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  • PROCESS RESEARCH
    Effect of deformation temperature on high temperature tensile deformation behavior of GWZ1031K magnesium alloy
    Huang Yuanchun, Luo Xiaoyu, Liu Yu, Wang Xu, Wang Zhou
    2021, 46(1):  1-6.  doi:10.13251/j.issn.0254-6051.2021.01.001
    Abstract ( 301 )   PDF (657KB) ( 236 )  
    High temperature deformation behavior of GWZ1031K magnesium alloy was investigated by high temperature tensile test at 250-400 ℃ and the deformation rate of 0.2 mm/min.Scanning electron microscope (SEM) and X-ray energy spectroscopy (EDS) were used to observe the microstructure and tensile fracture.The results show that the peak value appears in all the high temperature tensile stress-strain curves at different temperatures,and the peak stress decreases with the increase of deformation temperature,meanwhile the plasticity increases sharply,particularly superplasticity occurs at 400 ℃.Combining the analyse of microstructure and fracture morphology,it can be concluded that the GWZ1031K magnesium alloy has good heat resistance in the temperature range from 250 ℃ to 350 ℃.
    Effect of solid solution temperature on microstructure and microhardness of 2205 duplex stainless steel
    Gao Xiaodan, Li Jingkun, Ren Xueping, Yan Qiang
    2021, 46(1):  7-10.  doi:10.13251/j.issn.0254-6051.2021.01.002
    Abstract ( 263 )   PDF (579KB) ( 160 )  
    Hot-rolled 2205 duplex stainless steel was taken as the raw material and solid-solution treated at 1000-1350 ℃ for 30 min.X-ray diffraction (XRD),optical microscope (OM),scanning electron microscope (SEM) and microhardness tester were employed to measure the microstructure and microhardness of the solution-treated 2205 duplex stainless steels.The results show that with the increase of solution treatment temperature,the fraction of ferrite increases and the fraction of austenite decreases,both the recrystallization and grain growth occur,the difference in content of each element including Cr,Mo,and Ni in the two phases is reduced.The ferrite and austenite content is basically equivalent when solution treated at 1050 ℃.The microhardness increases with the increase of solution treatment temperature,and it increases abruptly at 1150 ℃ to 1200 ℃.In order to obtain a lower hardness for subsequent cold processing,the solution treatment temperature of the 2205 duplex stainless steel should be controlled at 1000-1150 ℃.
    Effect of cryogenic treatment on wear property of YG10 cemented carbide
    Yan Xianguo, Yao Yongchao, Chen Zhi, Guo Hong, Li Fan, Hou Qiang
    2021, 46(1):  11-18.  doi:10.13251/j.issn.0254-6051.2021.01.003
    Abstract ( 155 )   PDF (582KB) ( 79 )  
    With YG10 cemented carbide as the research object and cryogenic treatment technology as the methods,the specimens were treated at different cryogenic temperature,cryogenic holding time and alternating times by orthogonal test,and the treated specimens were subjected to wear test,hardness test and microstructure analysis test.The results show that the microhardness is increased by 33.6%,the wear resistance is increased by 72.8% after the optimal cryogenic treatment,and the cryogenic temperature is the biggest factor affecting the wear resistance of YG10 cemented carbide.The reasons for this phenomenon are as follows:in terms of microstructure,the dispersive distribution of η phase and the density change of Co phase enhance the wear resistance of cemented carbide.
    Effect of vacuum annealing treatment on microstructure and properties of Al-based composites by cold spray process
    Wang Qiang, Zhai Le, Niu Wenjuan, Zhang Mingxing
    2021, 46(1):  19-27.  doi:10.13251/j.issn.0254-6051.2021.01.004
    Abstract ( 110 )   PDF (583KB) ( 51 )  
    The aluminum matrix composites contained Al2O3 particles with different volume content were prepared by cold spraying additive manufacturing process,which included the volume fraction of 25%,50%,and 75%,respectively(i.e.Al-25Al2O3,Al-50Al2O3,and Al-75Al2O3).The influence of vacuum annealing treatment on microstructure and mechanical properties of cold sprayed aluminum matrix composites was analyzed by means of SEM,EBSD,hardness test and tensile test.The results show that the addition of Al2O3 particles increases the strength and hardness of the cold spray additive material,which enhances with the increase of Al2O3 content.The reason for this is that the hammer action of Al2O3 particles in the process of cold sprayed leads to mechanical interlocks and grain refinement due to severe plastic deformation and dynamic recrystallization.However,the strength and hardness of the material gradually decrease after annealing treatment,as well as thegradual increase of elongation.The internal structure of the material gradually become uniform.
    Effect of heat treatment process on microstructure and properties of KD sucker rod steel
    Sun Xiaoran, Zheng Wenyue
    2021, 46(1):  28-31.  doi:10.13251/j.issn.0254-6051.2021.01.005
    Abstract ( 119 )   PDF (579KB) ( 64 )  
    Mechanical properties and microstructure of KD grade experimental steel used for sucker rod,after three different heat treatment processes,were studied by means of mechanical properties test,OM,SEM and TEM.The results show that the comprehensive mechanical properties of the material are the best when tempering temperature starts from room temperature.The impact property of the material obtained is worst when tempering temperature starts from 500 ℃,which is due to the uneven distribution of M+A islands in granular bainite with different shapes,and the majority is large blocks with sharp corners,which results in stress concentration.The second phase precipitates make the material have higher strength.
    Effect of tempering temperature on microstructure and mechanical properties of 42CrMo steel
    Lü Chaoran, Shi Chao, Jiang Weibin, Liu Jinde, Xu Le, Wang Maoqiu
    2021, 46(1):  32-37.  doi:10.13251/j.issn.0254-6051.2021.01.006
    Abstract ( 254 )   PDF (585KB) ( 216 )  
    Through microstructure observation and mechanical properties test,the changes of microstructure and mechanical properties of 42CrMo steel at different tempering temperatures were analyzed.The distribution of elements in the 42CrMo steel tempered at 500 ℃ was analyzed by 3DAP technology,and the influence of Cr,Mn,Mo,etc.on the steel properties was studied.The results show that the microstructure of the steel is tempered troostite when tempered at 450 ℃ after water quenching.In the tempering range of 500-650 ℃,the microstructure are tempered sorbite.With the increase of tempering temperature,granular carbides increase,the tensile strength and the specified plastic elongation strength decrease,and the -40 ℃ low temperature impact performance increases.Tempering at 500 ℃ can reach the mechanical index of grade 12.9 bolts (Rm≥1200 MPa,KV2≥27 J) and obtain the best mechanical properties,and meet the requirements of bolt steel in low temperature environments.The 3DAP results show that the alloying elements in the steel improve the performance of steel through solid solution strengthening and precipitation strengthening.
    Effect of thermal hydrogen treatment on microstructure and properties of TA15 titanium alloy
    Hao Guojian, Yang Gang, Liang Peixin, Zhu Weidong, Sun Jianfei, Chen Zheming
    2021, 46(1):  38-42.  doi:10.13251/j.issn.0254-6051.2021.01.007
    Abstract ( 91 )   PDF (582KB) ( 34 )  
    TA15 titanium alloy specimen with different hydrogen contents was obtained by using a vacuum gas-phase thermal hydrogen treatment furnace,and the cutting force and microstructure of the specimen was tested and observed by means of a machine tool with sensors,and scanning electron microscope,Charpy impact tester,respectively.At the same time,the structural evolution and mechanical properties laws of TA15 titanium alloy specimen with different hydrogen content during thermal hydrogen treatment were studied.The results show that the TA15 titanium alloy specimen have different degrees of microstructure refinement after thermal hydrogen treatment;the main cutting force of the TA15 titanium alloy specimen after thermal hydrogen treatment increases with the increase of hydrogen content,and when the hydrogen content is 0.51%,the main cutting force decreases with the increase of cutting speed.The main cutting force of TA15 titanium alloy specimen with other hydrogen content first increases and then decreases with the increase of cutting speed;the impact absorbed energy of TA15 titanium alloy specimen after thermal hydrogen treatment decreases as the hydrogen content increases.
    Effect of annealing temperature on microstructure and properties of cold rolled low carbon high strength sheet by CSP
    Zhao Xiaolong, Wang Xiong, Luo Xiaoyang, Di Yanjun, Lin Xiaoliang, Feng Li
    2021, 46(1):  43-49.  doi:10.13251/j.issn.0254-6051.2021.01.008
    Abstract ( 76 )   PDF (580KB) ( 43 )  
    Taking low-carbon high-strength cold-rolled sheet as the research object,the microstructure of the annealed cold sheet was observed by using optical microscope,field emission scanning electron microscope and the mechanical properties were tested by using automatic tensile testing machine.The results show that when the tested sheet is annealed between 520 ℃ and 580 ℃,the ferrite grain morphology changes little,it is still elongated;the number of cementite distributed in the microstructure is small,and the yield strength and tensile strength change little,yield ratio remains above 0.9,and the elongation is about 1%.When the tested sheet is annealed between 610 ℃ and 700 ℃,undistorted recrystallized grains appear around the deformed ferrite,the recrystallized grains will grow into equiaxed ferrite with the increase of annealing temperature.The spheroidization process of cementite is the main reason for the increase in the number of granular cementite in the microstructure,and the yield strength and tensile strength decrease rapidly,the elongation increases rapidly,the yield ratio shows a downward trend,reaching a minimum of 0.86 at 670 ℃.When the tested sheet is annealed between 730 ℃ and 760 ℃,the ferrite grains grow sufficiently,the grain morphology changes little,there is almost no freely distributed cementite in the microstructure,the cementite aggregates and distributes only in grain boundaries,and the yield strength and tensile strength decrease slowly,the elongation slowly increases,and the yield ratio increases,reaching 0.91 at 760 ℃.Based on the comprehensive consideration,the optimum annealing tmperature of the tested sheet is 670 ℃.
    Effect of annealing process on microstructure and properties of dual phase steel DP590GA
    Li Huiyuan, Dai Jietao, Xian Lingbiao, Ren Jianping, Li Liejun
    2021, 46(1):  50-54.  doi:10.13251/j.issn.0254-6051.2021.01.009
    Abstract ( 98 )   PDF (584KB) ( 64 )  
    Effects of annealing and rapid cooling processes on the properties and microstructure of C-Mn DP590GA steel were studied.The results show that the Rp0.2 of the tested steel increases with the increase of soaking temperature,and the more significant the increase of Rp0.2 along with the increase of soaking temperature.The elongation of the tested steel increases initially as the soaking temperature increases and decreases afterwards.The strength and plasticity of the tested steel increase and decrease,respectively with the increase of rapid cooling ending temperature.When the soaking temperature of the steel is 820 ℃,the better mechanical properties can be obtained:the Rp0.2 is 400 MPa,the Rm is 625 MPa and the A50 is 25.5%.
    Effect of intercritical tempering temperature on microstructure and mechanical properties of Q690 steel with 7%Mn
    Liu Gang, Sun Xinjun, Liang Xiaokai
    2021, 46(1):  55-60.  doi:10.13251/j.issn.0254-6051.2021.01.010
    Abstract ( 72 )   PDF (639KB) ( 34 )  
    Effect of intercritical tempering temperature on microstructure and mechanical properties of 0.02C-7Mn steel was investigated by means of scanning electron microscope (SEM),X-ray diffraction (XRD),transmission electron microscope (TEM) and Thermo-Calc software calculation.The results indicate that the microstructure is basically quenched martensite accompanied by little amount of retained austenite after direct quenching,while the microstructure is mainly tempered martensite and the reverted austenite (retained austenite) after intercritical tempering.With the increase of tempering temperature,the content of retained austenite gradually increases and the maximum content of retained austenite is 18.78% at 650 ℃.Meanwhile,ε-martensite is appeared and its content is 6.57%.It is the decline of dislocation density and dispersed precipitation during the tempering that has resulted in the decrease of tensile strength and the increase of yield strength in different effects.Furthermore,the existence of ε-martensite not only reduces yield strength but also damages low-temperature toughness.After tempered at 600 ℃,the tested steel has excellent comprehensive mechanical properties (transverse direction:tensile strength of 984 MPa,yield strength of 973 MPa and the -40 ℃ impact absorbed energy of 163 J;rolling direction:tensile strength of 947 MPa,yield strength of 919 MPa and the -40 ℃ impact absorbed energy of 186 J) that can meet the properties requirement of Q690 steel.
    Effect of heat treatment process on microstructure and properties of 510 MPa grade ship steel
    Liu Xuan, Zhao Gang, Li Dahang, Zhou Hongqing, Zhang Youpeng, Zhu Yixuan, Wu Yuxin
    2021, 46(1):  61-64.  doi:10.13251/j.issn.0254-6051.2021.01.011
    Abstract ( 94 )   PDF (581KB) ( 52 )  
    Effects of different heat treatment on the grain size,microstructure,strength and impact absorbed energy of 510 MPa steel were studied by quenching at 870,900,and 930 ℃ and tempering at 620,650 and 680 ℃,respectively.The results show that with the increase of quenching temperature of 870,900 and 930 ℃,the grain size of 510 MPa ship steel becomes 7.5,7 and 6.5 respectively,the strength and the average impact absorbed energy decrease.With the increase of the tempering temperature of 620,650 and 680 ℃,the strength of specimen decreases,and the average impact absorbed energy increases first and then decreases.The 510 MPa grade ship steel has excellent strength and average impact absorbed energy when it is quenched at 900 ℃ for 1.5 h and tempered at 650 ℃ for 2 h.Quenching at 870 ℃ for 1.5 h and tempering at 620 ℃ for 2 h can be selected for higher strength requirements.
    Influence of austenitizing and tempering temperature on microstructure and properties of E550 low-temperature steel
    Xie Zhanglong, Chen Feng, Hu Qilong, Wang Zhaohua
    2021, 46(1):  65-69.  doi:10.13251/j.issn.0254-6051.2021.01.012
    Abstract ( 88 )   PDF (581KB) ( 38 )  
    Microstructure evolution rules of E550 steel austenitized between 850-1000 ℃ and microstructure and properties when quenched and tempered at different temperature were studied by means of OM,SEM,tensile and impact machines.A mathematical model of the relationship between austenitizing temperature and austenite grain size has been established.The results show that the calculated results of the model is in good agreement with the measured values.The microstructure and mechanical properties of the test plates quenched at different temperatures and then tempered at 600 ℃ and 670 ℃ show that prior autstenite grains are fine and uniform when the austenitizing temperature is selected in the range of 880-930 ℃ and a good combination properties can be obtained when tempered at 670 ℃.
    Effect of quenching temperature on mechanical properties and microstructure of 2200 MPa ultra-high strength steel
    Zhang Pengjie, Wang Chunxu, Li Yong, Han Shun, Liu Shaozun
    2021, 46(1):  70-74.  doi:10.13251/j.issn.0254-6051.2021.01.013
    Abstract ( 105 )   PDF (583KB) ( 36 )  
    Effect of quenching temperature on the mechanical properties and microstructure of 2200 MPa ultra-high strength steel was studied by means of mechanical properties test,optical microscope (OM),transmission electron microscope (TEM),X-ray diffraction (XRD) and other analysis methods.The results show that the optimal quenching temperature of the tested steel is 1025 ℃,so the subsequent heat treatment can obtain the best strength and toughness match:the tensile strength is 2244 MPa,the yield strength is 1836 MPa,the U-notch impact absorbed energy is 59 J,and the fracture toughness is 57.7 MPa·m1/2.When the quenching temperature is low,coarse primary carbides appear in Mo-rich M6C carbides,which seriously affect strength and toughness.As the quenching temperature increases,the primary carbide gradually decreases until it completely disappears at 1000 ℃.When the quenching temperature is higher than 1025 ℃,the grains are significantly coarsened,and the grain size becomes the main negative influencing factor.
    Effect of solution treatment on grain growth and hardness of GH4169 alloy
    Fu Jianhui, Zhou Yang, Lai Yu, Chen Qi
    2021, 46(1):  75-79.  doi:10.13251/j.issn.0254-6051.2021.01.014
    Abstract ( 124 )   PDF (583KB) ( 208 )  
    Effect of solid solution treatment on grain growth and hardness of GH4169 alloy was studied under different heating temperatures and holding time.The results show that the δ phase dissolution temperature of the alloy is between 980 ℃ and 1000 ℃.The grain growth of the alloy has different characteristics under different solid solution treatment processes.When the solution treatment temperature is lower than the δ dissolution temperature,the grain growth is slow;when the heat treatment temperature is higher than that,the grain size grows rapidly with the increase of temperature.The kinetic model of grain growth of the alloy during heat treatment above 1000 ℃ is established,with the activation energy of grain growth being 285.013 kJ/mol.The hardness of the alloy decreases with the increase of solution temperature and holding time,and the grain size and hardness of the alloy follow Hall-Petch relation.
    Application of cryogenic treatment in ZL204 aluminum alloy
    Li Jingmin, Li Fengchun, Teng Yu, Zhou Wenfeng, Tang Guangping
    2021, 46(1):  80-83.  doi:10.13251/j.issn.0254-6051.2021.01.015
    Abstract ( 108 )   PDF (584KB) ( 69 )  
    Influence of cryogenic treatment on mechanical properties and residual stress relief effect of ZL204 aluminum alloy was studied.The results show that the tensile strength,yield strength and elongation of the alloy increase when directly cryogenic treated after solution treatment and then artificial aged,and the effect of residual stress relief effect is better than the traditional relief aging and cycle heat treatment after aging.The best residual stress elimination process for ZL204 aluminum alloy is solution treated at 540 ℃ for 9 h with 60 ℃ water quenching,cryogenic treated at -196 ℃ for 1 h then stress relief aged for 1 h,and artificial aged at 175 ℃ for 3 h with air cooling.
    Discussion on a new isothermal normalizing process of 18CrNiMo7-6 carburizing steel
    Niu Wenming, Zhang Guiyang, Zuo Yongping, Wang Tao
    2021, 46(1):  84-87.  doi:10.13251/j.issn.0254-6051.2021.01.016
    Abstract ( 129 )   PDF (580KB) ( 74 )  
    18CrNiMo7-6 carburizing steel is treated with conventional isothermal normalizing,which is prone to produce granular bainite microstructure and difficult to change the secondary strip effectively.Microstructure and performance of the 18CrNiMo7-6 carburizing steel and isothermal normalizing new process were studied.The specific process consisted of,after austenitizing and holding,for the 40 mm specimen,directly immersed in the normalizing liquid and cooled to 700-750 ℃.The specimen was then quickly transferred to the isothermal furnace,at 650 ℃ for 5-7 h.The results show that the equilibrium microstructure of ferrite and lamellar pearlite is obtained by using the new isothermal normalizing process,the granular bainite is eliminated,the grain size is uniform,and there is no obvious crystal mixing,which is beneficial to reduce the heat treatment distortion.The hardness can be guaranteed at 170-185 HBW,which is conducive to machining.
    Effect of heat treatment processes on microstructure and properties of P20 die steel
    Huang Biaocai, Ning Bo, Chen Yuye, Wu Huibin, Wei Yong, Zhan Guangcao, Yan Xiaomin
    2021, 46(1):  88-91.  doi:10.13251/j.issn.0254-6051.2021.01.017
    Abstract ( 132 )   PDF (580KB) ( 55 )  
    Poperties and microstructure of P20 steel with different heat treatment processes of “quenching+tempering”,“normalizing+tempering” and “hot rolling+tempering”,were compared and analyzed by means of Rockwell hardness and scanning electron microscopy (SEM).The results show that in despite of the difference of the hardness before tempering,the change trend of the three specimens were similar showing “slow down - a steep fall - and then slow down again”,and in the range of 580-600 ℃ all the three kinds of specimens showing the “steep fall” trend.The hardness at the “steep fall” is 37.12-32.31 HRC for quenching+tempering specimen,34.87-31.07 HRC for normalizing+tempering specimen and 35.00-31.63 HRC for hot rolling+tempering specimen,which is basically coincides with the range of 28-36 HRC required by GB/T 1299—2014.For the same tempering temperature,the hardness of “quenching+ tempering” specimen is higher than that of “hot rolling &tempering” specimen,while the hardness of “normalizing+tempering” specimen is lower than that of “hot rolling+tempering” specimen.
    MATERIALS RESEARCH
    Effect of niobium on microstructure and properties of high strength 51CrV steel
    Wang Jiamin, Cao Yu, Xiang Haoliang, Cao Xiangzhi, Song Xinli, Liu Zhongzhu
    2021, 46(1):  92-96.  doi:10.13251/j.issn.0254-6051.2021.01.018
    Abstract ( 89 )   PDF (584KB) ( 55 )  
    Effect of niobium addition on austenite grain size,quenching and tempering microstructure and mechanical properties of 51CrV steel was observed by means of optical microscope,scanning electron microscope,transmission electron microscope and universal tensile testing machine.The results show that the austenite grain size of Nb free and 0.02wt%Nb steels is 10.0 μm and 3.1 μm,respectively.The grain size of 51CrV steel with Nb element is significantly refined,the size of lath martensite reduces,and the size of carbide precipitated during tempering is finer.After quenching at 850 ℃ and tempering at 400 ℃,both the yield strength and tensile strength of the two tested steels are greater than 1300 MPa and 1400 MPa,respectively.The elongation of 0.02wt%Nb tested steel increases to 9.50% because of the grain refinement.And the elongation of Nb free steel is 8.69%.51CrV steel microalloyed by Nb element has both high strength and high plasticity and its comprehensive properties are better than Nb-free steel.
    Effect of magnesium and heat treatment on electrical conductivity andmechanical properties of Al-4Si-(xMg) alloys
    Ye Hui, Cui Xiaoli, Cui Hongwei, Li Xinghui, Zhu Ze, Zhao Juan
    2021, 46(1):  97-103.  doi:10.13251/j.issn.0254-6051.2021.01.019
    Abstract ( 80 )   PDF (585KB) ( 33 )  
    Effects of Mg addition and different heat treatments on the electrical conductivity and hardness of Al-4Si-(xMg) (x=0-1.5%,mass fraction) alloys were analyzed by SEM,XRD,EDS,hardness tester and resistivity tester.The results show that for the as-cast alloys,the electrical conductivity and hardness increase first and then decrease with the increase of Mg addition and 1.1% is the optimum addition of Mg,while the Mg addition significantly improves the hardness,but damages the electrical conductivity.After different heat treatments,the electrical conductivity of Al-4Si-(xMg) alloys greatly increases and the hardness slightly decreases,where the solid solution+aging treatment significantly increase the electrical conductivity but reduce the hardness to the minimum,so that the Al-4Si-1.1Mg alloy has the best matching between electrical conductivity and hardness.Through the synergistic effect of Mg addition and solid solution+aging treatment,the electrical conductivity of the as-cast Al-4Si alloy can be improved from 43.3%IACS to 50.9%IACS,the hardness can be increased from 41.5 HV0.5 to 84.3 HV0.5.
    Annealing process and magnetic properties of a new type Fe80.5Si7.2B12.3 amorphous alloy strip
    Song Su, Chen Wenzhi, Zhang Guangqiang, Zheng Wei, Zhang Qian, Xing Yanxing, Zhou Shaoxiong
    2021, 46(1):  104-108.  doi:10.13251/j.issn.0254-6051.2021.01.020
    Abstract ( 87 )   PDF (654KB) ( 50 )  
    Magnetic properties and loss characteristics of a new type Fe80.5Si7.2B12.3 amorphous alloy strip under different annealing processes were studied and compared with the traditional iron-based amorphous alloy Fe80Si9B11.The results indicate that the new type Fe80.5Si7.2B12.3 amorphous alloy strip has a higher saturation magnetic induction intensity than that of Fe80Si9B11,its magnetic flux density value is 1.607 T under the excitation magnetic field intensity of 3500 A/m.After annealing without magnetic field,its magnetic loss value is higher than that of Fe80Si9B11,reaching 0.411 W/kg at f=50 Hz and Bm =1.4 T.After longitudinal magnetic annealing,its magnetic loss is 0.197 W/kg and basically equivalent to that of Fe80Si9B11.After transverse magnetic annealing,its magnetic loss is only 0.175 W/kg,lower than that of Fe80Si9B11,while the initial permeability and constant permeability are better than that of Fe80Si9B11.The optimal annealing temperature range (360-400 ℃) of the new type Fe80.5Si7.2B12.3 amorphous alloy strip is equivalent to that of Fe80Si9B11.
    Development of Nb-V microalloyed hot forming steel based on 22MnB5
    Liu Gang, Gan Yong, Liu Chong, Ma Mingtu, Wu Jian, Yang Yingdong, Hu Chunlin
    2021, 46(1):  109-113.  doi:10.13251/j.issn.0254-6051.2021.01.021
    Abstract ( 92 )   PDF (647KB) ( 36 )  
    Based on the common technical problems of insufficient cold bending performance and strong hydrogen embrittlement sensitivity of existing hot forming steel parts,the design idea of Nb and V microalloying was adopted on the basis of 22MnB5 steel,and the microstructure,hardenability and extreme tip cold bending performance of the tested steels were studied.The results show that the microstructure of hot forming steel 22MnB5 before and after microalloying is all martensite,while becomes finer after microalloying;Nb-V microalloying can effectively improve the hardenability of the 22MnB5 hot forming steel,the depth of hardened layer reaches 13-14 mm,and the extreme tip cold bending angle of the tested steels reaches 58°-72°,which further widens the processing window of hot forming forming.Based on the test results of microstructure,hardenability and extreme tip cold bending performance of the tested steels,the comprehensive strength and plasticity of the steel are improved by adding 0.04%Nb and 0.04%V,and meet the requirements of automotive parts with high extreme tip cold bending performance.
    Effect of Nb microalloying on microstructure and properties of Cr-Ni-Mo carburized gear steel
    Gui Weimin, Liu Yi, Zhou Genshu, He Liangliang, Wang Mengmeng, Tang Wenxin
    2021, 46(1):  114-119.  doi:10.13251/j.issn.0254-6051.2021.01.022
    Abstract ( 78 )   PDF (648KB) ( 45 )  
    Effect of Nb on microstructure and properties of Cr-Ni-Mo alloyed gear steel under different carburizing processes was investigated.The results show that Nb element has little influence on surface hardness,retained austenite content and non-martensite microstructure in the carburizing layer under different carburizing processes.However,the test steel with Nb element refining grain can make the effective hardening depth deepen by 10% and obtain a finer surface lamellar structure of lath martensite after a longer carburizing process.
    Development of cold-rolled 800 MPa grade high strength low alloy steel for automobile
    Wang Keqiang, Liu Rendong, Guo Jinyu, Fu Wei, Huang Qiuju, Sun Rongsheng
    2021, 46(1):  120-124.  doi:10.13251/j.issn.0254-6051.2021.01.023
    Abstract ( 111 )   PDF (648KB) ( 52 )  
    Cold-rolled 800 MPa low alloy high strength steel with good ductility and formability was developed by means of C-Si-Mn-Nb-Ti-Cr-Mo chemical composition design and key production process parameters control.The results show that the microstructure of the tested steel is composed of ferrite,martensite and a small amount of bainite.The second phase particles and carbide precipitation phases are dispersed in the ferrite matrix.The yield strength of the tested steel is more than 800 MPa,the elongation is more than 10.5%,the difference between tensile strength and yield strength is less than 35 MPa,the hole expansion rate is more than 56.5%,and there is no visible crack on the 180° cold bending test,which showing good formability.
    SURFACE ENGINEERING
    Effect of surface oxidizing at 550 ℃ on wear resistance of Ti-6Al-4V alloy
    Yang Jie, Zhang Qingke, Li Qiong, Song Zhenlun, Wu Xiaochun
    2021, 46(1):  125-132.  doi:10.13251/j.issn.0254-6051.2021.01.024
    Abstract ( 67 )   PDF (653KB) ( 35 )  
    Thermal oxidation (TO) of Ti-6Al-4V alloy was performed at 550 ℃ for 60 h in air,and the surface morphology,microstructure,composition,hardness,scratch performance and wear resistance of the TO treated and untreated alloy were evaluated and compared.The results reveal that the surface roughness of the Ti alloy increases a little after TO,an oxygen-diffusion layer of about 3.5 μm thickness is formed on the surface,and anatase,rutile,brookite TiO2 and Al2O3 phases are detected by X-ray diffraction (XRD).The microhardness and nano hardness of the oxygen-diffusion layer are 804.6 HV0.025 and 14.5 GPa,respectively,which is 143.7% higher than that of the untreated substrate,and no cracking is observed around the indentations.The maximum scratch depth is significantly reduced from 12 μm to 4 μm after TO,and the wear rate decreases from 354.33×10-6 mm3/Nm to 1.44×10-6 mm3/Nm,and the main wear mechanism of the oxygen-diffusion layer is slight abrasive wear.It is concluded that the surface TO treatment considerably increases the surface hardness and wear resistance of the Ti-6Al-4V alloy,but leads no obvious inner microstructure coarsening and softening,thus could be a potential method to improve the surface wear resistance of Ti alloys.
    Effect of rare earth Ce on properties of high-boron bainite coating prepared by laser cladding
    Zhang Jian, Huang Daosi, Zhao Longzhi, Jiao Haitao, Tang Yanchuan, Liu Dejia, Zhao Mingjuan, Li Jin
    2021, 46(1):  133-137.  doi:10.13251/j.issn.0254-6051.2021.01.025
    Abstract ( 85 )   PDF (647KB) ( 28 )  
    High boron bainite coatings with different Ce contents were prepared by laser cladding,then the microstructure,microhardness,fracture toughness,wear performance of the costings were studied by using SEM,microhardness tester,universal tensile machine,reciprocating friction and wear tester,respectively.The results show that the grain size of primary austenite decreases,and the morphology of intergranular trellis boride is improved after Ce modification.The three-point bending fracture toughness is improved,and the fracture changes from intergranular brittle fracture to quasi-cleavage fracture.With the increase of Ce content,the average friction coefficient of the coatings decreases first and then increases,and serious fatigue peeling occurs in all the wear marks.
    Preparation of Ti3SiC2 coating by electrical explosion powder spraying method
    Liu Zonghan, Zhu Liang, Lin Qiaoli, Zhang Aihua, Li Chu
    2021, 46(1):  138-142.  doi:10.13251/j.issn.0254-6051.2021.01.026
    Abstract ( 77 )   PDF (650KB) ( 32 )  
    Ti3SiC2 coating was prepared with Ti3SiC2 powder as electrical spraying material by using self-made continuous powder-feeding electrical explosion spraying equipment.According to the surface morphologies and cross-sectional characteristics of the prepared coating,the effects of charging voltage,powder particle size,and graphite blending amount on the electrical explosion spraying process were analyzed.The results show that when the particle size of the powder is 28 μm,the charging voltage is higher than 15 kV,and the appropriate amount of graphite powder is 10%,the coating deposition rate is higher and the uniformity is better.The XRD analysis results show that the coating is composed of TiC and Ti3SiC2.The bonding strength of the coating determined by using the cemented dual sample tensile test method is greater than 37 MPa.Therefore,graphite powder blending can improve the conductivity of the powder during electrical explosion,reduce the surface discharge of the outer edge of the powder particles,make the powder to be heated more thoroughly,and help the coating formation.
    Effect of chromium transition layer on interface bonding strength between chromium nitride film and magnesium alloy substrate
    Liu Ruixia, Guo Feng, Han Haipeng
    2021, 46(1):  143-148.  doi:10.13251/j.issn.0254-6051.2021.01.027
    Abstract ( 71 )   PDF (646KB) ( 28 )  
    To improve the bonding strength of magnetron sputtering chromium nitride film and magnesium alloy substrate,the chromium transition layer was deposited by different magnetron puttering processes between them,the influence of chromium transition layer on interface bonding strength between film and substrate and its mechanism were analyzed and discussed.The results show that adding chromium transition layer can increase the fracture critical load of film which characterizes the bonding strength of film and substrate,and the fracture critical load of film reaches the largest when the magnetron sputtering process of chromium transition layer is 100 W of sputtering power,30 V of negative bias voltage,25 ℃ of substrate temperature and 4 min of sputtering time,in which process the surface of chromium transition layer has the largest roughness and the smallest protuberance interval.The enhancing action of chromium transition layer on interface bonding is mainly reflected by improving the bonding between chromium nitride and magnesium alloy substrate,it is related to the larger contact area and the effective mechanical interlock between chromium transition layer and chromium nitride film,as well as the reduction of interface stress by chromium transition layer.
    Shot peening process of directionally solidified DZ125 alloy
    Wang Xin, Yang Qing, Yu Peng, Ma Shicheng
    2021, 46(1):  149-153.  doi:10.13251/j.issn.0254-6051.2021.01.028
    Abstract ( 76 )   PDF (650KB) ( 44 )  
    Cast-steel shot peening was employed on directionally solidified alloy DZ125 to analyze the fatigue property,surface residual stress and microhardness profile under various shot peening intensity and coverage conditions.The results show that with the increase of shot peening intensity,the estimated median fatigue life increases gradually.At high intensity,the estimated median fatigue life at 700 ℃/500 MPa is 2 times that of the original specimen.Moreover,with the increase of surface coverage,the estimated median fatigue life increases first and then stabilizes,and when the coverage reaches 400%,the estimated median fatigue life is stable.When the shot peening intensity is high and at the coverage rate of 400%,the fatigue limit is 480 MPa,which is 20% higher than the original value (400 MPa).Residual stress and microstructure strengthening mechanism are the strengthening factors of shot peening for DZ125 alloy.With the increase of shot peening intensity,the residual compressive stress decreases slightly,but it is still obviously larger than the original state.When the shot peening intensity is high and at the coverage rate of 400%,the surface hardness field of DZ125 alloy exceeds 200 μm in depth,and the surface hardness is 37% higher than that of the matrix (430 HV0.1).When the actual load at the notch is greater than the yield strength,the residual stress and hardness are relaxed obviously during fatigue process;the surface residual stress of the fractured specimen decreases by 54% and the surface hardness decreases by 14% after 700 ℃/600 MPa/1.5×105 cycles.
    MICROSTRUCTURE AND PROPERTIES
    Research progress on precipitation-free zone of aluminum alloy
    Liao Bin, Cao Lingfei, Wu Xiaodong
    2021, 46(1):  154-160.  doi:10.13251/j.issn.0254-6051.2021.01.029
    Abstract ( 99 )   PDF (647KB) ( 73 )  
    Researches of precipitation-free zone (PFZ) in aluminum alloy over the past 50 years were reviewed and the main formation mechanism and influencing factors and the influence of PFZ on the properties (mainly mechanical properties and corrosion resistance) of the alloy were emphatically discussed.The different view points of the related theories of PFZ on the formation mechanism and properties of the alloy were systematically introduced.Finally,the difficulty and key research direction of PFZ in aluminum alloy were put forward.
    Effect of aging treatment on microstructure and corrosion resistance of new Al-5.6Zn-1.6Mg-0.15Zr alloy
    Huang Yuanchun, Tan Weiyang, Zhang Chuanchao, Wang Yanling
    2021, 46(1):  161-166.  doi:10.13251/j.issn.0254-6051.2021.01.030
    Abstract ( 86 )   PDF (650KB) ( 33 )  
    Changes in the microstructure,corrosion states,and corrosion resistance of Al-5.6Zn-1.6Mg-0.15Zr alloy sheet after aging at 120 ℃ for different time were studied by means of intergranular corrosion experiment (IGC),exfoliation corrosion experiment (EXCO) and electrochemical corrosion experiment,optical microscope (OM),scanning electron microscope (SEM),energy spectrum analysis (EDS) and transmission electron microscope (TEM).The results show that the new Al-5.6Zn-1.6Mg-0.15Zr alloy has good overall corrosion resistance,and its sensitivity to intergranular corrosion and spalling corrosion decreases significantly with the increase of aging time.The polarization curve obtained by electrochemical corrosion experiments also shows the same trend.The effect of aging on corrosion resistance of the alloy is mainly related to the change of grain boundary precipitation phase η (MgZn2) and the precipitation-free zone (PFZ).With the increase of aging time,the grain boundary precipitation phase aggregates and coarsens,and changes from continuous precipitation to discontinuous precipitation,and the PFZ becomes wider.These changes cause the anodic corrosion channel to be cut off,and the corrosion cannot continue,thereby improves the corrosion resistance of the alloy.
    Microstructure evolution and aging behavior of Mg-Zn-Y alloy processed by high pressure torsion
    Wang Jinhui, Yin Xiaoming, Li Yansheng, Qu Cheng, Xu Rui
    2021, 46(1):  167-172.  doi:10.13251/j.issn.0254-6051.2021.01.031
    Abstract ( 63 )   PDF (647KB) ( 39 )  
    Microstructure evolution and aging behavior of high-pressure torsion (HPT) deformed Mg-Zn-Y alloy were studied by using transmission electron microscope (TEM),scanning electron microscope (SEM),X-ray diffraction (XRD) instrument and microhardness tester. The results show that before and after HPT deformation,the second phase particles in the alloy are W phase and Mg24Y5 phase,and the formation of any new precipitates is not observed after HPT processing,indicating that HPT deformation does not lead to phase transformation of the alloy.At the same time,it is found that the HPT deformation process is accompanied by the generation of deformation twins and the multiplication of a large number of dislocations.The deformation twins are subdivided by the second phase particles during the HPT process.Compared with undeformed alloys,HPT deformation can accelerate the aging process,that is,reach a relatively high peak hardness under a shorter aging time.The specimens after HPT deformed 7 turns of are aged at 175 ℃ for 8 h,the peak microhardness reaches about 114 HV0.1.After aging treatment,the precipitated phase preferentially nucleates at the dislocations and twin boundary,indicating that dislocations and twin boundary act as preferential nucleation sites for the precipitated phases.
    Effect of Zr and solution treatment on corrosion resistance of Mg-1.5Zn-0.5Ca-0.8Ce alloy
    Yao Xudong, Sun Bolin, Cai Zhenfei, Jiang Bin, Ma Yangzhou, Feng Xiaohua, Song Guangsheng
    2021, 46(1):  173-180.  doi:10.13251/j.issn.0254-6051.2021.01.032
    Abstract ( 73 )   PDF (650KB) ( 59 )  
    Taking Mg-1.5Zn-0.5Ca-0.8Ce alloy as the research object,alloying and solution treatment were carried out respectively to study the effect of Zr addition and solution treatment on the corrosion resistance of magnesium alloy Mg-1.5Zn-0.5Ca-0.8Ce,and to explore the mechanism of alloying and heat treatment on the corrosion resistance of magnesium alloy.The results show that both the addition of Zr and the solution treatment can effectively improve the corrosion resistance of the material,among which the Mg-1.5Zn-0.5Ca-0.8Ce-0.7Zr magnesium alloy specimen solution treated has the best corrosion resistance.It can be concluded that both the alloying and heat treatment have important effects on microstructure and corrosion resistance of the magnesium alloy.
    Effect of post-processing on microstructure and mechanical properties of selective laser melting K536 alloy
    Wang Dong, Su Mengyao, Mo Zhanhai, Xu Xingxing, Zhou Xiaowei, Xie Xiaolin
    2021, 46(1):  181-186.  doi:10.13251/j.issn.0254-6051.2021.01.033
    Abstract ( 74 )   PDF (646KB) ( 33 )  
    K536 alloy was formed by selective laser melting then post-processed.The microstructure and mechanical properties of the alloy were analyzed in as-deposited,as-annealed,and as-annealed+solid solution treated,as-annealed+solid solution treated+hot isostatic pressed,respectively.The results show that microcracks form in the transversal and longitudinal sections of the as-deposited specimens.For the as-annealed specimens,the transversal section microstructure is composed of equiaxed grains and the longitudinal one is of columnar grains,and the grain size fluctuates greatly,forming alternating fine and coarse-grained areas.Partial recrystallization occurs in the as-annealed+solid solution treated specimens,with twin crystals being observed in the recrystallized part.In addition,there are obvious equiaxed grain structure,uneven grain size,and grain boundary precipitates with long strip shape.After the hot isostatic pressing,the grain size of specimens increases obviously,the deposition generated cracks are basically healed,and the high-temperature durability index meets the requirements of related ASTM standard.The transgranular carbides are evenly distributed,and the carbides at the grain boundary are in chains.
    Effect of bainite content on mechanical properties of ferrite/bainite(F/B) dual phase pipeline steel
    Shi Xianbo, Yin Peihua, Yan Wei, Shan Yiyin, Ren Yi
    2021, 46(1):  187-192.  doi:10.13251/j.issn.0254-6051.2021.01.034
    Abstract ( 71 )   PDF (647KB) ( 46 )  
    A ferrite/bainite (F/B) dual-phase pipeline steel was heat treated at 700,720,740,and 760 ℃ in the dual-phase region and steel specimens with 4 different volume fractions (16%,28%,41%,48%)of bainite were obtained.The effect of volume fraction of bainite on the strength,plasticity and toughness of the steel was studied by using SEM,TEM and mechanical properties test.The results show that the F/B dual-phase microstructure has lower yield strength and comparable tensile strength,resulting in better strain capacity,namely,lower yield ratio,higher elongation and work hardening exponent compared with that of as-rolled original microstructure.The volume fraction of bainite has little effect on the strength,elongation and work hardening exponent for the F/B dual-phase pipeline steel,however,it plays an significant role in impact property.The excellent strength,plasticity and toughness can be obtained when the volume fraction of bainite is around 40%.
    Precipitation behavior of super austenitic stainless steel containing copper
    Li Bingbing, Chen Haitao, Lang Yuping, Qu Huanpeng, Tian Zhiling, Chen Qingming
    2021, 46(1):  193-199.  doi:10.13251/j.issn.0254-6051.2021.01.035
    Abstract ( 77 )   PDF (650KB) ( 47 )  
    Cu-containing super austenitic stainless steel was solution treated at 1200 ℃ for 2 h and aged at 600,700,800,900,1000 and 1100 ℃ for 2 h respectively,then the precipitated phases were studied by using Thermo-Calc,SEM,EDS and TEM.The results show that the precipitated phases at 600-800 ℃ are mainly intergranular σ phase,that at 1000 ℃ are intergranular bulk σ phase,rod-shaped Laves phase,and the long needle-like and fusiform χ phase,while that at 1100 ℃ no precipitation.As the temperature rises,the size of the precipitates increases,the total amount of precipitates first increases then decreases and reaches its peak value at 900 ℃,and the precipitation of Laves and χ phases is promoted with the increase of Cu content.
    Effect of finishing rolling temperature on microstructure, texture and formability of ferritic stainless steel 443
    Ren Juanhong, Chen Anzhong, Wang Changbo, Qian Zhangxin, Gao Renqiang
    2021, 46(1):  200-203.  doi:10.13251/j.issn.0254-6051.2021.01.036
    Abstract ( 57 )   PDF (654KB) ( 27 )  
    Effect of finishing rolling temperature on microstructure,texture,formability and surface ridging resistance of ultra-purified ferritic stainless steel 443 was investigated by means of optical microscope,EBSD and other analysis technologies.The results show that lowering the finishing rolling temperature promotes recrystallization of both hot rolled and annealed steel sheets,and makes the microstructure of final cold rolled-annealed sheet refined and homogenized.The γ-fiber texture in cold rolled-annealed state can be strengthened effectively by reducing the final rolling temperature,which is an effective way to improve the r value,cupping value,formability and surface ridging resistance.
    Hot ductility of brake disc CrMoV steel for high speed railway
    Wang Chengming, An Zhiguo, Sun Xiaoran, Sun Yan, Hai Yan
    2021, 46(1):  204-208.  doi:10.13251/j.issn.0254-6051.2021.01.037
    Abstract ( 67 )   PDF (529KB) ( 35 )  
    Hot ductility tests of brake disc CrMoV steel for high speed railway were carried out at temperatures between 600-1350 ℃ by a Gleeble-3800 thermal simulator,the fracture morphology was observed by means of scanning electron microscopy and the microstructure section fracture was observed by optical microscope.The results show that there are three brittle temperature zones for the experimental steel in the range of 600-1350 ℃,Ⅰ brittle zone is from melting point to 1320 ℃,Ⅱ brittle zone 1100-1000 ℃ and Ⅲ brittle zone 800-650 ℃.In the Ⅱ brittle zone,precipitates of V(C,N) and VN at grain boundary is the main cause of deterioration in ductility.It is imperative to avoid those zones when drawing up the rolling schedules.
    Effect of β annealing parameter on microstructure and properties of Ti6Al4V titanium alloy
    Tan Haibo, Shi Zhoulong, Zhang Shumei, Zhu Juanjuan
    2021, 46(1):  209-213.  doi:10.13251/j.issn.0254-6051.2021.01.038
    Abstract ( 75 )   PDF (529KB) ( 52 )  
    Lamellar structure produced by β annealing of titanium alloy can significantly improve the damage tolerance of the material.In this paper,the effect of β annealing parameter on microstructure and properties of Ti6Al4V alloy was analyzed and discussed through experiments.The experimental results show that with the annealing temperature increases in the range of Tβ+10 ℃-Tβ+50 ℃,the β grain size grows continuously.When the temperature increases to Tβ+50 ℃,the strength and plasticity of the alloy decrease obviously.The holding time of β annealing is basically the same as the effect of annealing temperature on microstructure and properties.The strength and plasticity decreases but the fracture toughness increases with the holding time prolonging.The stress relief annealing increases within a certain range,the α lamellar thickness increases,the strength decreases,but the plasticity and fracture toughness increase.After β annealing,the cooling rate has remarkably influence on the microstructure and properties of the material.The greater the cooling rate is,the thickness of lamellar,grain boundary width and α lamellar thickness are obviously reduced,the strength is increased,but the plasticity is decreased.
    NUMERICAL SIMULATION
    Fluid-thermal-solid coupling simulation analysis of thermohydrogen treatment furnace specially for large aviation components
    Qiao Da, Bian Xiangde, Fu Jinglun, Ding Linchao, Wang Tong, Lu Wenlin
    2021, 46(1):  214-219.  doi:10.13251/j.issn.0254-6051.2021.01.039
    Abstract ( 76 )   PDF (520KB) ( 43 )  
    Structure of the large-scale thermohydrogen treatment furnace designed with cold wall structure is complex,and the thickness of heat insulation panel of multi-layer heat insulation structure furnace lining is very thin,which makes meshing and simulated calculation to be very difficult.So the full-size fluid-thermal-solid coupling simulation of the thermohydrogen treatment furnace was realized by adopting a simplified idea of equivalent thermal resistance and assuming the multi-layer furnace structure being equivalent to one layer,which still ensures the calculation accuracy and can save the calculation resources.The results of evaluation of furnace heat insulation effect show that when the furnace temperature is 1000 ℃,the outer wall temperature of the furnace is only 200-350 ℃ and distributed in a stripe shape.The outer wall temperature of the furnace shell designed by the cold wall structure is about 25 ℃,which has good heat preservation and heat insulation effect.The maximum thermal stress is 264 MPa,which is located at the base of the material platform.The tensile test results show that the tensile strength of Q235 steel used for the material platform base is about 565 MPa after hydrogen permeation treatment at 300 ℃,and the safety factor is 2.14.Such temperature field and thermal stress field analyses of the furnace and safety reserve coefficient evaluation in this study may provide ideas for the full-scale simulation of large-scale thermohydrogen treatment furnace,and data support for the furnace structural design.
    Post-weld heat treatment distortion of longitudinal welds of steel containment vessel for nuclear power plant
    Hu Guangze, Wang Gang, Yu Jie, Yan Guizhen
    2021, 46(1):  220-224.  doi:10.13251/j.issn.0254-6051.2021.01.040
    Abstract ( 68 )   PDF (522KB) ( 45 )  
    Based on the SYSWELD software,a finite element model was established for the cylinder ring of steel containment vessel.The heat treatment process of longitudinal weld of the cylinder was simulated by finite element method.The distortion and residual stress after heat treatment were calculated.The distortion data of numerical simulation analysis were compared with the measured data.It is proved that the proposed process meets the technical requirements of the product and can provide reference for local post-welding heat treatment of super large vessels.
    TEST AND ANALYSIS
    EBSD scanning area parameter optimization based on quantification of retained austenite in steel
    Cui Guibin, Ju Xinhua, Meng Yang, Yin Lixin
    2021, 46(1):  225-229.  doi:10.13251/j.issn.0254-6051.2021.01.041
    Abstract ( 79 )   PDF (527KB) ( 46 )  
    In order to optimize the EBSD scan area parameters based on the quantification of retained austenite,the relationship between the confidence interval and type A standard uncertainty and the scan area parameters were studied and discussed in detail.The research shows that according to comprehensively considering the main influencing factors such as the number of scanning fields (n≥6),confidence interval,type A standard uncertainty,and analysis time related to the optimization of scanning area parameters,the total scanning area must reach 65 000 μm2.
    Analysis and control of color difference and black spots defects on the surface of DP980-GA dual-phase steel
    Zhang Peng, Liu Xueliang, Zhou Yu, Jia Dongmei
    2021, 46(1):  230-234.  doi:10.13251/j.issn.0254-6051.2021.01.042
    Abstract ( 156 )   PDF (518KB) ( 98 )  
    Causes of color difference and black spots defects on the coating surface of DP980-GA dual phase steel were analyzed by means of SEM,and the mechanism of defects formation was discussed.The results show that insufficient wet gas,too high content of hydrogen in annealing heating section and too low temperature of strip in annealing rapid cooling section cause the oxidation and enrichment of alloy elements Mn and Cr on the surface of strip,which affects the uniformity of diffusion between Zn and Fe;too high immersing temperature of strip after heat treatment increases the galvannealing degree of coating and causes significant diffusion of Fe from the boundary of alloy oxidation.During practical production,technological measures were adopted such as adjusting the amount of wet gas injection in annealing heating section,changing wet gas injection mode from single side to double side,increasing the temperature of strip in annealing rapid cooling section and decreasing hydrogen content of annealing heating section and the immersing temperature of strip,and color difference and black spots defects on the surface of alloy coating were effectively controlled.
    Failure analysis of gear fracture cracking during bench test
    He Liangliang, Wang Yuandong, Wang Mengmeng, Hou Shengwen, Wang Yan
    2021, 46(1):  235-238.  doi:10.13251/j.issn.0254-6051.2021.01.043
    Abstract ( 106 )   PDF (524KB) ( 62 )  
    Causes of gear fracture failure were analyzed by means of metallographic analysis,fracture analysis,tooth profile and lead analysis.The results show that though the surface unqualified non-martensite structure of the root was observed,it is not the main cause of this gear fracture.The main reason is the presence of large-scale oxide inclusion on the root subsurface of gear teeth,which is the fatigue source under the continuous stress during bench test,and leads to the fish-eye type fatigue cracking.