless steel shielding material
    Zhao Yong, Liu Yunming, Gu Mingfei, Pan Qianfu, Zhang Hongzhi, Qiang Rui, Wang Luquan
    2020, 45(5):  34-39.  doi:10.13251/j.issn.0254-6051.2020.05.007
    Abstract ( 53 )   PDF (590KB) ( 40 )  
    Precipitation behaviors of the second phase of toxic stainless steel was carried out by means of optical microscope (OM), scanning electron microscope (SEM) and X-ray diffraction (XRD), and the influence mechanism of the second phase precipitation on the stability of the matrix and rolling cracking was also analyzed. The results show that the second phase in the tested stainless steel is mainly Gd-Ni system, and its amount increases with the increase of Gd content. When the mass fraction of Gd increases from 1.87% to 7.87%, the area fraction of the second phase increases from 5.5% to 20.3%. Then, the precipitation of the second phase destroys the stability of the matrix structure. With the increase of Gd content, the matrix structure undergoes the transformation from single-phase austenite to austenite plus ferrite, and finally to single-phase ferrite. The precipitation of the second phase reduces the plasticity of the stainless steel and promotes the initiation and development of rolling cracks.
    Elimination of Al2CuMg phase during homogenization in Al-8.0Zn-2.0Mg-2.1Cu alloy
    Zhu Pengcheng, Jiang Lijun, Xiang Kangning, Huang Jie, Yao Dan, Yu Xinxiang
    2020, 45(5):  40-44.  doi:10.13251/j.issn.0254-6051.2020.05.008
    Abstract ( 55 )   PDF (591KB) ( 21 )  
    The formation of the insoluble phase Al2CuMg in a highly alloyed Al-8.0Zn-2.0Mg-2.1Cu (wt%) alloy during homogenization and the process of its full dissolution were studied by means of OM、SEM、EPMA、XRD and DSC. The results show that the main non-equilibrium solidification phase in as-cast alloy is Mg (Zn, Al, Cu)2 phase, and the elements of Zn, Mg and Cu are segregated seriously. After primary homogenization of heating at 470 ℃ for 40 h, although Mg (Zn, Al, Cu)2 phase gradually is dissolved back into the matrix and promotes the elimination of dendritic network in the alloy, a harmful phase Al2CuMg with high temperature stablity is formed in the alloy. Furthermore, the high temperature homogenization process of heating at 485 ℃ for 14 h is used to realize the full dissolution of the high temperature stable phase Al2CuMg. The proper homogenization processing is heating at 470 ℃ for 40 h and 485 ℃ for 14 h, which is consistent with the results of homogenizing kinetic analysis.
    Microstructure transformation of rapidly solidified high-silicon aluminum alloy during heating process
    Wu Xiaoping, Nie Junhui
    2020, 45(5):  45-50.  doi:10.13251/j.issn.0254-6051.2020.05.009
    Abstract ( 56 )   PDF (589KB) ( 25 )  
    The rapidly solidified powders of a high-silicon aluminum alloy were manufactured by gas atomization process. The microstructure and structural characteristics of the alloy with different powder size as well as the transformation of needle iron-rich phase and the coarsening behavior of β-Si phase were investigated by means of OM, SEM and so on. The results show that the microstructure of the rapidly solidified alloy is mainly characterized by a large number of fine granular and needle-like phases distributed in the matrix. During the heating process, with the increase of temperature and holding time, granular β-Si phase becomes coarser, the needle-like metastable non-equilibrium iron-rich phase changes into stable clubbed or granular phase gradually. The results of simulated stepped heating experiments show that microstructures with the needle-like phase almost disappeared and with the granular β-Si phase not obviously coarsened can be obtained.
    PROCESS RESEARCH
    Effect of recrystallization annealing temperature on corrosion resistance of copper-bearing ferritic antibacterial stainless steel
    Liu Yifei, Lu Hui, Sun Shaoheng, Zhao Aimin
    2020, 45(5):  51-55.  doi:10.13251/j.issn.0254-6051.2020.05.010
    Abstract ( 54 )   PDF (587KB) ( 29 )  
    Effects of recrystallization annealing temperature on corrosion resistance of copper-bearing ferritic antibacterial stainless steel were studied by means of microstructure analysis, pitting corrosion test, pitting morphology observation and dynamic potential polarization curve test. The results show that the recrystallization degree of copper-containing ferritic antibacterial stainless steel is gradually increased after holding for 5 min at 860-980 ℃, and the corrosion resistance first increases and then weakens. The optimum recrystallization annealing temperature is 900 ℃. The pitting pits of the copper-containing ferritic antibacterial stainless steel are open-type in the acidic FeCl3 solution, and the pitting pit area and the depth decrease with the increase of recrystallization annealing temperature. The number of pitting pits increases obviously after annealing at 980 ℃.
    Effect of solution cooling method on microstructure and mechanical properties of 17-4PH steel
    Sun Yongwei, Fan Fangxiong, Wang Lingshui
    2020, 45(5):  56-61.  doi:10.13251/j.issn.0254-6051.2020.05.011
    Abstract ( 65 )   PDF (585KB) ( 40 )  
    The influence of cooling method on microstructure evolution, strengthening phase and mechanical properties of the 17-4PH steel was investigated by means of OM, TEM and XRD test. The precipitation law of Cu phase under different cooling methods and its effect on strengthening mechanism of the 17-4PH steel were also discussed systematically. The results show that the average sizes of the Cu precipitated phase under different cooling methods are in the range between 10-20 nm. The yield strength of the steel increases with the increase of cooling rates while the ductility has a little change. And the impact absorbed energy of the 17-4PH steel decreases with the increase of cooling rates. The yield ratio has a lowest value under the condition of furnace cooling. The strengthening mechanism of the 17-4PH steel is mainly phase transformation strengthening, precipitation strengthening and grain boundary strengthening, and the precipitation strengthening is mainly based on the dislocation cutting mechanism.
    Effect of solution treatment on electrical properties and yield strength of Ni-Cr-Al-Fe alloy
    Yu Wenxin, Wang Yong, Yang Xianjun, Xu Yonghong, Wu Da, Wang Fenghong
    2020, 45(5):  62-68.  doi:10.13251/j.issn.0254-6051.2020.05.012
    Abstract ( 165 )   PDF (603KB) ( 21 )  
    The effects of solution temperature and time on the grain size, resistivity, TCR and yield strength of the precision resistance alloy wire were examined. Also, the properties of as-quenched and as-aged alloys were compared. The results show that the resistivity increases with the increase of solution temperature and holding time, while the TCR decreases. Both the variations are useful to improve the electrical properties of the alloy. The activation energy of grain boundary migration is 674.25 kJ/mol, and the comprehensive dynamic equation of grain growth is as follow: D-3.3t=3.80×1030texp-8.11×104T. The relationship between yield strength and grain size of this alloy is deduced to be Rp0.2=341.19+354.64D-0.5t. After solid solution at 950 ℃ for 7.5 min and aging at 430 ℃ for 0.5 h, the yield strength, resistivity and TCR are 445 MPa, 132.2 μΩ·cm and 2.2 × 10-6-1, respectively. And thus the alloy is suitable to be used as precision resistance component.
    Converter test of aging treatment based on DD5 single crystal superalloy parts
    Kong Lingli, Zhang Shanqing, Cheng Yifei, Luo Bingwei
    2020, 45(5):  69-73.  doi:10.13251/j.issn.0254-6051.2020.05.013
    Abstract ( 61 )   PDF (585KB) ( 28 )  
    In order to verify whether the aging treatment process of DD5 single crystal superalloy parts could meet the heat treatment technology requirements after converting to a newly introduced domestic vacuum furnace and at the same time to confirm the difference by comparing with the aging treatment in the imported vacuum furnace, the aging treatment process furnace convertering test was carried out. After the aeroengine turbine blades and tested rods of DD5 single crystal superalloy were aged in the newly introduced domestic vacuum furnace and the imported vacuum furnace respectively, the macrostructure of the blade, the poor chromium layer on the surface, and the tensile properties of the tested bar at high temperature were tested and analyzed. The results show that the parameters control capability of the domestic vacuum furnace is equal to that of the imported vacuum furnace at aging treatment stage, which can meet the requirements of aging treatment for DD5 single crystal alloy parts and replace the imported vacuum furnace to finish the aging treatment.
    Effect of solution process on microstructure and tensile properties of 6061 aluminum alloy
    Ma Dongwei, Zhang Chun, Zhang Yuanhao, Li Wenke
    2020, 45(5):  74-77.  doi:10.13251/j.issn.0254-6051.2020.05.014
    Abstract ( 71 )   PDF (590KB) ( 40 )  
    Effect of solution process on microstructure and mechanical properties of 6061 aluminum alloy was investigated by means of OM, SEM and tensile test. The results show that the soluble second phase particles gradually dissolve, recrystallization is enhanced, both grain refinement and tensile properties of the alloy increase with the increase of solution time and solution temperature, and with further increase of solution time and solution temperature, the grain begins to coarsen and the strength of the alloy decreases. The amount of residual coarse secondary particles and the grain size of the alloy are the main factors which affect the tensile properties and fracture morphology of the alloy. Under the condition of aging at 180 ℃ for 8 h, the optimum solution process of the 6061 aluminum alloy is at 535 ℃ for 80 min.
    Hot compression deformation characteristics of Al-12Si alloy doped with amorphous Fe powder
    Yang Hao, Wang Yuan, Wang Xiuchang
    2020, 45(5):  78-83.  doi:10.13251/j.issn.0254-6051.2020.05.015
    Abstract ( 50 )   PDF (595KB) ( 20 )  
    To improve the hot deformation resistance of Al-12Si alloy and to explore the effect of amorphous Fe powder doping on the hot compression behavior of Al-12Si alloy and the crystallization temperature of doped amorphous Fe powder in hot compression, the Al-12Si alloy specimens without and with doping of 10wt% amorphous Fe powder were prepared by continuous extrusion. The hot-pressing tests at different temperatures and strain rates were carried out to analyze the microstructure transformation of the specimens in hot-pressing, and the heat flux stress equation of the specimen was constructed by hyperbolic sinusoidal relation. The results show that Fe maintains amorphous when the doped alloy specimens are subjected to hot compression at 450 ℃ and below, while the crystallization is occurred at 500 ℃. The hot deformation resistance of the Al-12Si alloy is improved by doping 10wt% amorphous Fe powder, and its hot compression activation energy Q is 211.29 kJ/mol, which is 40.78 kJ/mol higher than that of the undoped alloy. Dynamic recovery and dynamic recrystallization occur during the hot compression. The heat flow stress equation of the doped alloy is constructed by hyperbolic sinusoidal relationship: ε·=4.42×1014[sinh(0.016 6σ)]6.13exp(-211 290/RT), with a linear regression coefficient of 0.99. It can provide some theoretical guidance for the hot working of amorphous Fe powder doped specimens.
    Effect of Q&P process on microstructure and properties of Fe-0.45C-1.6B high-boron steel
    Li Mingwei, Wu Run, Wang Kai, Zeng Songsheng
    2020, 45(5):  84-89.  doi:10.13251/j.issn.0254-6051.2020.05.016
    Abstract ( 55 )   PDF (586KB) ( 20 )  
    The microstructure and properties of Fe-0.45C-1.6B high-boron steel as-cast and after quenching and partitioning (Q&P) were analyzed by means of Thermo-Calc, OM, SEM, XRD, Rockwell hardness test and impact wear test. The results show that the as-cast microstructure of the high-boron steel is composed of a ferrite+martensite+retained austenite complex matrix and eutectic borides. Isothermal martensite transformation occurs below the Ms point in the Q&P process, the retained austenite in the matrix increases with the increase of quenching time, and reaches the limit when the quenching time is 120 s. While the retained austenite increases also with the increase of partitioning time, and reaches the maximum when the partitioning time is 80 s. However, more retained austenite causes the matrix too soft to support the boride, the wear resistance of the steel decreases.
    Effect of plasma electrolytic oxidation on mould corrosion resistance of aluminum alloy
    Wang Xiaobo, Yang Guohua, Quan Fengmei, Fa Tao, Zhu Shengfa
    2020, 45(5):  90-96.  doi:10.13251/j.issn.0254-6051.2020.05.017
    Abstract ( 52 )   PDF (590KB) ( 20 )  
    Plasma electrolytic oxidation (PEO) coatings were fabricated on the 2A12 aluminum alloy and mould corrosion resistance of the PEO coating was tested. SEM and XRD were employed to analyze the morphology, composition and phase component of the coatings. The results show that the mould growth behavior is observed on the surface of aluminum alloy under mould condition. Pitting corrosion occurs on the metal surface and the corrosion degree is grade I, while no mould growth behavior is observed on the PEO coating surface and the corrosion degree is grade 0. PEO treatment can improve the mould corrosion resistance of the aluminum alloy and expand their application.
    Thermal stress comparison of 304LN steel with weld joint at different cooling rates
    Li Yang, Huang Zhonghua, Shen Zihao
    2020, 45(5):  97-102.  doi:10.13251/j.issn.0254-6051.2020.05.018
    Abstract ( 77 )   PDF (586KB) ( 23 )  
    In order to explore whether the cooling rate had adverse effects on the thermal stress of the 304LN steel when it was cryogenic treated, 304LN specimens with welded joints was used to calibrate the base metal zone, weld zone and heat affected zone, respectively with the cooling treatment of 2 ℃/min, 5 ℃/min and direct liquid nitrogen immersion, and the rationality of the test results was verified by the finite element theory. The results show that with the decrease of temperatures, the perceived temperature of the upper and lower surfaces of the steel plate is different, and the temperature at the edge of the specimen is lower than that in the center, but the temperature difference is small. In the process of continuous cooling, the temperature stress of the specimen increases with the increase of cooling rates. According to the thermal stress-temperature curves, it is found that they have a nonlinear relationship. The precipitates are more uniform and stable at cooling rate of 5 ℃/min. Therefore, it can be concluded that there is little difference between the first two kinds of rates of cooling in general cryogenic processing, while 5 ℃/min is recommended based on the results of the practical mechanical properties testing and related processes.
    Retained austenite and carbide in 55SiCr spring steel
    Lu Hui, Chen Yinli, Wei He, Liu Zesheng
    2020, 45(5):  103-109.  doi:10.13251/j.issn.0254-6051.2020.05.019
    Abstract ( 94 )   PDF (588KB) ( 30 )  
    The microstructure and phase transition point of the spring steel 55SiCr, the microstructure evolution of retained austenite and carbide during heat treatment were studied by means of scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), transmission electron microscopy (TEM), X-ray diffractometry (XRD), thermal expansion, and Rockwell hardness tester. The results show that the retained austenite of 55SiCr spring steel is distributed in blocks on the substrate after quenching. As the tempering temperature increases, the retained austenite is reduced and distributed in a granular and film form. Carbon is enriched in retained austenite, which enhances its stability. Since Si suppresses the precipitation of carbides, the stability of retained austenite is improved. Si delays the precipitation of cementite when tempered at low temperature. When the steel is tempered at high temperature, the diffusion of carbon atoms is increased, and the precipitation of cementite is promoted to cause volume shrinkage. Carbon has enough time to diffuse, which promotes the formation of cementite and advances the formation temperature of cementite when tempered at low heating rate. Carbon does not have enough time to diffuse and inhibits the precipitation of cementite when tempered at high heating rate. When the tempering heating rate is the same, the hardness of the tested steel decreases as the tempering temperature increases. The hardness value is 51 HRC when the tempering temperature is 400 ℃ and the hardness value is 37 HRC when the tempering temperature is 650 ℃. The hardness value is 33 HRC when the heating rate is 0.1 ℃/s and the hardness value is 40 HRC when the heating rate is 200 ℃/s.
    Effect of double annealing process on mechanical properties and fracture morphology of TC21 titanium alloy
    Hu Shengshuang, Meng Xiaochuan, Wang Qing, Li Binbo, Liang Xiao, Wang Wenbo
    2020, 45(5):  110-114.  doi:10.13251/j.issn.0254-6051.2020.05.020
    Abstract ( 55 )   PDF (594KB) ( 26 )  
    The effect of double annealing on the microstructure and mechanical properties of TC21 titanium alloy was studied by means of OM, SEM, tensile test, impact test, and fracture toughness test. The results show that when the first annealing temperature keeps constant, the bulk α phase is easier to form with the increase of the second annealing temperature. When the second annealing temperature keeps constant, the probability of forming bulk α phase decreases with the increase of the first annealing temperature. The reduction of area of the TC21 alloy is the most sensitive to different double annealing processes. The specimens fabricated under double annealing process of 900 ℃×2 h+500 ℃×4 h have bent large stripe α phase and have the maximum impact absorbed. The specimens fabricated under double annealing process of 950 ℃×2 h+590 ℃×4 h can absorb the most energy during crack propagation and have the highest fracture toughness.
    Effect of continuous cooling rate on phase transformation and microstructure of 15B36-M track steel for excavator
    Zhang Qun, Wang Deyong, Kan Kai
    2020, 45(5):  115-118.  doi:10.13251/j.issn.0254-6051.2020.05.021
    Abstract ( 49 )   PDF (642KB) ( 19 )  
    Effect of different cooling rates on the phase transformation and microstructure of 15B36-M track steel for excavator was studied by thermal simulation test, and the specimens were cooled at the different cooling rates of 0.5, 1, 2, 5, 8, 10, 15, 20, 25, 30, 35 and 40 ℃·s-1. The results show that at different cooling rates, the thermal expansion curve of the 15B36-M steel has different microstructure transformation temperatures. The CCT curve can be used to guide the rolling process of the 15B36-M steel to obtain required microstructures.
    Regulation of residual stress of carbon steel parts by electropulsing treatment and tempering
    Pan Long, Chu Bin, Wang Baosheng, Xu Zhenqin
    2020, 45(5):  119-122.  doi:10.13251/j.issn.0254-6051.2020.05.022
    Abstract ( 62 )   PDF (589KB) ( 19 )  
    To optimize the residual stress controlled process, the effects of electropulsing treatment and tempering on quenched residual stress of the 45 carbon steel were studied. The voltage to generate electro pulse was 2120 V, and the capacitance was 400 μF. The results show that the release rates of quenched residual stress by electropulsing treatment, 600 ℃ tempering and 200 ℃ tempering are about 50%, 80% and 40% respectively, and the effective time is 30, 20 and 120 min respectively. Furthermore, the parts after electropulsing treatment and 200 ℃ tempering have high hardness about 51 HRC and the quenched martensite microstructure is remained, but the parts after 600 ℃ tempering have low hardness, 23 HRC and the microstructure changes greatly.
    Effect of temperature on microstructure and high temperature mechanical properties of low carbon steel
    Cui Guibin, Ju Xinhua, Zhang Qingshui, Yang Rui
    2020, 45(5):  123-128.  doi:10.13251/j.issn.0254-6051.2020.05.023
    Abstract ( 66 )   PDF (589KB) ( 31 )  
    The microstructure and high temperature mechanical properties of a low carbon steel at different temperatures were studied and discussed in detail by means of field emission scanning electron microscopy (FE-SEM), electron backscatter diffraction (EBSD) and electronic universal testing machine. The results show that regardless of room temperature tensile test or high temperature tensile test, carbide(Fe3C) particles located on grain boundaries are the main factor for inducing cracks for the tested low carbon steel. Compared with the tensile properties at room temperature, increasing the heating temperature, the tensile strength is significantly reduced and the elongation is significantly increased. At high temperatures, with the increase of temperature, the tensile strength decreases linearly, while the elongation decreases first and then stabilizes. A large number of slip bands are observed during the stretching at 520 ℃, which induces dynamic recovery. When the temperature is increased to 720 ℃, the pearlite structure becomes spheroidized, and the equiaxed small grains appear in the deformed ferrite grains, which means that dynamic recrystallization has occurred. According to the EBSD analysis, the misorientation between the deformed ferrite grains is large, and the misorientation between the equiaxed small grains where recrystallization occurs is small.
    Effect of tempering temperature on microstructure and mechanical properties of EA4T axle steel
    Ni Qixiao, Wang Zhanyong, Wang Zemin, Wang Binjun, Liu Min, Zhou Bing
    2020, 45(5):  129-132.  doi:10.13251/j.issn.0254-6051.2020.05.024
    Abstract ( 53 )   PDF (591KB) ( 24 )  
    EA4T axle steel was quenched and tempered at different tempering temperatures (500, 550, 600, and 650 ℃). The microstructure and mechanical properties of the material were tested and analyzed by means of OM, SEM, tensile test and impact test to study the effect of tempering temperature on microstructure and mechanical properties of the EA4T steel. The results show that as the tempering temperature increases, the sorbite structure is formed, which induces the decrease of strength and the increase of toughness and plasticity. The impact fracture morphology of the EA4T steel is dimpled when tempered at above 600 ℃. The empirical formula of tensile strength and hardness of the EA4T steel after tempering treatment is as follow: Rm =2.9477V+45.59.
    Effect of annealing temperature on microstructure and properties of marine Al-Mg-Mn-Cr alloy
    Zhu Xiyi, He Jianxian, Zhao Qizhong, Yang Hongchi, Wei Sunfei
    2020, 45(5):  133-137.  doi:10.13251/j.issn.0254-6051.2020.05.025
    Abstract ( 64 )   PDF (593KB) ( 22 )  
    Effect of different annealing temperature on the microstructure and properties of the actual pvoduction of 5AN6 aluminum alloy sheet was studied by means of mechanical properties test, optical microscope and corrosion property test. The results show that after annealing, the mechanical properties of the material continue to decline. After annealing at 280 ℃, the strength drops significantly. After annealing at 300-360 ℃, the mechanical properties tend to be stable. The grain structure in the original state is incomplete fiber structure, but the grain is obviously refined after annealing at 280 ℃. It can be considered that recrystallization occurs after annealing at 280 ℃. The temperature sensitive range of corrosion property of the 5AN6 alloy is 160-240 ℃, and the microstructure in this temperature range is continuous precipitation of β phase along the grain boundary.
    Effect of extrusion temperature on microstructure and properties of 2A12 aluminium alloy
    Wang Hongying, Peng Erbao
    2020, 45(5):  138-140.  doi:10.13251/j.issn.0254-6051.2020.05.026
    Abstract ( 50 )   PDF (589KB) ( 27 )  
    Effect of extrusion temperature on the microstructure and properties of the Al-Cu-Mg alloy 2A12 was studied by means of scanning electron microscopy (SEM), universal testing machine and Vickers hardness tester. The results show that after hot extrusion between 380-470 ℃, the primary second phase in the 2A12 alloy microstructure is crushed into island-like second phase, strip-like phase distributing along the extrusion direction, and small particle-like second phase is dispersed. With the increase of extrusion temperature, the granular second phase decreases gradually, the strength and hardness of the alloy increase gradually, but the elongation decreases gradually. The tensile strength, yield strength and hardness of the 2A12 alloy extruded at 470 ℃ are increased by 61.7%, 63.2% and 54.1%, respectively, which is higher than the homogenized 2A12 alloy.
    Effect of annealing process on microstructure and microhardness of magnesium alloy fabricated by friction stir processing
    Li Tianqi, Yin Chen, Yan Yuanyuan, Zhang Kuo, Wang Xi
    2020, 45(5):  141-146.  doi:10.13251/j.issn.0254-6051.2020.05.027
    Abstract ( 47 )   PDF (591KB) ( 20 )  
    Friction stir processing (FSP) technology was adopted to prepare AZ31 magnesium alloy. The microstructure evolution and microhardness of the FSP magnesium alloy during annealing was studied by varying annealing temperature and preserving time. The results show that the fine grained AZ31 magnesium alloy are successfully prepared by FSP, and the average grain size is refined by 54.9%. When the annealing temperature is between 200-300 ℃, the average grain size in the stirring zone (SZ) is rather stable, and the structure is homogenized and refined in different degrees. When the annealing temperature is higher than 300 ℃, in the SZ the grains grow rapidly by consuming each other. In the heat affected zone (HAZ), when the annealing temperature is low, the microstructural evolution is insignificant after short-time preservation, while long time preserving and high temperature makes the microstructure in the HAZ to be refined and homogenized rapidly. When the annealing temperature exceeds 300 ℃, the recrystallization will be completed in a short time, then the grains in the HAZ begin to grow again. Annealing at 300 ℃ for 60 min is the optimum annealing process, after which the microstructure in the SZ and the HAZ can be refined by 10.9% and 35.6%, respectively.
    Effect of homogenizing treatment on microstructure and mechanical properties of Mg-Nd-Zn-Zr alloy
    Su Zaijun, Zhu Wen, Yang Shuzhong, Luo Linshan
    2020, 45(5):  147-151.  doi:10.13251/j.issn.0254-6051.2020.05.028
    Abstract ( 48 )   PDF (590KB) ( 19 )  
    Effect of homogenizing treatment on the microstructures and mechanical properties of Mg-2.3Nd-0.5Zn-0.5Zr alloy was investigated by optical microscopy(OM), differential thermal analysis(DTA), X-ray diffractometry(XRD), scanning electron microscopy(SEM) and tensile test. The results show that the as-cast alloy is composed mainly of α-Mg, strip-like Mg12Nd phase and petaloid Zn-Zr phase. After homogenizing treatment, the strip-like Mg12Nd phase gradually dissolves into the matrix, while there are also partial petaloid Zn-Zr phase within the grains. The best homogenizing treatment for the alloy is 505 ℃×6 h, which leads the secondary phase at grain boundary to dissolve into the matrix so that the elongation of the alloy increases by 100%, and the fracture mode of the alloy changes from the brittle cleavage fracture in as-cast state to the ductile transgranular fracture. However, such a process causes weakening of both the secondary phase strengthening and the grain refinement strengthening so that offsets the solid solution strengthening, which result in that the tensile strength and yield strength of the alloy increase slightly.
    Effect of heat treatment on microstructure and mechanical properties of extruded Al-Zn-Mg-Cu alloy
    Wei Di, Yang Li, Zhang Yaocheng, Lu Wangzhang, Pang Song, Zhi Yating
    2020, 45(5):  152-156.  doi:10.13251/j.issn.0254-6051.2020.05.029
    Abstract ( 53 )   PDF (594KB) ( 23 )  
    The microstructure evolution and mechanical properties of Al-12Zn-2.4Mg-1.1Cu-0.3Zr-0.15Ni-0.12Mn (mass fraction, %) alloy under three different heat treatments were investigated by means of scanning microscope, hardness test, tensile test, and impact test. The results show that the microstructure of T6-treated alloy consists of α-Al matrix, η′ and η precipitation phases. The average microhardness and tensile strength of T6-treated alloy reach 210 HV and 597 MPa respectively, which are superior to that of T4-treated and T5-treatd alloy. The elongation of T6-treated alloy is slightly lower than that of T4-treated alloy because η′ and η precipitation phases have a certain mobility relative to the matrix which reduces the plasticity of the alloy. The impact fracture mechanism of T4-treated and T5-treatd alloy is brittle fracture. The impact property of T6-treated alloy is obviously improved and the fracture mechanism is ductile-brittle mixed fracture. T6 heat treatment should be adopted to the extruded Al-Zn-Mg-Cu alloy.
    Measurement of SH-CCT curves of TC4-DT titanium alloy
    Zhao Dong, Dong Wenchao, Jiao Qingyang, Quan Chunyi, Lu Shanping
    2020, 45(5):  157-160.  doi:10.13251/j.issn.0254-6051.2020.05.030
    Abstract ( 60 )   PDF (599KB) ( 21 )  
    The transformation temperature Tβ of TC4-DT titanium alloy was measured by metallographic method, and verified by thermal expansion method. According to the expansion curves at different cooling rates, the SH-CCT curves of the TC4-DT titanium alloy were plotted by means of metallographic analysis and hardness test. The results show that the transformation temperature of the TC4-DT titanium alloy is (945±5) ℃. When the cooling rate is less than 10 ℃/s, the α phase transformed from β phase is clustered with different orientations, and the net basket-like α phase appears. The microstructure is composed of martensite α phase and massive αm phase when the cooling rate is greater than 10 ℃/s. As the cooling rate exceeds 100 ℃/s, the martensite α′ phase is formed. The start temperature and the finish temperature of martensite transformation in the TC4-DT titanium alloy are 836 ℃ and 760 ℃, respectively.
    Influence of laser quenching on structure and property of EA4T axle steel for high-speed EMU
    Pan Xuexin, Chang Hong, Li Zhongwen, Hu Xiaofeng, Fu Hong, Jiang Haichang
    2020, 45(5):  161-165.  doi:10.13251/j.issn.0254-6051.2020.05.031
    Abstract ( 47 )   PDF (653KB) ( 30 )  
    In order to improve the surface hardness and wear resistance of the EA4T axle steel in quenched and tempered state, the surface of the axle was modified by laser quenching. The microstructure, phase transition depth and hardness of the laser quenched layer were characterized by scanning electron microscopy, microhardness tester and nano indentation meter. The results show that when the EA4T axle surface is subjected to different laser quenching processes, the quenched structure in the phase transition layer is mainly composed of fine lath martensite and granular bainite, and the depth varies from 100 μm to 800 μm according to the process. There is a tendency that the depth of the phase change layer gradually increases as the laser quenching power increases and the scanning speed decreases. The microhardness of the quenched phase transition layer is basically maintained at about 450 HV0.2, which is approximately twice the hardness of the matrix, so that the wear resistance of the axle steel is remarkably improved. Due to the overlapping between the quenching passes, the laser quenched layer exhibits a waveform distribution. The martensite content in the valley region is higher than that of the peak region, so that the hardness in the valley region is significantly higher than that of the peak region.
    Hardenability of 7A04 Al alloy super thick plate
    Chen Yuanqing, He Kezhun, Yao Xiang, Wei Xiuxun, Zhang Hang, Chen Shaowen
    2020, 45(5):  166-171.  doi:10.13251/j.issn.0254-6051.2020.05.032
    Abstract ( 61 )   PDF (596KB) ( 29 )  
    The microstructure, properties and hardenability of the 7A04 Al alloy super thick plate were studied by means of universal mechanical testing machine, optical microscope and scanning electron microscope. The results show that when the 225 mm thick 7A04 Al alloy hot rolled plate is solid solution treated at 475 ℃ for 340 min with water quenching, then artificially aged at 120 ℃ for 24 h, the surface mechanical properties of the plate are the optimum, with the tensile strength, yield strength, and elongation being 584 MPa, 500 MPa, and 11%, respectively. However, the T/4 thickness layer gets the poorest property combination, with the tensile strength, yield strength, and elongation being 396 MPa, 257 MPa, and 11%, that is, the tensile strength and yield strength differ from that of the surface by 32% and 49%, respectively. The one-side quenching depth is 32 mm. By adjusting the chemical composition, increasing rolling reduction and increasing quenching cooling rate, the differences of mechanical properties between the plate surface and center can be improved, so is the hardenability.
    Effect of quenching temperature on microstructure and mechanical properties of medium manganese QP steel
    Wang Yating, Wan Decheng, Feng Shuming, Li Jie
    2020, 45(5):  172-175.  doi:10.13251/j.issn.0254-6051.2020.05.033
    Abstract ( 60 )   PDF (587KB) ( 19 )  
    Effect of different quenching temperature on microstructure and mechanical properties of medium manganese steel was studied by means of partial austenitization-quenching-partition process. The results show that with the increase of quenching temperature, the elongation of the tested steel increases first and then decreases, while the tensile strength decreases gradually. When the quenching temperature is 140 ℃, the total volume fraction of primary martensite and fresh martensite in the tested steel is the largest, so the tensile strength is the highest. The tested steel has the largest volume fraction of retained austenite and the highest elongation when the quenching temperature is 180 ℃, the comprehensive mechanical properties are the best and the product of tensile strength and plasticity is up to 30 328.2 MPa·% particularly. When the quenching temperature is increased to 200 ℃, the elongation and tensile strength of the tested steel decrease because of the decrease of retained austenite content and the hardness of fresh martensite.
    Pockmarks on ground surface of nitrided 2Cr13 steel
    Zhao Mingpeng, You Pingping, Liu Minghu
    2020, 45(5):  176-179.  doi:10.13251/j.issn.0254-6051.2020.05.034
    Abstract ( 71 )   PDF (595KB) ( 22 )  
    Many pockmarks were detected on the inner hole surface after grinding of a nitrided bearing housing made of stainless steel 2Cr13. The pockmarks were a lot of small area of exfoliation, as big as a needle, and could be seen by the naked eye. By analyzing the possible influencing factors such as materials, brittleness, stress and process, it is determined that the pockmark failure is caused by perchloroethylene added in nitriding process.
    Effect of annealing process on microstructure of deformed high purity ytterbium
    Deng Yuehua, Wang Zhijian, Liu Hua, Liu Wei, Huang Meisong, Zhang Wenyang, Huang Pei
    2020, 45(5):  180-182.  doi:10.13251/j.issn.0254-6051.2020.05.035
    Abstract ( 53 )   PDF (592KB) ( 18 )  
    99.99% high purity ytterbium was rolled by multipass rolling with total deformation of 35.6% at room temperature, and then was annealed at 240, 270, 300, 330, and 360 ℃, respectively. The effects of annealing process on the microstructure and microhardness of the deformed high purity ytterbium were analyzed. The results show that the optimum annealing process is at 270 ℃ for 0.5 h. After annealing at 270 ℃ for 0.5 h, the deformed high purity ytterbium is fully recrystallized and obtains uniform fine grains with the average grain size of about 22.5 μm, while the hardness decreases to 18.96 HV0.5. With the increase of annealing temperature, the average grain size increases, the microhardness decreases and tends to be stable.
    Preparation technology of Ni3Al thin film of intermetallic compounds
    Wang Ming, Ji Hong, Lu Shuo
    2020, 45(5):  183-186.  doi:10.13251/j.issn.0254-6051.2020.05.036
    Abstract ( 66 )   PDF (586KB) ( 19 )  
    By means of DC magnetron co-sputtering, a 500 nm thick Ni3Al thin film was prepared on the substrate of SiO2 by one-step method or two-step method. Test results of X-ray diffraction(XRD) and transmission electron microscopy(TEM) show that the (111) oriented intermetallic compound with polycrystalline structure in Ni3Al thin film prepared by one-step method is better than that by the two-step process. The morphology of Ni-Al alloy thin film and intermetallic compound Ni3Al thin film after high temperature oxidation was observed by means of metallographic microscope. The results show that the high temperature antioxidant properties of Ni3Al intermetallic compound films are obviously better than the Ni-Al alloy films.
    Effect of severe plastic deformation on microstructure and mechanical properties of 2519A aluminum alloy
    Ye Zhifei, Sun Daxiang, Zhou Peng, Kuang Hongcong, Xiao Yongtong
    2020, 45(5):  187-191.  doi:10.13251/j.issn.0254-6051.2020.05.037
    Abstract ( 58 )   PDF (590KB) ( 17 )  
    Microstructures and mechanical properties of 2519A aluminum alloy after different severe plastic deformation processes were investigated by means of hardness test, tensile test, and transmission electron microscopy (TEM). The results show that after 50% cold rolling reduction and artificial aging at 165 ℃, the tensile strength, yield strength and elongation of the 2519A alloy are 522 MPa, 468 MPa, 8.5%, respectively. And adding 165 ℃×2 h pre-aging before cold rolling, the mechanical properties are further improved, and the tensile strength, yield strength and elongation of the alloy are 535 MPa, 497 MPa, 8%, respectively. Pre-aging treatment can increase the density of θ′ precipitates in the 2519A alloy and make them more uniformly distributed, which is helpful to improve the mechanical properties of the alloy.
    NUMERICAL SIMULATION
    Effect of microparticle shot peening on residual stress field of target
    Wang Chao, Zhang Hai, Li Dongfei, Yun Hao, Xu Wensu, Zhao Wu
    2020, 45(5):  192-198.  doi:10.13251/j.issn.0254-6051.2020.05.038
    Abstract ( 55 )   PDF (596KB) ( 25 )  
    In order to study the residual stress field of the target caused by multi-particle impact of microparticle shot peening, a 7-particle impact model with 6 particles distributed around the center particle was established. The effect of shot peening parameters such as overlap rate, impact velocity, impact angle and particle size on the residual stress field at the center of the impact crater was simulated by finite element software. The results show that when the overlap rate ζ≤0.5, the change of ζ has no effect on the depth of residual compressive stress field, but ζ=0.75 is the boundary of surface residual compressive stress SS changing. Only when ζ>0.75, the four characteristic values of residual compressive stress field increase with the increase of overlap rate. Increased diameter and reduced impact angle are beneficial to increase the depth of residual compressive stress field, but also to reduce the residual compressive stress. The depth of residual compressive stress field increases with the increase of impact velocity, while the magnitude of residual compressive stress field fluctuates to a certain extent, but both of them reach the maximum when the impact velocity is 200 m/s.
    Numerical simulation of induction hardening of 50AT switch rail
    Cheng Yi, Xu Jinhui, Feng Qingsong, Zhang Bin, Zou Xiaokui, Liu Changyu
    2020, 45(5):  199-205.  doi:10.13251/j.issn.0254-6051.2020.05.039
    Abstract ( 58 )   PDF (591KB) ( 35 )  
    The strength, wear resistance and service life of switch rail can be improved by medium frequency induction hardening. After the rail head is hardened, there will be a large residual stress. Through the establishment of 50AT switch rail model and the simulation of hardening, the distribution of residual stress after hardening was obtained, and the stress results were compared and verified by the method of blind hole stress measurement. The results show that the residual stress in the middle part of the rail bottom is larger, and the residual stress in the tip part is smaller. The difference between the simulated stress and the measured stress is smaller by selecting the same measuring point at the rail bottom. The test results can be used to guide the elimination of residual stress after hardening of switch rail and the placement of vibration exciter during vibration aging.
    Numerical simulation and optimization of pressure quenching process of armor plate with specification of extremely thin and wide
    Zhang Sai, Li Xianjun, Luo Ping, Wu Xiaolin, Liu Junjie
    2020, 45(5):  206-209.  doi:10.13251/j.issn.0254-6051.2020.05.040
    Abstract ( 49 )   PDF (628KB) ( 22 )  
    Distortion of armor plate with the specification of extremely thin and wide in the process of quenching was studied by means of numerical simulation, and the parameters of pulse-pressure quenching were also optimized. Comparing the distortion amount of armor plate under different cooling conditions, the pulse-pressure and period were determined. The results show that under the simulation condition of pulse constraint, the final distortion amount of armor plate in the thickness direction Z is 1.7 mm, which is not only less than the normal requirements of 2 mm, but also can meet the actual production requirements of the armor plate surface without indentation, scratch and other damage under the premise of less quenching deformation.
    Effect of quenching residual stress on stress intensity factors and propagation trend of crack of aluminum alloy thick plate
    Luo Jiayuan, Jia Ersuo
    2020, 45(5):  210-214.  doi:10.13251/j.issn.0254-6051.2020.05.041
    Abstract ( 53 )   PDF (622KB) ( 24 )  
    In order to explore the influence law of quenching residual stress on the fatigue crack propagation of the aluminum alloy thick plate, a numerical simulation model of three-dimensional crack on 7075 aluminum alloy plate was developed. The method of sequentially coupled thermal-stress was used to solve the quenching residual stress field, and the residual stress field was taken as the initial load condition to solve the stress intensity factors of the crack, then compared it with the value of stress intensity factors without residual stress field. Under these two conditions, the distribution of stress intensity factors and their similarities and differences were studied. By analyzing the evolution curve of crack stress intensity factors along with the crack position angle under different uniform tensile stress loading in different crack radius with initial quenching residual stress, the influence law of the quenching residual stress on crack propagation trend was found out. The results show that the existence of quenching residual stress changes the distribution of stress intensity factors and crack propagation trend of the aluminum alloy thick plate, and the crack propagation near the surface is restrained by quenching residual stress.The crack tends to propagate preferentially in the thickness direction.
    Prediction on microstructure, hardness and process parameter optimization in continuous induction hardening of stepped shaft
    Gao Yu, Gao Xingwang, Zhang Genyuan
    2020, 45(5):  215-220.  doi:10.13251/j.issn.0254-6051.2020.05.042
    Abstract ( 59 )   PDF (633KB) ( 30 )  
    A physical model of continuous induction hardening process for S45C steel step shaft was established, which was reasonably divided into areas and loaded with corresponding physical properties and process parameters. The hardening depth distribution of the hardened layer was predicted using the radial- axis temperature distribution at the end of the heating phase, the Maynier model, the Carsi correction model and the steel CCT curve fitting. The parameters of continuous induction hardening process were optimized by jointly analyzing the simulation results of each method. The results show that the depths of 100%, 50% and 0% martensite in the induction hardened layer of the tested key point b are 1.31, 1.49 and 2.97 mm with errors of -12.67%, -13.87% and -1.00%, respectively, as well as the key point e are 1.44, 2.02 and 2.54 mm with errors of -4.00%, -3.38% and -18.06%, which are in good agreement with the test results. The quasi-optimized induction hardening process parameters were discussed by changing the induction hardening process parameter and adjusting the physical model. The effect of heat exchange coefficient h change on the induction hardening layer was preliminarily investigated.
    Finite element simulation of influence of hot stamping process parameters on properties of 22MnB5 martensitic steel for automobile B-pillar
    Wang Zhangzhong, Ba Zhixin, Li Qi, Liu Yonggang, Cui Lei, Liu Langfeng, Dong Jiwu
    2020, 45(5):  221-228.  doi:10.13251/j.issn.0254-6051.2020.05.043
    Abstract ( 62 )   PDF (685KB) ( 28 )  
    Influence of parameters on wrinkle, rebound, thinning, martensitic volume fraction and strength of 22MnB5 martensitic steel B-pillar during hot stamping process were studied by means of finite element analysis software Autoform. The results show that the optimum process parameters of hot stamping for 22MnB5 martensitic steel B-pillar are heating temperature of 930 ℃ and cooling rate of 80 ℃/s, with which, the martensite transformation of B-pillar is completed, its hardness distribution is uniform, the material thinning rate is low, the hot stamping forming effect is good, the size accuracy is high, and the strength of stamping workpieces is higher than 1400 MPa.
    REVIEW
    Research status and development prospect of steels for shovel teeth at home and abroad
    Zheng Lili, Peng Jun, An Shengli, Zhang Fang, Peng Jihua, Li Junping, Jiao Haidong
    2020, 45(5):  229-235.  doi:10.13251/j.issn.0254-6051.2020.05.044
    Abstract ( 52 )   PDF (625KB) ( 25 )  
    The classification of the shovel teeth was summarized. From the different microstructures of steels for shovel teeth, the development of steels for various types of shovel teeth had been described at home and abroad, including the specific chemical composition, heat treatment, comprehensive performance and existing problems, etc. The advantages and disadvantages of austenitic wear-resistant steel shovel teeth, martensite wear-resistant steel shovel teeth, bainite wear-resistant steel shovel teeth and composite phase shovel teeth were summarized, and the problems of steels for shovel teeth in China were summarized. It can be found that the steels of the bainite structure has a broad development space.
    Research prospects and effect of high magnetic field on martensite transformation of steel
    Wu Guanghui, Hou Tingping, Li Zihua, Hu Feng, Zhou Wen, Xin Rui, Wu Kaiming
    2020, 45(5):  236-242.  doi:10.13251/j.issn.0254-6051.2020.05.045
    Abstract ( 55 )   PDF (623KB) ( 24 )  
    The external magnetic field will change the phase transformation process from austenite to martensite, and influence the microstructure of martensite due to the magnetic difference of these phases. In this paper, the effect of high magnetic field on martensitic transformation is discussed. Related research shows show that magnetic field can increase the starting temperature of martensite transformation, which is mainly caused by the effects of magnetostatic energy, high field susceptibility and magnetostriction of magnetic field. The magnetic field boosts the transformation of martensite by promoting its nucleation and growth. However, the magnetic field has little effect on the morphology of martensite. At the same time, the latest progress and future prospects of martensite transformation under high magnetic field are introduced.
    SURFACE ENGINEERING
    Effect of laser scanning speed on microstructure and properties of Fe-based alloyed layer on ductile iron hot roller surface
    Wang Shuoyu, Zhao Yi, Xie Mingxiang, Ye Wenhu
    2020, 45(5):  243-249.  doi:10.13251/j.issn.0254-6051.2020.05.046
    Abstract ( 85 )   PDF (632KB) ( 39 )  
    Fe-based alloyed layers were prepared on the surface of ductile iron QT600-3 by laser alloying technology. The effect of laser scanning speed on the phase composition, microstructure, mechanical properties, tribological properties at high temperature of the alloyed layers were investigated by scanning electron microscope (SEM), X-ray diffraction (XRD), Raman spectrometer, microhardness tester, friction and wear tester. The results show that the Fe-based alloyed layers exhibit good metallurgical bonding to the substrate and high microhardness (up to 830 HV0.1). And the friction coefficient and wear rate at high temperature decrease to 0.28 and 2.41×10-6 g·N-1·m-1, respectively. The microstructures of the Fe-based alloyed layers are mainly composed of γ-phase dendrites and eutectic carbides, and are refined with the scanning speed increasing. With the increase of laser scanning speed, the thickness of the Fe-based alloyed layers decreases and the crack rate increases, while the microhardness increases first and then decreases, and the wear resistance at 700 ℃ increases. In the high temperature friction and wear test, the wear mechanism of the Fe-based alloyed layers is mainly abrasive wear, fatigue wear and oxidation wear.
    Al-based amorphous powder cold sprayed coating and its wear resistance
    Jia Li, Chen Jie, Cui Lang, Zhao Jian
    2020, 45(5):  250-252.  doi:10.13251/j.issn.0254-6051.2020.05.047
    Abstract ( 58 )   PDF (631KB) ( 22 )  
    In order to improve the wear resistance of magnesium alloy, the Al-based amorphous coating was deposited on the magnesium alloy substrate by cold spraying (CS). The microstructure was characterized by scanning electron microscope, and the amorphous content in sprayed powder and coating was analyzed by means of X-ray diffraction analysis. The wear resistance and wear mechanism were also studied by means of miniature controlled atmosphere friction and wear tester. The results show that the amorphous structure of the powder is retained after the cold spraying process and the content of amorphous structure in the coating is about 48%. The coating performs dense microstructure and the coating porosity is 0.59%. The wear loss and wear rate of the coating are lower than the magnesium alloy matrix, but the friction coefficient is higher than that of the substrate.
    TEST AND ANALYSIS
    Fracture failure analysis of tram pantograph spring
    Liu Yong, Wang Hui, Zhang Ting, Liu Haibo, Gong Hou, Xuan Yixun, Cui Zhemin
    2020, 45(5):  253-256.  doi:10.13251/j.issn.0254-6051.2020.05.048
    Abstract ( 77 )   PDF (750KB) ( 28 )  
    Fracture occurred on a spring of pantograph on the top of a tram during normal vehicle operation. In order to find the cause, the spring was analyzed by means of scanning electron microscope, energy spectrometer, optical microscope and direct reading spectrum analyzer for macroscopic observation, fracture scanning, metallographic examination and chemical composition. The hardness gradient test was also carried out. The results show that the fractured spring is subjected to tensile stress during service and exposed to corrosive medium in the service environment. According to that the stress condition and the medium condition are satisfied simultaneously, the failure mode of the spring is judged to be stress corrosion fracture.
    Fracture failure analysis on shaft of torque gauge in heavy duty vehicles
    Pan Shumin, Wang Xiaohai, Liu Guoqiang, Xiang Hongyan, Yu Dawei, Yu Qingfeng
    2020, 45(5):  257-261.  doi:10.13251/j.issn.0254-6051.2020.05.049
    Abstract ( 64 )   PDF (627KB) ( 30 )  
    To study the crucial reason of fracture of the shaft of torque gauge, chemical composition, fracture morphology, metallographic analysis and hardness were investigated and analyzed. The results show that the major factor of fracture of the shaft is abnormal microstructure. The coarse tempered martensite and the upper bainite which propagates from grain boundaries towards inside of grains bring about the initiation and propagation of crack, and form the morphology along the grain boundaries and quasi-cleavage fracture. The banded structure accelerates the heterogeneity of microstructure and hardness distribution, which results in anisotropism of material and weakens the service performance of the part. In addition, due to the tensile stress, the stress concentration effect at the root of the keyway is also a vital factor of the fracture of shaft.
    Causes analysis on anormal elongation of low-alloyed high strength steel
    Sun Xuejiao
    2020, 45(5):  262-265.  doi:10.13251/j.issn.0254-6051.2020.05.050
    Abstract ( 68 )   PDF (627KB) ( 25 )  
    In view of the phenomenon of lower elongation about low-alloyed high strength steel, the chemical composition analysis, microstructure observation, fracture analysis and inclusion composition of the samples of the unqualified product were carried out. The results show that the main cause is related to the abnormal structure due to segregation of manganese elements, which formes hydrogen trap and then lead to hydrogen embrittlement, forming hydrogen brittle facets on the tensile fracture.
    Wear analysis of high chromium cast iron used for umbrella hat in corrosion environment of hot strong alkali
    Huang Wei
    2020, 45(5):  266-271.  doi:10.13251/j.issn.0254-6051.2020.05.051
    Abstract ( 53 )   PDF (702KB) ( 25 )  
    Wear mechanism under working conditions of high chromium cast iron Cr28 and Cr20 conventionally used for umbrella hat in the alumina industry was analyzed. And the composition, microstructure and properties of the failed parts made of these materials were compared and studied. The results show that, when the umbrella hat are eroded under the condition of high temperature and strong alkali, the abrasion loss is decided collaboratively by the mechanism of micro-cutting and deformation abrasion. The high chromium cast iron Cr28 with the more content of Cr has better erosion and abrasion properties than that of Cr20 cast iron. The service life of umbrella hat is depended on the slurry and cast iron materials on its surface. After quenching and tempering, the matrix microstructure of the two tested materials is mainly composed by tempered martensite, M7C3 carbide and a small amount of retained austenite. And the contents of eutectic carbides in the high chromium cast iron Cr28 is higher and more dispersed distribution, the average hardness is 64.0 HRC, which is higher than that of 60.2 HRC of Cr20 cast iron. Finally, it is determined that the umbrella hat produced by high chromium cast iron Cr28 can meet the requirements of the alumina production and overhaul period of the equipment.